CN102963890B - Carbonization activation integrated furnace - Google Patents
Carbonization activation integrated furnace Download PDFInfo
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- CN102963890B CN102963890B CN201210368594.2A CN201210368594A CN102963890B CN 102963890 B CN102963890 B CN 102963890B CN 201210368594 A CN201210368594 A CN 201210368594A CN 102963890 B CN102963890 B CN 102963890B
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- carbonization
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- supplies room
- water vapor
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- 230000004913 activation Effects 0.000 title claims abstract description 33
- 238000003763 carbonization Methods 0.000 title abstract 3
- 239000000463 material Substances 0.000 claims abstract description 53
- 238000002485 combustion reaction Methods 0.000 claims abstract description 40
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 36
- 238000010438 heat treatment Methods 0.000 claims abstract description 9
- 238000004519 manufacturing process Methods 0.000 claims description 24
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims description 12
- 239000003546 flue gas Substances 0.000 claims description 12
- 239000007789 gas Substances 0.000 claims description 11
- 238000012545 processing Methods 0.000 claims description 6
- 239000010881 fly ash Substances 0.000 claims description 4
- 238000001035 drying Methods 0.000 abstract 1
- 239000011449 brick Substances 0.000 description 21
- 239000003034 coal gas Substances 0.000 description 7
- 238000000034 method Methods 0.000 description 5
- 239000000779 smoke Substances 0.000 description 5
- 238000001816 cooling Methods 0.000 description 4
- 239000012190 activator Substances 0.000 description 3
- 238000007599 discharging Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 239000011464 hollow brick Substances 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 239000002699 waste material Substances 0.000 description 3
- 230000003213 activating effect Effects 0.000 description 2
- 239000000571 coke Substances 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000003610 charcoal Substances 0.000 description 1
- 239000000567 combustion gas Substances 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 230000008676 import Effects 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000008400 supply water Substances 0.000 description 1
- 238000013022 venting Methods 0.000 description 1
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- Carbon And Carbon Compounds (AREA)
Abstract
The invention relates to a carbonization activation integrated furnace, which includes a material chamber. The top of the material chamber is provided with a feed inlet, the bottom is provided with a discharge port, and the material chamber is used for storing and transporting materials. A drying section, a carbonization section, and an activation section that are communicated are disposed between the feed inlet and the discharge port from top to bottom in order. The furnace also includes a combustion chamber disposed outside the material chamber and used for heating materials in the material chamber. The activation section of the material chamber is equipped with a steam pipeline, which has several water vapor outlets molded in the vertical direction. The setting mode of the water vapor outlets enables water vapor to contact more materials in the vertical direction, and the water vapor outlets are uniformly distributed and are easy to operate. Meanwhile, water vapor moves in the horizontal direction, thus solving the problem that the pressure of materials above limits the upward movement range of water vapor.
Description
Technical field
The present invention relates to a kind of carbonization-activation integral furnace, specifically a kind of carbonization-activation integral furnace by the outer hot indirect heating of external combustion.
Background technology
The preparation of activated coke or gac needs use to prepare stove to complete, and is preparing in stove the process completing charing or activation, final obtained required activated coke or gac.At present, gac/Jiao prepares stove and mainly contains following form, and one is Stepple furnace, and mainly in China's application, it is for being interrupted the mode of production, and separate unit treatment capacity is low, only has hundreds of ton every year; Another kind is multiple hearth furnace, is derived from the U.S., and the body of heater shell of multiple hearth furnace is cylindrical, is rolled form by general steel plate; Inner lining refractory, stove is made to be partitioned into multistage with heterotypic fire brick or common laying fireproof bricks hearth structure, every section of siege respectively around siege and/or middle section material falling hole is set, solid materials is stirred by the stirrer gear be installed on slow speed of revolution central shaft agitating arm step by step by (then by Inside To Outside on lower floor's siege) inside lateral on siege, is entered next section of siege, the design of this stove is comparatively complicated, and very high to the equipment requirements such as central shaft, rake teeth.In addition, above-mentioned Stepple furnace and multiple hearth furnace can only complete activation, and charing needs to carry out in a separate device, increases the complicacy of production technique.One is also had to be pierce smith converter, because its material advances by body of heater self angle of inclination and oblique flight, the rate of advance of the bad control material of production lightweight charcoal, and above-mentioned activation furnace is all interior heating, combustion gases directly contact with material, inevitably cause raw material surface combustion, reduce the quality of gac, and be usually arranged on below due to the heating unit of pierce smith converter, be heated evenly so material barrel needs ceaselessly to rotate guarantee material.
In prior art, Chinese patent literature CN2535399 discloses a kind of bucket-type carbon activation furnace apparatus, comprise furnace wall, storagetank, oxidation air flue, combustion chamber, cooling zone, water vapour import, discharger, discharging hopper, blast pipe, dividing plate, side flue, exhanst gas outlet, packing, stove seat, crown cap, water seal, combustion chamber in furnace wall is arranged in order with bucket type brick to form, laterally horizontal air flue is formed between adjacent brick wall, repeatedly put up and down, vertical material road is formed between brick hole, joint, brick hole forms venting port, horizontal air flue communicates with the side flue being provided with blast pipe, dividing plate is divided into arid zones combustion chamber, carbide bound, activation zone, bucket type brick is the hollow brick of outer image bucket, the upper surface of brick is square, brick hole inwall section is trapezoidal, brick inwall arranges leg.Described bucket type brick is profile is round table-like hollow brick, and the upper surface of brick is square, and brick hole inwall section is trapezoidal, and brick inwall arranges leg.Described bucket type brick is the hollow brick of outer image bucket, and the upper surface of brick is square, and brick hole inwall section is trapezoidal, and brick wall face, front and back is vertical surface, and brick wall face, left and right is inclined-plane.The oxidation air flue of oxygenizement has been set on combustion chamber top.Water vapor inlet mouth is arranged on the bottom of cooling zone.Exhanst gas outlet is arranged on bottom of furnace body side flue or is arranged on body of heater top side flue.
The vertical material road of above-described bucket type brick composition, there is opening joint, brick hole, make the volatile matter of material after being heated can precipitate into horizontal air flue, this structure makes partial material be directly exposed in smoke chamber, when volatile matter is separated out, can partial material be brought in smoke chamber, pollute and the waste of raw material, flue gas directly contacts the burning that can cause material with material simultaneously, affects the quality of gac; And the water vapor as activator needed for above-mentioned activation zone, its inlet mouth is arranged on the bottom of cooling zone, water vapor needs to pass through cooling zone, reduction temperature of charge becomes superheated vapour and enters material road activation zone after heat exchange, material is activated, because water vapor enters activation zone from bottom, water vapour moves from the bottom to top, be subject to the inhibition of top pressure and material, water vapor upwards range ability is little, so just limit the scope of activation zone, activation efficiency is reduced, thus have impact on the production efficiency of product.Although the activating apparatus of described pierce smith converter is inserted into material barrel inside, but just spray water vapor by activating apparatus top end opening, make water vapor diffusion even by the rotation of material barrel, in addition, body of heater rotates need use very large power, and the complex structure of this body of heater.
Summary of the invention
Technical problem to be solved by this invention is that in prior art, activator feedway is arranged on below activation section, water vapor upwards range ability is little, have impact on range of activation and activation efficiency, thus provide one that water vapor can be made to be uniformly distributed at described activation section, thus improve the carbonization-activation integral furnace of activation efficiency.
For solving the problems of the technologies described above, the present invention is achieved by the following technical solutions:
A kind of carbonization-activation integral furnace, comprising:
Supplies room, described supplies room top is provided with opening for feed, and bottom is provided with discharge opening, for storing and convey materials, sets gradually the dryer section of connection between described opening for feed and described discharge opening from top to bottom, charing section, activation section;
Combustion chamber, is arranged on the outside of described supplies room, for heating the material in described supplies room;
At the activation section of described supplies room, be vertically provided with steam-pipe from the bottom to top, described steam-pipe forms several steam outlet at vertical direction.
Described steam outlet is evenly arranged.
Described steam outlet is provided with 400-600.
The outer wall of described supplies room forms production well, and described production well is uniformly distributed and for angling hole, and the vergence direction of described production well is higher than its one end towards described supplies room towards one end of described combustion chamber.
The sidewall of described combustion chamber is provided with burner, described burner layered arrangement, every layer of described burner is arranged on described body of heater surrounding uniformly, and the described burner that layering is arranged is arranged on the middle hypomere of described body of heater.
Be provided with below described sidewall of combustion chamber and let out grey mouth.
Be provided with exhaust gases passes in described combustion chamber, the top of described combustion chamber is provided with flue gas processing device, and described flue gas processing device comprises the fly-ash separator, induced draft fan and the chimney that connect successively.
Described discharge opening lower end is connected with refrigerating unit.
Described refrigerating unit comprises vapour line and circulating water pipework, and described vapour line is connected with described water vapour pipeline.
Described supplies room is at least one.
Technique scheme of the present invention has the following advantages compared to existing technology:
(1) a kind of carbonization-activation integral furnace of the present invention, comprise supplies room, described supplies room top is provided with opening for feed, bottom is provided with discharge opening, for storing and convey materials, the dryer section of connection is set gradually from top to bottom, charing section, activation section between described opening for feed and described discharge opening; Combustion chamber, is arranged on the outside of described supplies room, for heating the material in described supplies room; At the activation section of described supplies room, be vertically provided with steam-pipe from the bottom to top, described steam-pipe forms several steam outlet at vertical direction.The set-up mode of described steam outlet, make water vapor in the vertical direction touch more material, and be evenly distributed, convenient operation, simultaneously water vapor is to horizontal motion, reduces because the pressure of top material causes water vapor to move up range limited problem.
(2) outer wall of supplies room of the present invention forms production well, and described production well is uniformly distributed and is angling hole, and the vergence direction of described production well is higher than its one end towards described supplies room towards one end of described combustion chamber.Described charing section material is heated the coal gas of rear generation, described activation section material is heated the water-gas of rear generation, enter in described combustion chamber by this production well, there is combustion reactions, the high-temperature flue gas produced can heat material, and the setting of described production well, re-uses inflammable gas, both decrease coal gas treatment process, it also avoid calorific loss simultaneously; Secondly, described production well is obliquely installed, and makes coal gas when entering described combustion chamber, is unlikely to described material together to be brought into into combustion chamber, avoids waste and the pollution of resource.
(3) sidewall of combustion chamber of the present invention is provided with burner, described burner layered arrangement, and every layer of described burner is arranged on described body of heater surrounding uniformly, and the described burner that layering is arranged is arranged on the middle hypomere of described body of heater.Described burner is placed in the below of described combustion chamber, and add thermogenetic heat smoke from bottom to top by described supplies room outer wall and heat exchange, temperature reduces gradually, thus avoids the calorific loss discharging high-temperature flue gas and bring.
Accompanying drawing explanation
In order to make content of the present invention be more likely to be clearly understood, below in conjunction with accompanying drawing, the present invention is further detailed explanation, wherein,
Fig. 1 is the front view of a kind of carbonization-activation integral furnace of the present invention;
Fig. 2 is the vertical view of a kind of carbonization-activation integral furnace of the present invention;
Fig. 3 is the schematic diagram of the production well of supplies room outer wall of the present invention.
In figure, Reference numeral is expressed as:
1-opening for feed, 2-dryer section, 3-carbonizes section, 4-activation section, 5-steam-pipe, 6-vapour line, 7-discharge valve, 8-refrigerating unit, 9-circulating water pipework, 10-lets out grey mouth, 11-burner, 12-fly-ash separator, 13-induced draft fan, 14-chimney, 15-water vapour, 16-coal gas, 17-water-gas, 18-discharge opening, 19-supplies room, 20-flue, 21-combustion chamber, 22-production well.
Embodiment
As Figure 1-3, in the present embodiment, described a kind of carbonization-activation integral furnace, its ecto-entad comprises combustion chamber 21 successively, supplies room 19;
Described supplies room 19 top is provided with opening for feed 1, and bottom is provided with discharge opening 18, for storing and convey materials, sets gradually the dryer section 2 of connection between described opening for feed 1 and described discharge opening 18 from top to bottom, charing section 3, activation section 4;
Described combustion chamber 21 is arranged on the outside of described supplies room 19, for heating the material in described supplies room 19;
Wherein, at the activation section 4 of described supplies room 19, be vertically provided with steam-pipe 5 from the bottom to top, for providing the water vapor as activator needed for activation section 4, described steam-pipe 5 forms several steam outlet at vertical direction.And described steam outlet is evenly arranged, as preferred embodiment, described steam outlet is provided with 500.As the embodiment that other can convert, steam outlet herein also can select 400-600.The set-up mode of described steam outlet, make water vapor in the vertical direction touch more material, and be evenly distributed, convenient operation, simultaneously water vapor is to horizontal motion, reduces because the pressure of top material causes water vapor to move up range limited problem.
On the basis of above-described embodiment, production well 22 is formed further on the outer wall of described supplies room 19, described production well 22 is uniformly distributed and for angling hole, and the vergence direction of described production well 22 is higher than its one end towards described supplies room 19 towards one end of described combustion chamber 21.Described dryer section 2 material is heated the water vapor 15 of rear generation, described charing section 3 material is heated the coal gas 16 of rear generation, described activation section 4 material is heated the water-gas 17 of rear generation, enter in described combustion chamber 21 by this production well 22, combustion reactions occurs, and the high-temperature flue gas of generation can heat material, the setting of described production well 22, inflammable gas is re-used, had both decreased coal gas treatment process, and it also avoid calorific loss simultaneously; Secondly, described production well 22 is obliquely installed, and makes coal gas when entering described combustion chamber 21, is unlikely to together to be brought into by material into described combustion chamber 21, avoids waste and the pollution of resource.
The sidewall of described combustion chamber 21 is provided with burner 11, described burner 11 layered arrangement, every layer of described burner 11 is arranged on described body of heater surrounding uniformly, and the described burner 11 that layering is arranged is arranged on the middle hypomere of described body of heater.Described burner 11 is placed in the below of described combustion chamber 21, and add thermogenetic heat smoke from bottom to top by described supplies room 19 outer wall and heat exchange, temperature reduces gradually, thus avoids the calorific loss discharging high-temperature flue gas and bring.
As preferred embodiment, be provided with below the sidewall of described combustion chamber 21 and let out grey mouth 10.
Be provided with exhaust gases passes 20 in described combustion chamber 21, the tortuous flue that described exhaust gases passes 20 is made up of temperature-resistant material, heat smoke passes through tortuous flue by the outer wall homogeneous heating of described supplies room 19.
As preferably, described supplies room 19 can be set to multiple, and when arranging multiple, have certain distance between the outer wall of described supplies room 19, described distance can make flue gas pass through, and ensures that the outer wall-heated of each described supplies room 19 is even.
The top of described combustion chamber 21 is provided with flue gas processing device, and described flue gas processing device comprises the fly-ash separator 12, induced draft fan 13 and the chimney 14 that connect successively.
Described discharge opening 18 lower end is provided with discharge valve 7, and by the time of the carbonization-activation of described discharge valve 7 adjustable material, when opening described discharge valve 7, the lag cooler that described activation material enters into the described refrigerating unit 8 of below cools.
Described refrigerating unit 8 comprises vapour line 6 and circulating water pipework 9, and described vapour line 6 is connected with described steam-pipe 5.The water vapor absorbing heat enters into described steam-pipe 5 by described vapour line 6, activates the material of described activation section 4.Certainly, as selectable embodiment, the water vapor described in described activation section 4, also can supply water vapor by other devices to described water vapor pipeline 5, and the embodiment selected in the present embodiment farthest can make use of the heat of native system self, improve thermo-efficiency.
Described discharge opening 18 place of multiple described supplies room 19 according to the number setting supporting with it of described supplies room 19, also can be connected with same described refrigerating unit 8 by described refrigerating unit 8.
Obviously, above-described embodiment is only for clearly example being described, and the restriction not to embodiment.For those of ordinary skill in the field, can also make other changes in different forms on the basis of the above description.Here exhaustive without the need to also giving all embodiments.And thus the apparent change of extending out or variation be still among protection scope of the present invention.
Claims (8)
1. a carbonization-activation integral furnace, comprising:
Supplies room (19), described supplies room (19) top is provided with opening for feed (1), bottom is provided with discharge opening (18), for storing and convey materials, the dryer section (2) of connection is set gradually from top to bottom between described opening for feed (1) and described discharge opening (18), charing section (3), activation section (4);
Combustion chamber (21), is arranged on the outside of described supplies room (19), for heating the material in described supplies room (19);
It is characterized in that, described supplies room is set to multiple, and at the activation section (4) of described supplies room (19), be vertically provided with steam-pipe (5) from the bottom to top, described steam-pipe (5) forms several steam outlet at vertical direction;
The outer wall of described supplies room (19) forms production well (22), described production well (22) is uniformly distributed and for angling hole, and the vergence direction of described production well (22) is higher than its one end towards described supplies room (19) towards the one end of described combustion chamber (21).
2. a kind of carbonization-activation integral furnace according to claim 1, is characterized in that, described steam outlet is evenly arranged.
3. a kind of carbonization-activation integral furnace according to claim 1, is characterized in that, described steam outlet is provided with 400-600.
4. a kind of carbonization-activation integral furnace according to claim 1 and 2, it is characterized in that, the sidewall of described combustion chamber (21) is provided with burner (11), described burner (11) layered arrangement, every layer of described burner (11) is arranged on body of heater surrounding uniformly, and the described burner (11) that layering is arranged is arranged on the middle hypomere of described body of heater.
5. a kind of carbonization-activation integral furnace according to claim 3, is characterized in that, is provided with and lets out grey mouth (10) below described combustion chamber (21) sidewall.
6. a kind of carbonization-activation integral furnace according to claim 4, it is characterized in that, exhaust gases passes (20) is provided with in described combustion chamber (21), the top of described combustion chamber (21) is provided with flue gas processing device, and described flue gas processing device comprises the fly-ash separator (12), induced draft fan (13) and the chimney (14) that connect successively.
7. a kind of carbonization-activation integral furnace according to claim 1 and 2, is characterized in that, described discharge opening (18) lower end is connected with refrigerating unit (8).
8. a kind of carbonization-activation integral furnace according to claim 7, is characterized in that, described refrigerating unit (8) comprises vapour line (6) and circulating water pipework (9), and described vapour line (6) is connected with described steam-pipe (5).
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| Application Number | Priority Date | Filing Date | Title |
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| CN201210368594.2A CN102963890B (en) | 2012-09-28 | 2012-09-28 | Carbonization activation integrated furnace |
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| CN201210368594.2A CN102963890B (en) | 2012-09-28 | 2012-09-28 | Carbonization activation integrated furnace |
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| CN102963890B true CN102963890B (en) | 2015-04-01 |
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Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103395782B (en) * | 2013-08-08 | 2015-05-20 | 北京金润华扬科技有限公司 | Movable carbon activation method |
| CN103449432B (en) * | 2013-08-30 | 2015-05-06 | 林旭 | Spouted type activation furnace and method for producing super-capacitor carbon by virtue of same |
| CN104100980B (en) * | 2014-07-01 | 2016-03-16 | 深圳合续环境科技有限公司 | A kind of small-sized rubbish charing combustion furnace |
| CN104310393B (en) * | 2014-09-29 | 2016-08-17 | 大连理工大学 | The device of a kind of continuous prodution activated carbon and utilize the method that this device prepares activated carbon |
| CN107954426A (en) * | 2017-12-08 | 2018-04-24 | 山东汉菱电气有限公司 | For generating the device of activated carbon |
| CN108190852A (en) * | 2017-12-21 | 2018-06-22 | 湖南顶立科技有限公司 | A kind of multistage vertical type continuous carbonization furnace |
| CN109368641B (en) * | 2018-12-12 | 2024-02-20 | 宁夏尼西活性炭有限公司 | Device for recycling combustible gas prepared from activated carbon |
| CN109607536B (en) * | 2019-01-30 | 2023-08-08 | 安徽宝隽机车部件有限公司 | Carbonization and activation combined type vertical furnace |
| CN109629042A (en) * | 2019-02-13 | 2019-04-16 | 江苏苏通碳纤维有限公司 | A kind of carbon activation integral furnace continuously preparing phenolic resin based activated carbon fiber |
| CN110819363B (en) * | 2019-10-24 | 2021-06-01 | 东南大学 | Multi-cavity series self-heating external heating converter biomass carbonization-activation device and method |
| CN110734066B (en) * | 2019-10-24 | 2023-04-21 | 东南大学 | Internal and external heating self-heating type integrated biomass carbonization-activation device and method |
| CN111807364A (en) * | 2020-08-11 | 2020-10-23 | 聚农(湖州)新能源科技有限公司 | Movable miniaturized biomass continuous steam activation method and activation machine |
| CN113636694A (en) * | 2021-09-07 | 2021-11-12 | 北京国电富通科技发展有限责任公司 | Transformer substation/convertor station domestic sewage treatment system and treatment method |
| CN117146256B (en) * | 2023-08-31 | 2024-04-09 | 青岛冠宝林活性炭有限公司 | Method for co-production of activated carbon and steam and comprehensive utilization of heat energy |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2535399Y (en) * | 2002-03-29 | 2003-02-12 | 林勇胜 | Bucket-type carbon activation furnace apparatus |
| US8568569B2 (en) * | 2009-12-09 | 2013-10-29 | Chavond-Barry Engineering | Method and apparatus for efficient production of activated carbon |
| CN102649550A (en) * | 2011-02-25 | 2012-08-29 | 王全祥 | Carbonization-activation integrated activated carbon production apparatus |
| CN102295282B (en) * | 2011-08-08 | 2015-11-04 | 北京国电富通科技发展有限责任公司 | Carbonization-activation integral furnace |
| CN202246074U (en) * | 2011-09-19 | 2012-05-30 | 山东科技大学 | Carbonization furnace for activated coke production |
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