CN1029768C - Flue-cured tobacco bud cream and its application method - Google Patents
Flue-cured tobacco bud cream and its application method Download PDFInfo
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- CN1029768C CN1029768C CN 93101941 CN93101941A CN1029768C CN 1029768 C CN1029768 C CN 1029768C CN 93101941 CN93101941 CN 93101941 CN 93101941 A CN93101941 A CN 93101941A CN 1029768 C CN1029768 C CN 1029768C
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- cream
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Abstract
The present invention relates to a fluecured tobacco bud cream and an application method thereof. The cream is extracted by fluecured tobacco buds to be red brown pasty substance, and the cream which has intense fluecured tobacco fragrance is dissolved in distilled water. The cream contains 64% of alcohol-soluble ingredients, 36% of alcohol insoluble ingredients, 1.2% to 1.5% of total vegetable alkaloid, 2.2% to 2.5% of total sugar and 4.2% to 4.5% of total nitrogen. The cream can be used for fragrance for cigarettes, tobacco sheets and expansion stem shreds, and the leaf group formulation cost can be reduced after fragrance. The fragrance and the cigarette smell concentration of smoke of the cigarettes are enhanced, the stem shred wood sense is lightened, the taste is improved, and the present invention has good taste, and clean and comfortable after taste. The cream effectively makes up for the conditions of low tobacco nicotine content and insufficient tobacco fragrance of tobaccos in China, and the present invention is an ideal fragrance substance.
Description
The invention belongs to balm and the using method class thereof from the flue-cured tobacco bud, extracted.
Cigarette market demands cigarette commodity have the attribute of " high fragrance, high concentration, high strength, low tar " both at home and abroad at present.And owing to low, the cigarette insufficient fragrance of nicotine content in China's raw tobacco, for the cigarette of producing this attribute has caused objective obstacle, this has not only influenced the domestic market of cigarette, also influences China's cigarette and squeezes into the international market.Be meeting the market requirement, remedy the raw tobacco defective, utilize material production cigarette, the reconstituted tobacoo of tobacco leaf itself, the perfuming material of expanded cut stem, thereby reform China cigarette composition is necessary.
Cigarette is to get the leaf material, presses the tobacco cultivation standard, must pinch and pluck bud.China's year plantation tobacco leaf can be plucked flue-cured tobacco dried flower flower bud every year more than 40,000 tons more than 2,000 ten thousand mu, and these buds were all thrown away in vain in the past, and this not only causes the wasting of resources, also causes tobacco diseases to propagate, and influences the land for growing field crops leaf tobacco production.
The objective of the invention is to develop a kind of flue-cured tobacco bud cream that from the flue-cured tobacco bud, extracts.Balm flue-cured tobacco fragrance is true to nature, is used for the perfuming of cigarette and reconstituted tobacoo, can increase cigarette flavor and smoke concentration, increases the physiological strength of cigarette, covers assorted gas, make jealous pure and mild, pleasant impression is totally comfortable, coordinate.
The objective of the invention is to realize in the following manner, flue-cured tobacco bud cream is extracted by the flue-cured tobacco bud, be the brownish red paste, has strong flue-cured tobacco cigarette fragrance, proportion (d25/25 ℃) 1.2-1.5, nicotine content 4-4.9% is dissolved in the distilled water, the molten amount 64% of alcohol, pure insoluble amount 36% contain total alkaloid 1.2-1.5%, total reducing sugar 2.2-2.5%, total nitrogen 4.2-4.5%.
The flue-cured tobacco bud is used for cigarette, reconstituted tobacoo, expanded cut stem perfuming, and the addition in reconstituted tobacoo is 0.8-1.4%, is excellent with 1-1.2%, and directly the addition in cigarette shreds is 0.3-1%, is excellent with 0.5-0.8%.
Balm of the present invention extracts from the flue-cured tobacco bud, its extraction process such as application for a patent for invention " extracting the technology of balm from tobacco bud " (application number 90107606.6, date of publication 910227) described technology: earlier bud is dried in the shade, screens impurity elimination, with 95% alcohol mixing, sealing preliminary treatment 5-7 days, pour in the extractor, the mother liquor that adds back operation generation carries out the extraction first time under the temperature in normal pressure.Under 1.8-2.7kg/cm2 pressure, 130-135 ℃, carry out the extraction second time again.Adding distil water carries out third and fourth time extraction under 95-100 ℃ again.First and second time collection liquid merges also and filters, and staticly settles, thermal release goes out Ca
++, Mg
++, again in vacuum concentration pot under negative pressure low temperature vacuum concentrate, take out and join perfume (or spice), quality inspection, packing and promptly get balm.The gas that produces when vacuum concentrates, liquid are through separating, liquid vacuum again concentrates, and gas pumps after cooling, with third and fourth time extract and staticly settle, the steam condensate after the thermal release filters, after staticly settling, clear liquid is made the mother liquor of first and second time extraction.
Balm of the present invention detects through Zhengzhou Tobacco Research Institute of CNTC, on average contains total reducing sugar 2.36%, total alkaloid 1.36%, total nitrogen 4.34%.
Detect through Institute of Analysis of Wuhan University and food inspection center, Hubei Province, its result is: be dissolved in the distilled water pure molten amount 64%, pure insoluble amount 36%, nicotine content 4%-4.9%.
Because of balm of the present invention is to extract from the flue-cured tobacco bud, spices extracts fully, and balm flue-cured tobacco fragrance is true to nature, can be used for reconstituted tobacoo cigarette and expanded cut stem perfuming.
The Changde Cigarette Factory scientific research institution has carried out adding the experimental formula of this balm in reconstituted tobacoo, first and second grades of Virginian-type cigarettes and first and second grades of blended type cigarettes, its experimental result is as follows:
1. to the influence of cigarette inherence, presentation quality:
In the first class Virginian-type cigarette, add 0.3%, 0.4%, 0.5%, 1% balm respectively, roll up by the machine cigarette, cure back the packing with YT13B, MK8/MA8, MK9-5/PATF3, unpack after seven days inspection, do not find that cigarette has propped up macula lutea, oil stain, the preproduction inherent quality is smoked panel test by national GB5606-5610-85 standard, its comparing result sees Table 1, table 2, table 3.
Table 1(measurement unit branch)
The assorted gas of test item color and luster fragrance stimulates pleasant impression to add up to
Testing result 14 37.75 14.25 9 17.5 92.5
Conclusion: in the first class Virginian-type cigarette, add this balm of 1%, it is strong and brisk in taste, stimulation reduces, pleasant impression is totally comfortable.To smoke panel test in the same old way 91 minutes.
Table 2(measurement unit branch)
The assorted gas of test item color and luster fragrance stimulates pleasant impression to add up to
Testing result 13.5 37.25 14.25 8.625 17.875 91.5
Conclusion: in the first class Virginian-type cigarette, add this balm of 1%, reduce in the prophyll assembly side 12% tobacco leaf service rating, only outside the dim spot, its fragrance, pleasant impression all are better than or equal prophyll assembly side cigarette gloss, reach first class cigarette standard a little, and cost reduces by 37%.To smoke panel test in the same old way 91 minutes.(table 3 is seen the literary composition back)
As seen from the table, add this balm after, the nicotine content of cigarette improves, tar content reduces, cigarette props up middle TPM, a mouthful number slightly reduces, resistance to suction equates, helps cigarette quality and improves.
2. the credit of cigarette branching is analysed and be the results are shown in Table 4.(table 4 is seen the literary composition back)
As seen from the table: after adding balm the main chemical compositions of cigarette cigarette itself is not had influence, chemical composition is coordinated, and only propping up at cigarette increases cigarette fragrance, strength, reduction tar when burning and sucking.
Jianshi cigar factory with in the flue-cured tobacco in first class Virginian-type cigarette " seedling man " and flat taste blended type cigarette " group camel " prescription two use instead in three, apply 0.7% flue-cured tobacco bud cream sample preparation then, contrast is smoked panel test through Zhengzhou tobacco scientific research institute, and strength increases, cigarette fragrance enrichment, coordination, cleaner.
Zhengzhou Tobacco Research Institute of CNTC adds the experiment of this balm amount in reconstituted tobacoo and pipe tobacco, its conclusion is: by smokeing panel test, identify, and more satisfactory with the 1.0-1.2% addition in reconstituted tobacoo, more satisfactory with 0.5-0.8% in pipe tobacco.Along with the increase of balm addition, inhaling flavor has improvement, the increase of cigarette fragrance, smoke concentration to increase, and strength slightly increases, improves color and luster, pleasant impression coordination, comfortable, clean, and combustibility improves.How Germany consults after tobacco spice company gives this balm opium factory of a few family of this state detect to smoke panel test, and thinks the novel tobacco aromatics using that cigarette is fabulous.
This flue-cured tobacco bud cream is water-soluble, has strong cigarette fragrance, be used for cigarette, reconstituted tobacoo, expanded cut stem perfuming, can change the tobacco leaf formulation service rating after the adding, reduce cost, improve the cigarette grade, improve smoke concentration, improve cigarette fragrance, improve jealous, alleviate the wooden breath of stem, stem and thin slice color and luster are significantly improved.China's nicotine content of tobacco leaves is low to remedying, the cigarette insufficient fragrance is fruitful for this balm, is desirable perfuming material.
Table 3
NO
Analysis result 123456
Analysis project
TPM (milligram /) 28.23 27.94 27.59 28.37 27.59 28.30
Moisture content (milligram /) 3.105 3.073 3.035 3.1207 3.035 3.113
Transfer alkali (milligram/prop up) 0.914 0.929 0.923 0.928 0.935 0.943
Tar (milligram /) 24.21 23.94 23.63 24.32 23.62 24.24
Mouth number (mouthful /) 9.5 9.2 9.0 9.5 9.4 9.6
Cigarette average weight (gram) 0.92 0.92 0.92 1.00 1.00 1.00
Cigarette Zhi Pingjun resistance to suction (millimetres of mercury) 60 ± 5 60 ± 5 60 ± 5 65 ± 5 65 ± 5 65 ± 5
Annotate: 1,4 is golden lotus cigarette in the table, and 2,3,5,6 for adding the golden lotus cigarette of this balm.
Table 4
NO total reducing sugar % total nicotine % total nitrogen % total alkali nitrogen % protein % total volatile alkaline % schmuck value candy alkali ratio
1 19.02 1.08 1.53 0.187 8.39 0.1210 2.27 17.61
2 19.15 1.10 1.47 0.190 8.00 0.1223 2.39 17.41
Annotate: 1 is golden lotus pipe tobacco contrast sample in the table, and 2 for adding the golden lotus cigarette sample of 0.5% balm.
Claims (3)
1, flue-cured tobacco bud cream is characterized in that being extracted by the flue-cured tobacco bud, is the brownish red paste, has strong flue-cured tobacco cigarette fragrance, and proportion (d25/25 ℃) 1.2-1.5 is dissolved in the distilled water, pure molten amount 64%, pure insoluble amount 36%; Contain total alkaloid 1.2-1.5%, total reducing sugar 2.2-2.5%, total nitrogen 4.2-4.5%, nicotine content 4-4.9%.
2, the using method of flue-cured tobacco bud cream is characterized in that can be used for cigarette, reconstituted tobacoo and expanded cut stem perfuming, and the addition in reconstituted tobacoo is 0.8-1.4%, and the addition in cigarette shreds is 0.3-1%.
3, using method according to claim 2 is characterized in that the addition of balm in reconstituted tobacoo is 1-1.2%, and the addition in cigarette shreds is 0.5-0.8%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 93101941 CN1029768C (en) | 1993-02-18 | 1993-02-18 | Flue-cured tobacco bud cream and its application method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 93101941 CN1029768C (en) | 1993-02-18 | 1993-02-18 | Flue-cured tobacco bud cream and its application method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1077358A CN1077358A (en) | 1993-10-20 |
| CN1029768C true CN1029768C (en) | 1995-09-20 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 93101941 Expired - Fee Related CN1029768C (en) | 1993-02-18 | 1993-02-18 | Flue-cured tobacco bud cream and its application method |
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| Country | Link |
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| CN (1) | CN1029768C (en) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20100116281A1 (en) * | 2008-11-07 | 2010-05-13 | Jerry Wayne Marshall | Tobacco products and processes |
| US8955523B2 (en) * | 2010-01-15 | 2015-02-17 | R.J. Reynolds Tobacco Company | Tobacco-derived components and materials |
| US20130014771A1 (en) | 2011-01-13 | 2013-01-17 | R. J. Reynolds Tobacco Company | Tobacco-derived components and materials |
| CN103190693B (en) * | 2013-04-19 | 2015-03-25 | 安徽中烟工业有限责任公司 | Extracting method for tobacco flower extract and application thereof |
| CN105212260A (en) * | 2014-05-26 | 2016-01-06 | 何氪 | A kind of reconstituted tobacoo and cigarette products |
-
1993
- 1993-02-18 CN CN 93101941 patent/CN1029768C/en not_active Expired - Fee Related
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| Publication number | Publication date |
|---|---|
| CN1077358A (en) | 1993-10-20 |
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