CN102992254B - Sterile cold-filling method of dry type goji berry fruit wine - Google Patents
Sterile cold-filling method of dry type goji berry fruit wine Download PDFInfo
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- CN102992254B CN102992254B CN201210486995.8A CN201210486995A CN102992254B CN 102992254 B CN102992254 B CN 102992254B CN 201210486995 A CN201210486995 A CN 201210486995A CN 102992254 B CN102992254 B CN 102992254B
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- 238000011049 filling Methods 0.000 title claims abstract description 52
- 238000000034 method Methods 0.000 title claims abstract description 29
- 235000019990 fruit wine Nutrition 0.000 title claims abstract description 23
- 244000241838 Lycium barbarum Species 0.000 title abstract 5
- 235000015459 Lycium barbarum Nutrition 0.000 title abstract 5
- 239000007788 liquid Substances 0.000 claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 21
- RTKIYNMVFMVABJ-UHFFFAOYSA-L thimerosal Chemical compound [Na+].CC[Hg]SC1=CC=CC=C1C([O-])=O RTKIYNMVFMVABJ-UHFFFAOYSA-L 0.000 claims description 20
- 229940033663 thimerosal Drugs 0.000 claims description 20
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 claims description 19
- 238000004659 sterilization and disinfection Methods 0.000 claims description 19
- 235000017784 Mespilus germanica Nutrition 0.000 claims description 16
- 235000000560 Mimusops elengi Nutrition 0.000 claims description 16
- 235000007837 Vangueria infausta Nutrition 0.000 claims description 16
- 238000004140 cleaning Methods 0.000 claims description 15
- OSVXSBDYLRYLIG-UHFFFAOYSA-N dioxidochlorine(.) Chemical compound O=Cl=O OSVXSBDYLRYLIG-UHFFFAOYSA-N 0.000 claims description 12
- 239000007921 spray Substances 0.000 claims description 12
- 238000012371 Aseptic Filling Methods 0.000 claims description 10
- 239000011521 glass Substances 0.000 claims description 10
- 239000002253 acid Substances 0.000 claims description 8
- 239000007799 cork Substances 0.000 claims description 8
- 239000003513 alkali Substances 0.000 claims description 7
- 239000004155 Chlorine dioxide Substances 0.000 claims description 6
- 235000019398 chlorine dioxide Nutrition 0.000 claims description 6
- 238000003958 fumigation Methods 0.000 claims description 6
- 238000002372 labelling Methods 0.000 claims description 6
- 238000002791 soaking Methods 0.000 claims description 6
- 238000012859 sterile filling Methods 0.000 claims description 6
- 241000894006 Bacteria Species 0.000 claims description 5
- 240000002624 Mespilus germanica Species 0.000 claims 2
- 235000014101 wine Nutrition 0.000 abstract description 12
- 239000002932 luster Substances 0.000 abstract description 4
- 235000016709 nutrition Nutrition 0.000 abstract description 4
- 238000001914 filtration Methods 0.000 abstract description 3
- 239000000796 flavoring agent Substances 0.000 abstract description 3
- 235000019634 flavors Nutrition 0.000 abstract description 3
- 230000001954 sterilising effect Effects 0.000 abstract description 3
- 238000007789 sealing Methods 0.000 abstract description 2
- 230000035939 shock Effects 0.000 abstract description 2
- 230000000249 desinfective effect Effects 0.000 abstract 1
- 239000004615 ingredient Substances 0.000 abstract 1
- 235000019640 taste Nutrition 0.000 abstract 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Inorganic materials [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 18
- 244000182216 Mimusops elengi Species 0.000 description 14
- 239000000243 solution Substances 0.000 description 9
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 230000002599 biostatic effect Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 230000009931 harmful effect Effects 0.000 description 2
- 229910017604 nitric acid Inorganic materials 0.000 description 2
- 230000035764 nutrition Effects 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 235000009754 Vitis X bourquina Nutrition 0.000 description 1
- 235000012333 Vitis X labruscana Nutrition 0.000 description 1
- 240000006365 Vitis vinifera Species 0.000 description 1
- 235000014787 Vitis vinifera Nutrition 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 230000001066 destructive effect Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000005429 filling process Methods 0.000 description 1
- -1 fruital Substances 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000012858 packaging process Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
Abstract
The invention relates to a sterile cold-filling method of dry type goji berry fruit wine. The method is characterized by comprising the following steps: disinfecting and sterilizing all the devices and apparatuses contacted by dry type goji berry fruit wine in the process of filling firstly, then degerming and filtering the dry type goji berry fruit wine and finally completing processes of filling, corking and sealing of the wine liquid in a sterile and clean space, and thus completing sterile cold-filling. The invention provides a sterile cold-filling method of dry type goji berry fruit wine; the quality of the product is ensured by the sterile cold-filling; the wine is filled under a normal-temperature aseptic condition in cold-filling, so that the intrinsic colour and luster, fruity flavor, taste and nutritional ingredient are maintained at a maximum extent; the requirement on the bottle in the cold filling is low, so that the bottle body is prevented from bearing hot and cold shock; and consumption a great amount of steam is not needed in the cold filling, and only the normal-temperature filling is needed.
Description
Technical field
The present invention relates to a kind of cold-aseptic filling method of dry-type medlar fruit wine.
Background technology
Generally dry type grape wine is because himself containing certain wine degree essence and the sugar content lower than 4g/L, adopts cold filling can reach the object of Biostatic within the shelf-life under relatively strict sanitary condition.Other dry type and sweet type fruit wine all to adopt hot filling or filling after carry out pasteurize the technique germ killed on wine liquid and container reach the object of Biostatic.On the one hand, the technique of hot filling or pasteurize all wants the energy of at substantial, causes productive costs to remain high, and complex procedures, and expend time in length; On the other hand, high temperature has very large destructive effect to the heat-sensitive nutrition in wine liquid, and causes harmful effect to the fragrance of wine body, color and luster mouthfeel.
Because dry-type medlar fruit wine contains certain alcohol concentration and sugar content is low, possesses certain bacteriostasis, its aseptic condition and operation are different from fruit drink, and therefore dry-type medlar fruit wine needs a kind of with low cost, is different from the cold-aseptic filling method of beverage efficiently.
Summary of the invention
The object of this invention is to provide a kind of cold-aseptic filling method of dry-type medlar fruit wine, the filling process of dry-type medlar fruit wine can be simplified, reduction productive costs of increasing work efficiency.
A kind of cold-aseptic filling method of dry-type medlar fruit wine, its special feature is, comprise the steps: that the equipment that first dry-type medlar fruit wine in filling operation touched and utensil are all through sterilization process, then by dry-type medlar fruit wine aseptic filtration, last complete in aseptic space wine liquid filling, beat and fill in sealing process, namely complete cold-aseptic filling.
Whole filling operation completes between the sterile filling of hundred grades of purifications, and filling front 30min-1h opens clean air system and at 18-22 DEG C of temperature-constant operation, keeps uviol lamp often to open; Time filling, uviol lamp is closed, operating personal is worn clean garment and is drenched at Airshower chamber wind and at least enter bottling department after 15s, ozone disinfection cabinet is used to carry out disinfection to cork, immersing type disinfection machine is used to carry out disinfection to empty glass bottle, rinse with sterilized water again, then dry up with filtrated air, adopt CIP washing system to clean up in the equipment of wine liquid process, pipeline; Finally that wine liquid is filling after the sterilization film of 0.2-0.25 μm carries out aseptic filtration.
Wherein the thimerosal of immersing type disinfection machine adds pure water dilution with ClO 2 solution to be mixed with the solution that chlorine dioxide concentration is 200-300PPM.
Wherein sterilized water is according to 2-5g/m
3ozone addition be mixed with the ozone solution of concentration 0.5-1mg/L.
Wherein Airshower chamber wind drench refer to filter efficiency be 95%-99.99%, ejection wind speed be 15-20m/s condition leeward drench 15-30s.
Wherein refer to the cleaning of CIP washing system and pipeline, pump, bottle placer are connected into circulation closed pipeline, successively with the alkali lye of mass concentration 2%, the acid solution of 3% and each circulation cleaning 30min of hot water of 90-95 DEG C.
Wherein the process of empty glass bottle is referred to that sky glass bottle makes thimerosal fill whole bottle when entering thimerosal, the air driven in bottle outlet makes the surfaces externally and internally of bottle be immersed in completely in thimerosal, and stop 10-15s, then put into sterilized water soaking compartment after having been toppled over by the thimerosal in bottle and soak 10-15s, then with sterilized water, inside and outside spray is carried out to empty glass bottle and be in reason, then with bottle in blow pouring, until empty glass bottle is dry with the filtrated air of equipressure.
Wherein cork is carried out disinfection and refer to the ozone disinfection cabinet fumigation 15-25min of cork at 1-2% ozone concentration.
Wherein also the bottle after filling to be played plug, spray air-dry, paste labels, contracting cap, coding and vanning.
Hot filling is the packaging process that fruit wine is conventional, but the filling cost of hot filling is high, and equipment investment is large, and cost of product is high, and wine body is because being heated for a long time in the process of hot filling, and nutrition is impaired, and color and luster, flavour, fragrance also can by harmful effects to a certain extent.The invention provides a kind of cold-aseptic filling method of dry-type medlar fruit wine, cold-aseptic filling ensure that product design, and in cold filling, wine body is filling under normal temperature germ-free condition, farthest maintains original color and luster, fruital, flavour and nutritional labeling.The requirement of cold filling to bottle is lower, avoids bottle to bear thermal shock; Cold filling does not need to consume a large amount of steam yet, only needs normal temperature filling.Cold-aseptic filling has very strong science, and technique is very tight to environmental requirement, and the technology management step wherein mainly comprised filling apparatus, peopleware and technique are taked requires very high.
Detailed description of the invention
The experiment material that the embodiment of the present invention adopts and equipment as follows:
Embodiment 1:
Adopt between hundred grades of sterile fillings purified.Uviol lamp is opened, and opens clean air system and 18 DEG C of temperature-constant operation 1h.Filtrated air enters filling room and adopts intensive streamline air diffuser, top supplying air mode, and sterile wind keeps blast even by spoiler back balance ground.
Uviol lamp is closed, operating personal wear clean garment filter efficiency be 95%, ejection wind speed is enter aseptic area after the condition leeward of 20m/s drenches 30S.Empty bottle enters concentration and is 300PPM chlorine dioxide disinfection liquid and makes thimerosal fill in whole bottle, drive the air in bottle outlet, the surfaces externally and internally of bottle also must be immersed in thimerosal completely, and stop 10S, ensure that bacterium is killed completely, soak 15S in the sterilized water soaking compartment of then thimerosal in bottle having been toppled over rear introduction ozone concentration 0.5mg/L, again with sterilized water, the inside and outside spray of bottle is carried out to glass bottle and be in reason output (namely from then on link enters next link) is front.Then with bottle in blow pouring, until dry with the filtrated air of equipressure.Cork is the ozone disinfection cabinet fumigation 15min of 2% at ozone concentration.Dry-type medlar fruit wine is that the degerming plate of 0.2 μm filters through aperture.Bottle economy-combat plug after filling, spray air-dry, labeling mark, contracting cap, coding, vanning, fillingly to complete.Before first time is filling or other filling shutdown gap, adopts CIP method of cleaning, successively with each circulation cleaning 30min of hot water of the alkali lye of 2%, the acid solution of 3% and 95 DEG C.
Embodiment 2:
Adopt between hundred grades of sterile fillings purified.Uviol lamp is opened, and opens clean air system and 22 DEG C of temperature-constant operation 1h.Filtrated air enters filling room and adopts intensive streamline air diffuser, top supplying air mode, and sterile wind keeps blast even by spoiler back balance ground.
Uviol lamp is closed, operating personal wear clean garment filter efficiency be 95%, ejection wind speed is enter aseptic area after the condition leeward of 20m/s drenches 30S.Empty bottle enters concentration and is 200PPM chlorine dioxide disinfection liquid and makes thimerosal fill in whole bottle, drive the air in bottle outlet, the surfaces externally and internally of bottle also must be immersed in thimerosal completely, and stop 15S, ensure that bacterium is killed completely, soak 10S in the sterilized water soaking compartment of then thimerosal in bottle having been toppled over rear introduction ozone concentration 1mg/L, before output, again with sterilized water, the inside and outside spray of bottle is carried out to glass bottle be in reason.Then with bottle in blow pouring, until dry with the filtrated air of equipressure.Cork is the ozone disinfection cabinet fumigation 25min of 1% at ozone concentration.Dry-type medlar fruit wine is that the degerming plate of 0.2 μm filters through aperture.Bottle economy-combat plug after filling, spray air-dry, labeling mark, contracting cap, coding, vanning, fillingly to complete.Before first time is filling or other filling shutdown gap, adopts CIP method of cleaning, successively with each circulation cleaning 30min of hot water of the alkali lye of 2%, the acid solution of 3% and 95 DEG C.
Embodiment 3:
Adopt between hundred grades of sterile fillings purified.Uviol lamp is opened, and opens clean air system and 18 DEG C of temperature-constant operation 30min.Filtrated air enters filling room and adopts intensive streamline air diffuser, top supplying air mode, and sterile wind keeps blast even by spoiler back balance ground.
Uviol lamp is closed, operating personal wear clean garment filter efficiency be 99.99%, ejection wind speed is enter aseptic area after the condition leeward of 15m/s drenches 30S.Empty bottle enters concentration and is 300PPM chlorine dioxide disinfection liquid and makes thimerosal fill in whole bottle, drive the air in bottle outlet, the surfaces externally and internally of bottle also must be immersed in thimerosal completely, and stop 10S, ensure that bacterium is killed completely, soak 15S in the sterilized water soaking compartment of then thimerosal in bottle having been toppled over rear introduction ozone concentration 0.5mg/L, before output, again with sterilized water, the inside and outside spray of bottle is carried out to glass bottle be in reason.Then with bottle in blow pouring, until dry with the filtrated air of equipressure.Cork is the ozone disinfection cabinet fumigation 25min of 1% at ozone concentration.Dry-type medlar fruit wine is that the degerming plate of 0.25 μm filters through aperture.Bottle economy-combat plug after filling, spray air-dry, labeling mark, contracting cap, coding, vanning, fillingly to complete.Before first time is filling or other filling shutdown gap, adopts CIP method of cleaning, successively with each circulation cleaning 30min of hot water of the alkali lye of 2%, the acid solution of 3% and 95 DEG C.
Embodiment 4:
Adopt between hundred grades of sterile fillings purified.Uviol lamp is opened, and opens clean air system and 20 DEG C of temperature-constant operation 30min.Filtrated air enters filling room and adopts intensive streamline air diffuser, top supplying air mode, and sterile wind keeps blast even by spoiler back balance ground.
Uviol lamp is closed, operating personal wear clean garment filter efficiency be 95%, ejection wind speed is enter aseptic area after the condition leeward of 20m/s drenches 15S.Empty bottle enters concentration and is 300PPM chlorine dioxide disinfection liquid and makes thimerosal fill in whole bottle, drive the air in bottle outlet, the surfaces externally and internally of bottle also must be immersed in thimerosal completely, and stop 10S, ensure that bacterium is killed completely, soak 10S in the sterilized water soaking compartment of then thimerosal in bottle having been toppled over rear introduction ozone concentration 1mg/L, before output, again with sterilized water, the inside and outside spray of bottle is carried out to glass bottle be in reason.Then with bottle in blow pouring, until dry with the filtrated air of equipressure.Cork is the ozone disinfection cabinet fumigation 15min of 2% at ozone concentration.Dry-type medlar fruit wine is that the degerming plate of 0.25 μm filters through aperture.Bottle economy-combat plug after filling, spray air-dry, labeling mark, contracting cap, coding, vanning, fillingly to complete.Before first time is filling or other filling shutdown gap, adopts CIP method of cleaning, successively with each circulation cleaning 30min of hot water of the alkali lye of 2%, the acid solution of 3% and 95 DEG C.
According to existing routine techniques, CIP cleaning adopts strong acid, highly basic, such as NaOH, phosphoric acid, nitric acid usually, and in embodiments of the invention, alkali lye and acid solution adopt NaOH and nitric acid respectively, but the cleaning liquid adopting other to meet the requirement of CIP cleaning is feasible equally.
Claims (1)
1. the cold-aseptic filling method of a dry-type medlar fruit wine, it is characterized in that, comprise the steps: between the sterile filling that employing hundred grades purifies, uviol lamp is opened, open clean air system and 18 DEG C of temperature-constant operation 1h, filtrated air enters filling room and adopts intensive streamline air diffuser top supplying air mode, and sterile wind keeps blast even by spoiler back balance ground, uviol lamp is closed, it is 95% that operating personal wears clean garment at filter efficiency, ejection wind speed is enter aseptic area after the condition leeward of 20m/s drenches 30 S, empty bottle enters concentration and is 300PPM chlorine dioxide disinfection liquid and makes thimerosal fill in whole bottle, drive the air in bottle outlet, the surfaces externally and internally of bottle also must be immersed in thimerosal completely, and stop 10S, ensure that bacterium is killed completely, 15S is soaked in the sterilized water soaking compartment of then thimerosal in bottle having been toppled over rear introduction ozone concentration 0.5mg/L, again carry out in bottle with sterilized water to glass bottle before output, outer spray is in reason, then with bottle in blow pouring with the filtrated air of equipressure, until dry, cork is the ozone disinfection cabinet fumigation 15min of 2% at ozone concentration, dry-type medlar fruit wine is that the degerming plate of 0.2 μm filters through aperture, bottle economy-combat plug after filling, spray air-dry, labeling mark, contracting cap, coding, vanning, fillingly to complete, before first time is filling or other filling shutdown gap, adopts CIP method of cleaning, successively with each circulation cleaning 30min of hot water of the alkali lye of 2%, the acid solution of 3% and 95 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210486995.8A CN102992254B (en) | 2012-11-27 | 2012-11-27 | Sterile cold-filling method of dry type goji berry fruit wine |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201210486995.8A CN102992254B (en) | 2012-11-27 | 2012-11-27 | Sterile cold-filling method of dry type goji berry fruit wine |
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| Publication Number | Publication Date |
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| CN102992254A CN102992254A (en) | 2013-03-27 |
| CN102992254B true CN102992254B (en) | 2015-05-27 |
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| CN201210486995.8A Active CN102992254B (en) | 2012-11-27 | 2012-11-27 | Sterile cold-filling method of dry type goji berry fruit wine |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107161936A (en) * | 2017-06-06 | 2017-09-15 | 石家庄鹏海制药股份有限公司 | The production technology of the big transfusion of vial |
| CN108946631B (en) * | 2018-05-30 | 2020-06-12 | 浙江瑞宝包装机械有限公司 | Agricultural product packaging equipment |
| CN115068647A (en) * | 2022-06-20 | 2022-09-20 | 合肥中辰轻工机械有限公司 | Online beverage bottle sterilizing system |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1837023A (en) * | 2006-04-10 | 2006-09-27 | 江苏新美星包装机械有限公司 | Empty bottle sterilization process used in sterilized cold filling production line of polyester bottled beverage |
| JP4862993B2 (en) * | 2006-04-14 | 2012-01-25 | 東洋製罐株式会社 | Filling and sealing thin bottles |
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Denomination of invention: Sterile cold-filling method of dry type goji berry fruit wine Effective date of registration: 20180126 Granted publication date: 20150527 Pledgee: Cao Guangjiang Pledgor: Ningxiahong Zhongning Wolfberry Products Co., Ltd. Registration number: 2018990000078 |
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Effective date of registration: 20191231 Address after: 755000 Ningxia iron and Steel Group Co., Ltd. Meili Industrial Park, Shapotou District, Zhongwei City, Ningxia Hui Autonomous Region Patentee after: Cao Guangjiang Address before: The new 751200 the Ningxia Hui Autonomous Region city centre in the county of Fort Street Patentee before: Ningxiahong Zhongning Wolfberry Products Co., Ltd. |
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Effective date of registration: 20210726 Address after: 755000 Xinbao Town, Zhongning County, Zhongwei City, Ningxia Hui Autonomous Region Patentee after: NINGXIAHONG CHINESE WOLFBEERY INDUSTRY Co.,Ltd. Address before: 755000 Ningxia iron and Steel Group Co., Ltd., Meili Industrial Park, Shapotou District, Zhongwei City, Ningxia Hui Autonomous Region Patentee before: Cao Guangjiang |