CN102988243A - Face cleaning crystal hard gel and preparation method thereof - Google Patents
Face cleaning crystal hard gel and preparation method thereof Download PDFInfo
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- CN102988243A CN102988243A CN2012105644190A CN201210564419A CN102988243A CN 102988243 A CN102988243 A CN 102988243A CN 2012105644190 A CN2012105644190 A CN 2012105644190A CN 201210564419 A CN201210564419 A CN 201210564419A CN 102988243 A CN102988243 A CN 102988243A
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- cocos nucifera
- lauroyl
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- glycine
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Abstract
The invention relates to a face cleaning crystal hard gel. The face cleaning crystal hard gel is characterized by comprising a glutamic acid type surface active agent, a glutamate type surface active agent, a glycinate type surface active agent, a sarcosinate type surface active agent, a polypeptide surface active agent, ethanol amine type alkali, polylol, betaine, urea, plant essential oil and purified water. The preparation method of the face cleaning crystal hard gel comprises the following steps: adding the components according to a certain sequence and mixing the components uniformly at a certain temperature and under the condition of stirring; pouring the mixture into a die for molding; and demolding and dehydrating to obtain a finished product. Compared with the prior art, the face cleaning crystal hard gel overcomes the defects of the prior art, and a novel green face cleaning product namely the amino acid face cleaning crystal hard gel is provided; and the face cleaning crystal hard gel has the characteristics of high stability, strong detersive capability, soft foams, pleasant skin feeling, glittering and translucent shape, low cost, no allergy and stimulation to the skin, nourishing and moisturizing effects and the like.
Description
Technical field
The present invention relates to daily skin protection face-cleaning articles, refer in particular to a kind of clean quartzy hard gel and preparation method thereof.
Background technology
Raising along with people's living standard, especially the women like to be beautiful consciousness enhancing, requirement for the make-up and beauty articles for use is more and more higher, the classical theory of the skin protection trilogy that Clinique is advocated (cleaning, cleaning cortex and moist) is rooted in the hearts of the people, and " clean facial soap, astringent, specially good effect milky lotion " face nursing combined complete is subject to beyond example favor.The clean skin of face, owing to refuse and residual, the airborne dirty dirt of cosmetics such as some sebums that can remove the discharge of skin metabolism process, dead angle cell plastids, reduce potential killer (intensive ultraviolet, vehicle exhaust, dry air and computer electrical equipment radiation) to the injury of skin, therefore have irreplaceable important function for beauty treatment, only the effect of the follow-up skin protection work of guarantee under the prerequisite that clean skin basic steps is handled properly.But the solid-state clean skin product of washing one's face on the existing market is all deposited many deficiencies on prescription and preparation technology, be summarized as follows:
1. the traditional fancy soap take soap base (sodium soap) and other a small amount of surfactants as major ingredient has than strong basicity (pH value approximately about 10); life-time service can destroy the intrinsic acid-base balance of skin surface; and the film phosphide class of protectiveness Natural ester and Skin Cell and memebrane protein class are produced abrasive part remove effect; thereby the facial twinge that presents the long period, the sense of discomfort such as tight and dry and astringent, can only rely on skin self-regulation functional rehabilitation to original weak acid environment just slightly has mitigation.This very strange dermopathic growing that be highly advantageous to;
2. be difficult to thoroughly remove on the residual skin of the soap scum that in cleaning process, forms of fancy soap (main component is fatty acid calcium, fatty acid magnesium, the oils and fats on water stain, other compositions of soap base and the human body, scurf etc.), easily stop up pore, affect the normal metabolism of skin;
3. the main component of releasing afterwards is synthetic surfactant " synthetic soap ", although it is excessively strong to have overcome traditional fancy soap alkalescence, easily produce the drawback of soap scum, but defat is excessively strong, is difficult for flushing, and skin has soapy feeling and is detained the synthetic chemistry composition, increase the sensitization source, and the formed product difficulty, easy moisture absorption and deformation, difficult for a long time storage is still weak point;
4. " neutral soap ", transparent soap and the handmade soap that are the theme with environmental protection that appeared on the market in recent years again take soap base (sodium soap) as main component, add simultaneously a large amount of lime soap dispersant, compose fat agent, wetting agent and other function additives even powdered carbon.The aqueous solution pH of this type of soap is about 7-8, is difficult for during cleaning forming soap scum, washes rear tight sense and obviously improves, but its pH still exceeds than the faintly acid of skin, and has the component compatibility problem, and clean skin lacks in ability, wash the residual complicated of rear skin, sensitization hidden danger is on the high side.This type of soap is strict to production equipment and industrial requirements, and on the high side.
5. the clean facial soap of gel-type of new generation take the transparent moisturizing crystal soap of DHC aminoacid as representative adopts heavy dose of low amino acid surfactant that stimulates, and skin side-effects is greatly reduced.But the comprehensively regulating effect is weak, and the clean power of oily skin is had much room for improvement, and trace solvent residual in the course of processing still can consist of the sensitization threat to the idiosyncratic, and the production cycle is oversize, needs more than 40 day, expensive raw material price, and product is difficult to popular.
Summary of the invention
Technical problem to be solved by this invention is that the present situation for prior art provides a kind of with short production cycle, good stability, strong detergency, foam performance is desirable, skinfeel is pleasant, outward appearance is beautiful and cost is low Novel cleaning face product---the quartzy hard gel of amino acid cleansing.
Another technical problem to be solved by this invention provides a kind of with short production cycle, good stability, strong detergency, foam performance is desirable, skinfeel is pleasant, outward appearance is beautiful and cost is low Novel cleaning face product---the preparation method of the quartzy hard gel of amino acid cleansing.
The present invention solves the problems of the technologies described above the technical scheme that adopts: this clean quartzy hard gel is characterized in that comprising the following weight component:
Preferably, described glutamic acid-type surfactant is selected from cocos nucifera oil acyl glutamic acid or lauroyl glutamic acid.Consider manufacturing efficient, preferably, the purity of described glutamic acid-type surfactant is more than or equal to 98%, and the water content in the glutamic acid-type surfactant is less than or equal to 0.55%,, enhances productivity in the time with the baking of shortening follow-up finished product.
Described glutamate surfactant is selected from cocos nucifera oil acyl glutamic acid triethanolamine, cocos nucifera oil acyl sodium glutamate, cocos nucifera oil acyl disodium glutamate, cocos nucifera oil acyl Kaglutam, cocos nucifera oil acyl glutamic acid dipotassium, lauroyl glutamic acid triethanolamine, sodium lauroyl glutamate, lauroyl disodium glutamate, lauroyl Kaglutam and the lauroyl glutamic acid dipotassium one or more.
Described glycine salt surfactant is selected from one or more in cocos nucifera oil acyl glycine triethanolamine, cocos nucifera oil acyl Glycine sodium, cocos nucifera oil acyl glycine potassium, lauroyl glycine triethanolamine, lauroyl Glycine sodium and the lauroyl glycine potassium, first-selected cocos nucifera oil acyl Glycine sodium.Further, the consumption of described glycine salt surfactant is 2.0～4.0%.
Described sarcosine salt surfactant is selected from one or more in cocos nucifera oil acylsarcosine triethanolamine, cocos nucifera oil acylsarcosine sodium, cocos nucifera oil acylsarcosine potassium, Hamposyl L triethanolamine, sodium lauroyl sarcosine and the potassium lauroyl sarcosine; The consumption of described glycine salt surfactant is 2.0～4.0%.
Described polypeptide class surfactant is selected from one or more in cocos nucifera oil acyl silk peptide sodium and lauroyl silk peptide sodium, myristoyl silk peptide sodium and the stearoyl silk peptide sodium.
Described ethanolamines alkali is selected from monoethanolamine, diethanolamine, triethanolamine or triisopropanolamine.Ethanolamines alkali can carry out gelation reaction with the cocos nucifera oil acyl glutamic acid that belongs to the glutamic acid-type surfactant, and clean product presented than hard ground.
Described polyhydric alcohol is selected from one or more in glycerol, propylene glycol, butanediol and the sorbitol.
Described betanin is the trimethyl glycine of natural betanin or cosmetics-stage; Described carbamide is the carbamide of cosmetics-stage; Described plants essential oil is selected from natural rose essential, jasmin quintessence oil, Herba Lysimachiae foenum-graeci quintessence oil, Flos Matricariae chamomillae quintessence oil, orange blossom quintessence oil, Cananga odorata quintessence oil, Flos micheliae Albae quintessence oil, Fructus Citri Limoniae quintessence oil or Bergamot; Described water is pure water, distilled water or deionized water.
The preparation method of above-mentioned clean quartzy hard gel is characterized in that comprising the steps:
L) with described polyhydric alcohol and water mixed dissolution, under 80～100rpm, stir and be heated to 80 ℃, then add successively described carbamide, described betanin, described polypeptide class surfactant, described glycine salt surfactant, sarcosine salt surfactant and glutamate surfactant by the prescription consumption, control 80rpm stirs and was clear state to system in 30 minutes;
2) above-mentioned feed liquid is heated to 90 ℃, under the stirring of 80～100rpm, adds described glutamic acid-type surfactant, then control 80rpm and stir and be clear state to system in 30 minutes, add the plants essential oil mix homogeneously;
3) in 15～25 minutes described ethanolamines alkali liquor is splashed in the above-mentioned feed liquid under 80～100rpm, regulation system pH is 6.5, continues to stir 30 minutes;
4) above-mentioned sizing material is poured in the mould, the demoulding after cooling curing is shaped is volatilized or the hot blast drying moisture content hard gel that gets product naturally.
Compared with prior art, the present invention utilizes ultralow stimulation to have clean major ingredient cocos nucifera oil acyl glutamic acid of antibacterial effect concurrently, cooperate with triethanolamine dexterously, consist of the regid gel system, and by the comprehensively regulating function of many effects of polypeptide class surfactant, avoid adding compatibility and the process complexity problem that numerous components cause, simultaneously, the present invention replaces easily consisting of the low boiling point organic solvent of safety and environmental protection hidden danger with water, can finish fast the product shaping operation of doing something in disregard of obstacles, not only improved production efficiency, and the hard gel finished product that makes effect no matter, safety or the feature of environmental protection all rank first among similar products.
Simultaneously, the present invention also has following characteristics:
1. will have originally the silk peptide class surfactant of gentle Jing Xi ﹑ hair Pao ﹑ Hu cut ﹑ Fu Zhi ﹑ Bao Shi ﹑ detoxifcation and skin care effect as the comprehensive blender of the clean skin product of face, and make final products be fit to comprise clean use of most consumers of oiliness, neutrality, dryness and Combination skin quality;
2. ingeniously construct in high resilience and the cold water easily molten cocos nucifera oil acyl glutamic acid triethanolamine gel rubber system, build the subacidity clean skin environment close with the skin pH value, avoid many drawbacks that the clean skin product of conventional gel bring because adding the high molecular polymer thickening agent, can not stop up pore, not satiny, the finished product flushing is easily bathed and is felt pleasant, skin side-effects is down to minimum;
3. the multiplex environmental type aminoacid of potion and the best compatibility of polypeptide class surfactant, make finished product under the prerequisite of omitting the natural and synthetic effect component of multi-flavor, disposablely finish clean skin, compose fat and moisturizing operation, and the importing of stopping numerous sensitizing agents from the source;
4. filter out originally amino acid surfactant, it not only has conventional effect, and and the present invention prescription in other material be used in conjunction with, creationaryly embodied extraordinary antiseptic effect, that is to say, although do not use in the prescription provided by the present invention in the prior art the antiseptic that must add, its antiseptic effect but is 2～3 times of prior art; What in the prior art there be the consumption of conventional preservatives reaches 0.8% unexpectedly, and its pot-life only had about 1 year, and the application's pot-life can reach 2～3 years.And antiseptic is the arch-criminal who causes skin allergy.The hidden danger that clean the quartzy hard gel that the application provides effectively avoided the chemosynthesis antiseptic that health is consisted of.
5. preparation method of the present invention has proposed the rapidly solidified moulding process of a kind of organic solvent-free steam seasoning, make the product dry-hard time foreshorten to a week from traditional 40 days, thoroughly eliminate the low boiling point solvents such as micro-isopropyl alcohol residual in the course of processing to the sensitization threat of skin.And the step of preparation process of this preparation method is few, preparation method is simple, and reaction is control easily, and the preparation process environmental protection is fit to suitability for industrialized production.
To sum up, the present invention has overcome the deficiencies in the prior art, provide a kind of novel green clean product---the quartzy hard gel of amino acid cleansing, it has good stability, strong detergency, foam is soft, skinfeel is pleasant, the brilliant firefly of outward appearance is bright, cost is low, to skin without irritated, without irritating and the characteristics such as the moisture-keeping function of nourishing being arranged.
The specific embodiment
Below in conjunction with embodiment the present invention is described in further detail.
Embodiment 1
Charge ratio:
In 100 liter reaction pots, inject 13 kilograms of deionized waters, start blender, the control mixing speed is 80rpm, and the logical Steam Heating of chuck adds 3 kilograms of glycerol simultaneously, in 30 minutes minutes material temperature is risen to 75 ℃, add 0.5 kilogram of 0.5 kilogram in carbamide and betanin, stirring is transparent.Add 5 kilograms of 20% cocos nucifera oil acyl silk peptide sodium liquid in 10 minutes minutes, mix thoroughly, add successively 4 kilograms of 5 kilograms of 98.5% cocos nucifera oil acyl sodium glutamate solids, 98% 2 kilograms of cocos nucifera oil acyl Glycine sodium solids and 98% sodium lauroyl sarcosine solids in 30 minutes minutes, stir and make the system attitude that is translucent half an hour.
Above-mentioned feed liquid is heated to 80 ℃, and fast 100rpm is mixed in control, and two batches at interval 20 minutes minutes adds 16 kilograms of 99.5% cocos nucifera oil acyl glutamic acid solids, stirs to make the system attitude that is translucent half an hour, adds 0.3 kilogram of Fructus Citri Limoniae quintessence oil, mixes thoroughly;
Fast 100rpm is mixed in control, in 20 minutes 12.8 kilograms of triethanolamine liquid is splashed in high-order Drop-adding device the above-mentioned feed liquid, strictly controls material temperature and is no more than 80 ℃, and regulation system pH is 6.5.Continue to stir and to be easy circulating water dissolubility sizing material to mixed system in 20 minutes;
Enter the injection molding operation, while hot above-mentioned sizing material is pumped into some small-sized liquid receivers after, in ten minutes, pour in the mould, put Indoor Natural cooling or low temperature environment solidified forming.The demoulding, naturally volatilization moisture content, in case of necessity the hot blast drying hard gel that gets product.
The brilliant firefly of the quartzy hard gel of the amino acid cleansing that makes is bright, abnormal smells from the patient fragrance, and quality is hard, stable performance, decontamination and skin-moisturizing, skin effect are all good, are the up-to-date upgraded product of clean facial soap in the skin protection trilogy.
Compare with the transparent type Japan DHC moisturizing crystal soap of present highest level, the quartzy hard gel of amino acid cleansing of the present invention is washed the rear face lubricious pool of silk, and more without tight sense, the barrier action of lock water is more obvious, responsive skin quality is not consisted of desquamation cause the pruritus danger, it serves to show creativeness of the present invention.
Embodiment 2 to embodiment 6
The weight proportion of each component and each component is as shown in table 2 among the embodiment 2 to embodiment 6
Table 1 embodiment 2 to embodiment 6 prescriptions
Do not contain glycine salt surfactant and sarcosine salt surfactant in the prescription of embodiment 2, so removed this two kinds of components in its preparation method, remainder is identical with embodiment 1.
The preparation method of embodiment 3 to embodiment 6 is identical with the direction of embodiment 1.
Clean the quartzy hard gel result of use for preparing is identical with embodiment 1, all has a brilliant firefly bright, abnormal smells from the patient fragrance, and quality is hard, stable performance, decontamination and skin-moisturizing, skin effect be good characteristics all.
Claims (10)
1. clean quartzy hard gel is characterized in that comprising the following weight component:
2. clean quartzy hard gel according to claim 1 is characterized in that described glutamic acid-type surfactant is selected from cocos nucifera oil acyl glutamic acid or lauroyl glutamic acid.
3. clean quartzy hard gel according to claim 1 is characterized in that described glutamate surfactant is selected from cocos nucifera oil acyl glutamic acid triethanolamine, cocos nucifera oil acyl sodium glutamate, cocos nucifera oil acyl disodium glutamate, cocos nucifera oil acyl Kaglutam, cocos nucifera oil acyl glutamic acid dipotassium, lauroyl glutamic acid triethanolamine, sodium lauroyl glutamate, lauroyl disodium glutamate, lauroyl Kaglutam and the lauroyl glutamic acid dipotassium one or more.
4. clean quartzy hard gel according to claim 1, it is characterized in that described glycine salt surfactant is selected from one or more in cocos nucifera oil acyl glycine triethanolamine, cocos nucifera oil acyl Glycine sodium, cocos nucifera oil acyl glycine potassium, lauroyl glycine triethanolamine, lauroyl Glycine sodium and the lauroyl glycine potassium, first-selected cocos nucifera oil acyl Glycine sodium.Further, the consumption of described glycine salt surfactant is 2.0～4.0%.
5. clean quartzy hard gel according to claim 1 is characterized in that described sarcosine salt surfactant is selected from one or more in cocos nucifera oil acylsarcosine triethanolamine, cocos nucifera oil acylsarcosine sodium, cocos nucifera oil acylsarcosine potassium, Hamposyl L triethanolamine, sodium lauroyl sarcosine and the potassium lauroyl sarcosine; The consumption of described glycine salt surfactant is 2.0～4.0%.
6. clean quartzy hard gel according to claim 1 is characterized in that described polypeptide class surfactant is selected from one or more in cocos nucifera oil acyl silk peptide sodium and lauroyl silk peptide sodium, myristoyl silk peptide sodium and the stearoyl silk peptide sodium.
7. clean quartzy hard gel according to claim 1 is characterized in that described ethanolamines alkali is selected from monoethanolamine, diethanolamine, triethanolamine or triisopropanolamine.
8. clean quartzy hard gel according to claim 1 is characterized in that described polyhydric alcohol is selected from one or more in glycerol, propylene glycol, butanediol and the sorbitol.
9. clean quartzy hard gel according to claim 1 is characterized in that described betanin is the trimethyl glycine of natural betanin or cosmetics-stage; Described carbamide is the carbamide of cosmetics-stage; Described plants essential oil is selected from natural rose essential, jasmin quintessence oil, Herba Lysimachiae foenum-graeci quintessence oil, Flos Matricariae chamomillae quintessence oil, orange blossom quintessence oil, Cananga odorata quintessence oil, Flos micheliae Albae quintessence oil, Fructus Citri Limoniae quintessence oil or Bergamot; Described water is pure water, distilled water or deionized water.
10. the preparation method of clean quartzy hard gel as claimed in claim 1 is characterized in that comprising the steps:
L) with described polyhydric alcohol and water mixed dissolution, under 80～100rpm, stir and be heated to 80 ℃, then add successively described carbamide, described betanin, described polypeptide class surfactant, described glycine salt surfactant, sarcosine salt surfactant and glutamate surfactant by the prescription consumption, the system of being stirred to is clear state;
2) above-mentioned feed liquid is heated to 90 ℃, adds described glutamic acid-type surfactant under the stirring of 80～100rpm, the system of being stirred to is clear state, adds the plants essential oil mix homogeneously;
3) in 15～25 minutes described ethanolamines alkali liquor is splashed in the above-mentioned feed liquid under 80～100rpm, regulation system pH is 6.5, continues to stir 30 minutes;
4) above-mentioned sizing material is poured in the mould, the demoulding after cooling curing is shaped is volatilized or the hot blast drying moisture content hard gel that gets product naturally.
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104042507A (en) * | 2014-06-17 | 2014-09-17 | 宁波御坊堂生物科技有限公司 | High-light-transmission pure amino-acid self-thickening soft cleansing gel and preparation method thereof |
| CN104352364A (en) * | 2014-11-11 | 2015-02-18 | 上海万淇生物科技有限公司 | Portable facial cleanser-containing wet tissue |
| CN104800091A (en) * | 2015-04-22 | 2015-07-29 | 湖南艾丽科技实业有限公司 | Composition used for self thickening of transparent type pure amino acid surfactant system cleaning product, and thickening method |
| CN105147532A (en) * | 2015-08-19 | 2015-12-16 | 广州科玛生物科技有限公司 | Amino acid facial cleanser and preparation method thereof |
| CN107080708A (en) * | 2017-03-30 | 2017-08-22 | 广州善草纪化妆品有限公司 | A kind of gentle multiple-effect face cleaning composition |
| CN107213090A (en) * | 2017-06-16 | 2017-09-29 | 苏州永创达电子有限公司 | Epoxy resin with environmentally friendly moistening effect |
| CN108096048A (en) * | 2018-01-20 | 2018-06-01 | 广州康芙莱生物科技有限公司 | A kind of pure amino acid mildy wash with reproducibility and preparation method thereof and application method |
| CN108587802A (en) * | 2018-05-19 | 2018-09-28 | 山东朱氏药业集团有限公司 | A kind of transparent amino acid crystal soap and preparation method thereof |
| CN108929814A (en) * | 2018-05-19 | 2018-12-04 | 山东朱氏药业集团有限公司 | A kind of amino acid soap and preparation method thereof |
| WO2024078286A1 (en) * | 2022-10-13 | 2024-04-18 | 苏州欧丽特生物医药有限公司 | Gel composition, and preparation and use thereof |
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104042507A (en) * | 2014-06-17 | 2014-09-17 | 宁波御坊堂生物科技有限公司 | High-light-transmission pure amino-acid self-thickening soft cleansing gel and preparation method thereof |
| CN104352364A (en) * | 2014-11-11 | 2015-02-18 | 上海万淇生物科技有限公司 | Portable facial cleanser-containing wet tissue |
| CN104800091A (en) * | 2015-04-22 | 2015-07-29 | 湖南艾丽科技实业有限公司 | Composition used for self thickening of transparent type pure amino acid surfactant system cleaning product, and thickening method |
| CN104800091B (en) * | 2015-04-22 | 2017-12-29 | 湖南艾丽科技实业有限公司 | Composition and method for thickening for transparent type pure amino acid surfactant system cleaning products from thickening |
| CN105147532A (en) * | 2015-08-19 | 2015-12-16 | 广州科玛生物科技有限公司 | Amino acid facial cleanser and preparation method thereof |
| CN107080708A (en) * | 2017-03-30 | 2017-08-22 | 广州善草纪化妆品有限公司 | A kind of gentle multiple-effect face cleaning composition |
| CN107080708B (en) * | 2017-03-30 | 2020-04-03 | 广州善草纪化妆品有限公司 | Mild multi-effect face cleaning composition |
| CN107213090A (en) * | 2017-06-16 | 2017-09-29 | 苏州永创达电子有限公司 | Epoxy resin with environmentally friendly moistening effect |
| CN108096048A (en) * | 2018-01-20 | 2018-06-01 | 广州康芙莱生物科技有限公司 | A kind of pure amino acid mildy wash with reproducibility and preparation method thereof and application method |
| CN108587802A (en) * | 2018-05-19 | 2018-09-28 | 山东朱氏药业集团有限公司 | A kind of transparent amino acid crystal soap and preparation method thereof |
| CN108929814A (en) * | 2018-05-19 | 2018-12-04 | 山东朱氏药业集团有限公司 | A kind of amino acid soap and preparation method thereof |
| WO2024078286A1 (en) * | 2022-10-13 | 2024-04-18 | 苏州欧丽特生物医药有限公司 | Gel composition, and preparation and use thereof |
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Application publication date: 20130327 Assignee: YOFOTO (CHINA) HEALTH INDUSTRY Co.,Ltd. Assignor: NINGBO YUFANGTANG BIOTECHNOLOGY Co.,Ltd. Contract record no.: X2021330000082 Denomination of invention: Cleansing Gel crystal hard gel and preparation method thereof Granted publication date: 20141203 License type: Common License Record date: 20210819 |
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