CN102993835A - Fireproof and high temperature resistant coating - Google Patents
Fireproof and high temperature resistant coating Download PDFInfo
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- CN102993835A CN102993835A CN2012104224040A CN201210422404A CN102993835A CN 102993835 A CN102993835 A CN 102993835A CN 2012104224040 A CN2012104224040 A CN 2012104224040A CN 201210422404 A CN201210422404 A CN 201210422404A CN 102993835 A CN102993835 A CN 102993835A
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Abstract
The invention relates to a fireproof and high temperature resistant coating comprising the following components by weight: 20-25 parts of polybutylene, 10-13 parts of decabromodiphenyl ether, 5-8 parts of fireproof short fiber, 4-6 parts of ethyecellulose, 3-5 parts of hexamethylenetetramine, 4-8 parts of titanium dioxide, 5-8 parts of dibutyl benzoate, 2-4 parts of pentaerythritol, 1-5 parts of plaster, 8-11 parts of acrylate resin, 10-15 parts of fire retardant, 2-5 parts of foaming agent, 0.8-2.5 parts of reinforcing agent and 10-20 parts of solvent, wherein the fire retardant is borax or aluminum borate, the foaming agent is ammonium carbonate or melamine, and the reinforcing agent is phenolic fiber or glass fiber. According to the fireproof and high temperature resistant coating provided by the invention, a coating formulation is improved, an environment-friendly flame resistant material is selected, some inorganic materials are added, the high temperature resistant performance of the coating is improved while the coating is fireproof, and the fireproof performance meets the demands of national regulation.
Description
Technical field
The invention provides a kind of fire-proof high-temperature resistant coating, belong to technical field of coatings.
Background technology
Building Fire Protection is a key areas of science and technology of fire protection, and frie retardant coating is the important component part in the fire-proof construction material.Frie retardant coating is coated on body surface, and itself the difficult combustion or do not fire of filming when meeting fire has the better protecting effect to base material, for fire extinguishing and personnel withdraw the time won, therefore its research and application has been caused the great attention of countries in the world.The research starting evening of China's fire-proof high-temperature resistant coating, present frie retardant coating is a kind of to be that the organic polymer that adopts difficulty to fire is base-material, another is to add fire retardant at coating, representative halogen system, phosphorus are that frie retardant coating is in the development, but some bromine class frie retardant coatings are controversial because of environmental issue in the halogen system.Although can stand the baking of high temperature for inorganic fireproof coating, the defective such as it adheres to relatively poor, and intensity is low, and it is more crisp to film.
Summary of the invention
The purpose of this invention is to provide a kind of fire-proof high-temperature resistant coating, by improving formulation for coating material, select feature of environmental protection fire retardant material, add some inorganic materials, fp improves the resistance to elevated temperatures of coating simultaneously.
To achieve these goals, technical scheme of the present invention is: a kind of fire-proof high-temperature resistant coating, include following component by weight: 20～25 parts of polybutene, 10～13 parts of decabromodiphynly oxides, 5～8 parts on staple fibre of fire prevention, 4～6 parts of ethyl cellulose, 3～5 parts of vulkacit Hs, 4～8 parts of titanium dioxide, 5～8 parts of phenylformic acid dibutylesters, 2～4 parts of tetramethylolmethanes, 1～5 part in gypsum, 8～11 parts of acrylate resins, 10 ~ 15 parts of fire retardants, 2 ~ 5 parts of whipping agents, 0.8 ~ 2.5 part of toughener, 10～20 parts of solvents.
Described fire retardant is borax or aluminum borate.
Described whipping agent is amine carbonate or trimeric cyanamide.
Described toughener is phenolic fibre or glass fibre.
Preparation method: solvent, polybutene, decabromodiphynly oxide, vulkacit H, titanium dioxide, phenylformic acid dibutylester, tetramethylolmethane, gypsum, acrylate resin, fire retardant are mixed in proportion, grind again; Then add fire prevention staple fibre, ethyl cellulose, whipping agent stirring and evenly mixing, add at last toughener, stir packing and get final product.
Fire-proof high-temperature resistant coating provided by the invention is selected feature of environmental protection fire retardant material by improving formulation for coating material, adds some inorganic materials, and fp improves the resistance to elevated temperatures of coating simultaneously, and fire resistance meets national regulation.
Embodiment
Embodiment 1:
A kind of fire-proof high-temperature resistant coating, include following component by weight: 20 parts of polybutene, 10 parts of decabromodiphynly oxides, 5 parts on staple fibre of fire prevention, 4 parts of ethyl cellulose, 3 parts of vulkacit Hs, 4 parts of titanium dioxide, 5 parts of phenylformic acid dibutylesters, 2 parts of tetramethylolmethanes, 1 part in gypsum, 8 parts of acrylate resins, 10 parts in sand, 2 parts of amine carbonates, 0.8 ~ 2.5 part of phenolic fibre, 10 parts of etoh solvents.
Embodiment 2:
A kind of fire-proof high-temperature resistant coating, include following component by weight: 25 parts of polybutene, 13 parts of decabromodiphynly oxides, 8 parts on staple fibre of fire prevention, 6 parts of ethyl cellulose, 5 parts of vulkacit Hs, 8 parts of titanium dioxide, 8 parts of phenylformic acid dibutylesters, 4 parts of tetramethylolmethanes, 5 parts in gypsum, 11 parts of acrylate resins, 15 parts of aluminum borates, 5 parts of trimeric cyanamides, 2.5 parts in glass fibre, 20 parts of etoh solvents.
Performance test
When the frie retardant coating in above-described embodiment is used for wood substrate, carry out the fire resistance test according to GB12442.1-95, when above paint formulation is 1 mm when dry film Baidu, after toasting 30 min with spirit lamp, investigate the carbonization situation of coating expansion height and wood substrate, disclosed frie retardant coating is as contrast in the patent CN92102102.
Table 1 embodiment 1 and 2 and the performance test data of reference examples
| Test subject | Detection method | Embodiment 1 | Embodiment 2 | Reference examples |
| Sticking power | GB/T1720-89 | 1 grade | 1 grade | 2 grades |
| Surface drying time | GB/T1728-89 | 1 hour | 1 hour | 2 hours |
| Wood substrate carbonization situation | ? | Carbonization does not occur under 120 ℃ | Carbonization does not occur under 120 ℃ | Carbonization appears |
Claims (4)
1. fire-proof high-temperature resistant coating, include following component by weight: 20～25 parts of polybutene, 10～13 parts of decabromodiphynly oxides, 5～8 parts on staple fibre of fire prevention, 4～6 parts of ethyl cellulose, 3～5 parts of vulkacit Hs, 4～8 parts of titanium dioxide, 5～8 parts of phenylformic acid dibutylesters, 2～4 parts of tetramethylolmethanes, 1～5 part in gypsum, 8～11 parts of acrylate resins, 10 ~ 15 parts of fire retardants, 2 ~ 5 parts of whipping agents, 0.8 ~ 2.5 part of toughener, 10～20 parts of solvents.
2. fire-proof high-temperature resistant coating according to claim 1, it is characterized in that: described fire retardant is borax or aluminum borate.
3. fire-proof high-temperature resistant coating according to claim 1, it is characterized in that: described whipping agent is amine carbonate or trimeric cyanamide.
4. fire-proof high-temperature resistant coating according to claim 1, it is characterized in that: described toughener is phenolic fibre or glass fibre.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210422404.0A CN102993835B (en) | 2012-10-30 | 2012-10-30 | Fireproof and high temperature resistant coating |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210422404.0A CN102993835B (en) | 2012-10-30 | 2012-10-30 | Fireproof and high temperature resistant coating |
Publications (2)
| Publication Number | Publication Date |
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| CN102993835A true CN102993835A (en) | 2013-03-27 |
| CN102993835B CN102993835B (en) | 2015-01-07 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201210422404.0A Expired - Fee Related CN102993835B (en) | 2012-10-30 | 2012-10-30 | Fireproof and high temperature resistant coating |
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| CN (1) | CN102993835B (en) |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103305066A (en) * | 2013-06-26 | 2013-09-18 | 关锦池 | Fireproof coating |
| CN104031509A (en) * | 2014-06-26 | 2014-09-10 | 无锡市崇安区科技创业服务中心 | Exterior wall coating for old wall reconstruction and preparation method thereof |
| CN104974572A (en) * | 2015-06-23 | 2015-10-14 | 苏州博利迈新材料科技有限公司 | Nano particle compound type anticorrosive coating and preparation method therefor |
| CN105131732A (en) * | 2015-08-13 | 2015-12-09 | 蚌埠市时代电子有限公司 | Long-acting led heat-dissipating coating material and preparation method thereof |
| CN107140928A (en) * | 2017-06-20 | 2017-09-08 | 和县明生环保材料有限责任公司 | A kind of waterproof and heat-insulating exterior coating and its production technology |
| CN107163798A (en) * | 2017-06-30 | 2017-09-15 | 朱燕萍 | A kind of fireproof coating |
| CN107236393A (en) * | 2017-07-26 | 2017-10-10 | 合肥铭佑高温技术有限公司 | A kind of fire resistant coating and preparation method thereof |
| CN112694815A (en) * | 2020-12-03 | 2021-04-23 | 湖南格仑新材股份有限公司 | Graphene heat dissipation coating, preparation method and application thereof |
| CN116239907A (en) * | 2023-03-29 | 2023-06-09 | 汪辉 | High-temperature-resistant fireproof coating and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1423981A (en) * | 2001-12-10 | 2003-06-18 | 侯关荣 | Natural fibre cigarette tip and production thereof |
| CN101113280A (en) * | 2006-07-28 | 2008-01-30 | 中宏（天津）实业有限公司 | Method for producing water-proof, fire-proof, antiseptic, heat-insulation, heat-preservation, insulating waterproofing paint |
| CN101386719A (en) * | 2008-08-28 | 2009-03-18 | 冯守中 | Multifunctional coatings and preparation method thereof |
| CN101724302A (en) * | 2009-12-02 | 2010-06-09 | 山东鲁阳股份有限公司 | Light inorganic silicate fiber reinforcing fireproof paint and preparation method thereof |
-
2012
- 2012-10-30 CN CN201210422404.0A patent/CN102993835B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1423981A (en) * | 2001-12-10 | 2003-06-18 | 侯关荣 | Natural fibre cigarette tip and production thereof |
| CN101113280A (en) * | 2006-07-28 | 2008-01-30 | 中宏（天津）实业有限公司 | Method for producing water-proof, fire-proof, antiseptic, heat-insulation, heat-preservation, insulating waterproofing paint |
| CN101386719A (en) * | 2008-08-28 | 2009-03-18 | 冯守中 | Multifunctional coatings and preparation method thereof |
| CN101724302A (en) * | 2009-12-02 | 2010-06-09 | 山东鲁阳股份有限公司 | Light inorganic silicate fiber reinforcing fireproof paint and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 沈春林: "《化学建材配方手册》", 31 December 1999, 化学工业出版社 * |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103305066A (en) * | 2013-06-26 | 2013-09-18 | 关锦池 | Fireproof coating |
| CN104031509A (en) * | 2014-06-26 | 2014-09-10 | 无锡市崇安区科技创业服务中心 | Exterior wall coating for old wall reconstruction and preparation method thereof |
| CN104974572A (en) * | 2015-06-23 | 2015-10-14 | 苏州博利迈新材料科技有限公司 | Nano particle compound type anticorrosive coating and preparation method therefor |
| CN105131732A (en) * | 2015-08-13 | 2015-12-09 | 蚌埠市时代电子有限公司 | Long-acting led heat-dissipating coating material and preparation method thereof |
| CN107140928A (en) * | 2017-06-20 | 2017-09-08 | 和县明生环保材料有限责任公司 | A kind of waterproof and heat-insulating exterior coating and its production technology |
| CN107163798A (en) * | 2017-06-30 | 2017-09-15 | 朱燕萍 | A kind of fireproof coating |
| CN107236393A (en) * | 2017-07-26 | 2017-10-10 | 合肥铭佑高温技术有限公司 | A kind of fire resistant coating and preparation method thereof |
| CN112694815A (en) * | 2020-12-03 | 2021-04-23 | 湖南格仑新材股份有限公司 | Graphene heat dissipation coating, preparation method and application thereof |
| CN116239907A (en) * | 2023-03-29 | 2023-06-09 | 汪辉 | High-temperature-resistant fireproof coating and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102993835B (en) | 2015-01-07 |
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Effective date of registration: 20190606 Address after: 221000 Xuzhou Industrial Park, Xuzhou City, Jiangsu Province Patentee after: JIANGSU AIDEKA BUILDING MATERIALS TECHNOLOGY Co.,Ltd. Address before: 215200 Nanliu Village, Songling Town, Wujiang City, Suzhou City, Jiangsu Province Patentee before: Suzhou Deler Building Material Technology Co.,Ltd. |
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Granted publication date: 20150107 Termination date: 20211030 |