CN102960722A - Production method of edible carbon powder - Google Patents
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Abstract
The invention relates to an edible health care product and particularly relates to a production method of edible carbon powder. The production method comprises the following steps of: A) preparing a decoction liquid: taking oat flour, black sesame and soybean, adding 3-5 times of water, performing decoction for 4-5h, filtering and concentrating to obtain a first decoction liquid with the solid content of 5%-20%; taking bletilla and Chinese angelica root powder, adding 1-2 times of water, performing decoction for 6-7h, filtering and concentrating to obtain a second decoction liquid with the solid content of 30%-40%; and then merging the first decoction liquid with the second decoction liquid to obtain the decoction liquid; and B) preparing the edible carbon powder: weighing 40-60 parts by weight of carbon powder with the particle size of 600-1100 meshes, 15-20 parts by weight of millet flour, 0.5-1.8 parts by weight of peppermint, 3-5 parts by weight of Szechwan lovage rhizome powder and 40-50 parts by weight of tea liquor, mixing with the decoction liquid obtained in the step A), and then performing microwave vacuum treatment which is specifically realized by vacuumizing till the vacuum degree is (-0.09MPa)-(-0.06MPa); and further performing microwave treatment, wherein the microwave frequency is 245MHz-400MHz, and the microwave treatment time is 0.5-1min. The edible carbon powder prepared by the invention has good health care effects.
Description
Technical field
The present invention relates to a kind of edible health care product, relate in particular to the production method of edible powdered carbon.
Background technology
Charcoal can eat, and it is arranged from ancient times, mostly is used for curing the disease, the Han dynasty well-known doctor opens grandfather's elder brother (teacher of Zhang Zhongjing) and just summed up the Chinese medical ancient prescription in the past, swallow with charcoal porphyrize Cheng Fenrang patient, the diarrhoea that the treatment cold of insufficiency type causes is fired into charcoal treatment enterogastritis with mountain quarrel and nuclear thereof.Also there be " silicon carbon is peaceful " to be used for the patient day in the modern doctor trained in Western medicine medicine and take toxicity reduction antidiarrheal.Thisly day take charcoal and generally at high temperature process and get through dry distillation charring and with superheated steam with timber, xylocarp shell and beastly bone, its unharmful substance, such as heavy metal lead, arsenic, mercury etc., also without malignant bacteria, the harmful material such as nonpersistent pesticide more.By former its chemical bonding structure quite stable of molecular charcoal molecule of charcoal, generally not with weak acid or weak base chemically reactive, can not be absorbed so enter in the human body, and can the performance its function after, all excrete.
CN101120790B (2011-8-10) discloses a kind of edible bamboo charcoal paste and production method thereof, however the bamboo charcoal function singleness that the method is produced, and health-care effect haves much room for improvement.
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Summary of the invention
The purpose of this invention is to provide a kind of preparation method with edible powdered carbon of excellent health functions.
Above-mentioned technical purpose of the present invention is achieved by the following technical programs:
The production method of edible powdered carbon, it may further comprise the steps:
The preparation of A, decoction liquor: take by weighing by weight oatmeal 5-10 part, Semen sesami nigrum 3-5 part, soybean 5-10 part, bletilla 4-6 part, angelica powder 3-5 part, get described oatmeal, Semen sesami nigrum and soybean, add 3-5 times of decocting and boil 4-5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain the first decocting liquid of solid contents 5%-20%; Get described bletilla and angelica powder, add 1-2 times of decocting and boil 6-7h, filter, concentrate with reverse osmosis membrane, obtain the second decocting liquid of solid contents 30%-40%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor;
The preparation of B, edible powdered carbon: take by weighing by weight particle diameter and be 600-1100 purpose powdered carbon 40-60 part, millet powder 15-20 part, peppermint oil 0.5-1.8 part, rhizome of chuanxiong powder 3-5 part, tea juice 40-50 part and mix with steps A gained decoction liquor, then carrying out microwave vacuum processes, send in the microwave vacuum tank after specifically all substances being mixed, then vacuumize process to vacuum for-0.09MPa～-0.06MPa; Carry out microwave treatment, microwave frequency is 245MHz～400MHz again, and microwave treatment time is 0.5～1min.
In the decoction liquor of the present invention, oat is rich in microorganism and mineral matter and various nutrition, can give skin more moisture, Semen sesami nigrum is rich in anthocyanidin, have remarkable anti-aging effects, and its selenium that is rich in and various vitamin, can make skin be full of gloss and elasticity; Soybean is rich in dimension E and lecithin, can prevent skin aging and recover skin elasticity; Bletilla convergence myogenic, skin care can prevent pachylosis and aging, help to recover skin elasticity.Radix Angelicae Sinensis is rich in 17 seed amino acids and 23 kinds of inorganic elements of abundant dimension A, E, B12 and needed by human, can increase skin elasticity.
Millet is rich in protein, and contains carrotene, compound vitamin B, calcareous and potassium, is a kind of healthy food, has nourishing yin and nourishing blood, stomach strengthening and digestion promoting and the effect of calming the nerves.
Anti-oxidant and the radiation-resisting functional of intrinsic Tea Polyphenols, theanine, tea polysaccharide in the tea juice can prevent skin aging and recover skin elasticity.
Decoction liquor of the present invention and tea juice, powdered carbon, millet powder and the acting in conjunction of rhizome of chuanxiong powder can strengthen skin elasticity, reach the detoxicating, relieving inflammation effect; Under microwave vacuum is processed, synergistic function can occur between each material, play better health detoxifcation and health-care effect.
Microwave vacuum of the present invention is processed, fuel factor and non-thermal effect occur in each component simultaneously, during carry out microwave radiation heating, the frequency inverted directions that electromagnetic field in the microwave is several hundred million time even billions of times with per second so that polarization and this polarization of the different electric charges of material internal do not possess the ability of catching up with rapidly alternating electric field, cause the material internal friction and generate heat, i.e. so-called " interior heating ", so that each component blends mutually, and some reactions may occur, synergistic function occurs.
As preferably, the preparation of described decoction liquor is to get described oatmeal, Semen sesami nigrum and soybean, adds 3-5 times of decocting and boils 4-5h, filters, and filtered solution is concentrated with reverse osmosis membrane, obtains the first decocting liquid of solid contents 13%; Get described bletilla and angelica powder, add 1-2 times of decocting and boil 6-7h, filter, concentrate with reverse osmosis membrane, obtain the second decocting liquid of solid contents 32-35%; Then merge the first decocting liquid and the second decocting liquid.
As preferably, described edible powdered carbon preparation takes by weighing by weight 50 parts of particle diameter 800-1000 purpose powdered carbons, 18 parts of millet powder, 1 part of peppermint oil, 4 parts in rhizome of chuanxiong powder, 45 parts in tea juice and mixes with steps A gained decoction liquor, then carries out the microwave vacuum processing.
As preferably, the preparation method of described tea juice is:
(1), first witch hazel and tealeaves are cleaned, pulverize, press the weight ratio of 1:4-9 and mix witch hazel and tealeaves, add in the deionized water fully immersion 2-3 hour, then pour in the countercurrent extraction machine and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in the coarse filtration liquid, obtain preliminary filtered fluid;
(2), preliminary filtered fluid is carried out ultra-filtration filters, again ultrafiltration is seen through liquid and concentrate with reverse osmosis membrane, obtain the first concentrate of solid contents 5%-20%; Half of getting the first concentrate carried out Vacuum Concentration, and obtaining solid contents is the second concentrate of 30%-35%; Remaining the first concentrate and the second concentrate are mixed to get tea juice.
As preferably, it is to send in the microwave vacuum tank after all substances are mixed that described microwave vacuum is processed, and then vacuumizes to process to vacuum to be-0.07Pa; Carry out microwave treatment, microwave frequency is 300MHz again, and microwave treatment time is 0.5～1min.
As preferably, described powdered carbon is bamboo charcoal powder.
More preferably, the preparation method of described bamboo charcoal powder is:
(1) soil sample of bamboo wood Proterozoic is detected, requiring lead, arsenic, mercury content is zero;
(2) bamboo wood is experienced successively drying, pre-charing, charing, calcining and cooling, control combustion is warming up to 700-750 ℃ and be incubated 40-80min with the speed of 5-15 ℃/min, and then be warming up to 1000-1500 ℃ and be incubated 2-8h with the speed of 5-15 ℃/min, then the speed with 18-25 ℃/min is cooled to 300-400 ℃, cools to room temperature with the furnace again and obtains bamboo charcoal;
(3) powder crushing process.
More preferably, also comprise activation process before the described powder crushing process: being the Potassium Oxalate Solution 1:3-4 mixing submergence 3-5h in mass ratio of 8-10% with bamboo charcoal and the mass fraction that obtains, is neutrality with washed with de-ionized water to pH value then, drying.
The inventor finds to carry out activation process after the bamboo charcoal preparation again, can strengthen the antibacterial ability of charcoal, and the negative ion releasing function of charcoal of the present invention is improved, and can improve user's lung capacity, improves sleep quality.
As preferably, described powdered carbon is the Korean pine active carbon powder.
More preferably, the preparation method of described Korean pine active carbon powder is:
(1) soil sample of pine Proterozoic is detected, requiring lead, arsenic, mercury content is zero;
(2) pine is experienced successively drying, pre-charing, charing, calcining and cooling, control combustion is warming up to 900-1000 ℃ and be incubated 40-80min with the speed of 5-15 ℃/min, and then be warming up to 1600-1800 ℃ and be incubated 2-8h with the speed of 5-15 ℃/min, then the speed with 18-25 ℃/min is cooled to 300-400 ℃, cools to room temperature with the furnace again;
(3) powder crushing process.
As preferably, described step B carries out after microwave vacuum processes, and it is the pill of 1-2mm or the tablet of 2-4mm that material is further made diameter.
The specific embodiment
Embodiment one
The preparation of decoction liquor: take by weighing by weight 5 parts of oatmeals, 3 parts of Semen sesami nigrums, soybean 5-10 part, 4 parts of bletillas, 3 parts of angelica powders, get described oatmeal, Semen sesami nigrum and soybean, add 3 times of decoctings and boil 4h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain the first decocting liquid of solid contents 5%; Get described bletilla and angelica powder, add 1 times of decocting and boil 6h, filter, concentrate with reverse osmosis membrane, obtain the second decocting liquid of solid contents 30%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor.
The preparation method of bamboo charcoal powder is: the soil sample to the bamboo wood Proterozoic detects, and requiring lead, arsenic, mercury content is zero; Bamboo wood is experienced drying, pre-charing, charing, calcining and cooling successively, control combustion is warming up to 700-720 ℃ and be incubated 40-60min with the speed of 5-10 ℃/min, and then be warming up to 1000-1200 ℃ and be incubated 2-3h with the speed of 5-10 ℃/min, then the speed with 18-20 ℃/min is cooled to 300-350 ℃, cools to room temperature with the furnace again and obtains bamboo charcoal; Powder crushing process.
The preparation method of tea juice is: (1), first witch hazel and tealeaves are cleaned, pulverize, wherein, tealeaves is that mass ratio is the ripe tea of Pu'er tea and the white tea that 1:1 mixes; Press the weight ratio of 1:4 and mix witch hazel and tealeaves, add in the deionized water and fully soaked 2 hours, then pour in the countercurrent extraction machine and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in the coarse filtration liquid, obtain preliminary filtered fluid;
(2), preliminary filtered fluid is carried out ultra-filtration filters, again ultrafiltration is seen through liquid and concentrate with reverse osmosis membrane at 20 ℃, obtain the first concentrate of solid contents 5%; Half of getting the first concentrate be at 40 ℃ of Vacuum Concentrations, obtains solid contents and be the second concentrate of 30%; Remaining the first concentrate and the second concentrate are mixed to get tea juice.
Edible bamboo charcoal paste powder preparation: take by weighing by weight and pulverize 50 parts of gained particle diameter 800-1000 purpose bamboo charcoal powder, 18 parts of millet powder, 1 part of peppermint oil, 4 parts in rhizome of chuanxiong powder, 45 parts in tea juice and mix with steps A gained decoction liquor, then carrying out microwave vacuum processes, send in the microwave vacuum tank after all substances are mixed, then vacuumize to process to vacuum and be-0.07Pa; Carry out microwave treatment, microwave frequency is 300MHz again, and microwave treatment time is 0.6～0.8min.After carrying out the microwave vacuum processing, material is further made the pill that diameter is 1-2mm.
After testing, properties of product such as content of beary metal and persticide residue all reach state health standards.Product of the present invention is direct-edible, not only brings into play the characteristics such as toxin expelling of charcoal, and presents the nutrition and health care performance of each additive.
Embodiment two
The preparation of decoction liquor: take by weighing by weight 10 parts of oatmeals, 5 parts of Semen sesami nigrums, 10 parts of soybean, 6 parts of bletillas, 5 parts of angelica powders, get described oatmeal, Semen sesami nigrum and soybean, add 5 times of decoctings and boil 5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain the first decocting liquid of solid contents 20%; Get described bletilla and angelica powder, add 2 times of decoctings and boil 7h, filter, concentrate with reverse osmosis membrane, obtain the second decocting liquid of solid contents 40%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor.
The preparation method of bamboo charcoal powder is: the soil sample to the bamboo wood Proterozoic detects, and requiring lead, arsenic, mercury content is zero; Bamboo wood is experienced drying, pre-charing, charing, calcining and cooling successively, control combustion is warming up to 720-750 ℃ and be incubated 60-80min with the speed of 8-15 ℃/min, and then be warming up to 1300-1500 ℃ and be incubated 6-8h with the speed of 10-15 ℃/min, then the speed with 23-25 ℃/min is cooled to 380-400 ℃, cools to room temperature with the furnace again and obtains bamboo charcoal; Powder crushing process.
The preparation method of tea juice is: (1), first witch hazel and tealeaves are cleaned, pulverize, wherein, tealeaves is the ripe tea of Pu'er tea and the white tea that 1:2 mixes; Press the weight ratio of 1:9 and mix witch hazel and tealeaves, add in the deionized water and fully soaked 2.5 hours, then pour in the countercurrent extraction machine and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in the coarse filtration liquid, obtain preliminary filtered fluid;
(2), preliminary filtered fluid is carried out ultra-filtration filters, again ultrafiltration is seen through liquid and concentrate with reverse osmosis membrane at 40 ℃, obtain the first concentrate of solid contents 20%; Half of getting the first concentrate be at 45 ℃ of Vacuum Concentrations, obtains solid contents and be the second concentrate of 33%; Remaining the first concentrate and the second concentrate are mixed to get tea juice.
Edible bamboo charcoal paste powder preparation: take by weighing by weight particle diameter and be 600-800 purpose bamboo charcoal powder 40-60 part, millet powder 15-18 part, peppermint oil 0.5-0.8 part, rhizome of chuanxiong powder 3-4 part, tea juice 40-45 part and mix with steps A gained decoction liquor, then carrying out microwave vacuum processes, send in the microwave vacuum tank after specifically all substances being mixed, then vacuumize process to vacuum for-0.09MPa～-0.08MPa; Carry out microwave treatment, microwave frequency is 245MHz～300MHz again, and microwave treatment time is 0.5～0.6min.After carrying out the microwave vacuum processing, material is further made the tablet that diameter is 2-4mm.
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Embodiment three
The preparation of decoction liquor: take by weighing by weight 8 parts of oatmeals, 4 parts of Semen sesami nigrums, 10 parts of soybean, 6 parts of bletillas, 5 parts of angelica powders, get described oatmeal, Semen sesami nigrum and soybean, add 5 times of decoctings and boil 5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain the first decocting liquid of solid contents 20%; Get described bletilla and angelica powder, add 1.5 times of decoctings and boil 6.5h, filter, concentrate with reverse osmosis membrane, obtain the second decocting liquid of solid contents 35%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor.
The preparation method of bamboo charcoal powder is: the soil sample to the bamboo wood Proterozoic detects, and requiring lead, arsenic, mercury content is zero; Bamboo wood is experienced drying, pre-charing, charing, calcining and cooling successively, control combustion is warming up to 720-730 ℃ and be incubated 50-60min with the speed of 10-15 ℃/min, and then be warming up to 1100-1300 ℃ and be incubated 3-6h with the speed of 10-12 ℃/min, then the speed with 20-23 ℃/min is cooled to 330-350 ℃, cools to room temperature with the furnace again and obtains bamboo charcoal; Being the Potassium Oxalate Solution 1:3-4 mixing submergence 3-5h in mass ratio of 8-10% with the bamboo charcoal that obtains and mass fraction, is neutrality with washed with de-ionized water to pH value then, drying.And then powder crushing process.
The preparation method of tea juice is: (1), first witch hazel and tealeaves are cleaned, pulverize, wherein, tealeaves is the ripe tea of Pu'er tea and the white tea that 1:1.5 mixes; Press the weight ratio of 1:5 and mix witch hazel and tealeaves, add in the deionized water and fully soaked 1.5 hours, then pour in the countercurrent extraction machine and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in the coarse filtration liquid, obtain preliminary filtered fluid; (2), preliminary filtered fluid is carried out ultra-filtration filters, again ultrafiltration is seen through liquid and concentrate with reverse osmosis membrane at 40 ℃, obtain the first concentrate of solid contents 15%; Half of getting the first concentrate be at 45 ℃ of Vacuum Concentrations, obtains solid contents and be the second concentrate of 35%; Remaining the first concentrate and the second concentrate are mixed to get tea juice.
Edible bamboo charcoal paste powder preparation: take by weighing by weight and pulverize the gained particle diameter and be 600-1100 purpose bamboo charcoal powder 40-60 part, millet powder 15-20 part, peppermint oil 0.5-1.8 part, rhizome of chuanxiong powder 3-5 part, tea juice 40-50 part and mix with steps A gained decoction liquor, then carrying out microwave vacuum processes, send in the microwave vacuum tank after specifically all substances being mixed, then vacuumize process to vacuum for-0.09MPa～-0.06MPa; Carry out microwave treatment, microwave frequency is 245MHz～400MHz again, and microwave treatment time is 0.5～1min.After carrying out the microwave vacuum processing, material is further made the pill that diameter is 1-2mm.
Embodiment four
The preparation of decoction liquor: take by weighing by weight oatmeal 5-10 part, Semen sesami nigrum 3-5 part, soybean 5-10 part, bletilla 4-6 part, angelica powder 3-5 part, get described oatmeal, Semen sesami nigrum and soybean, add 3-5 times of decocting and boil 4-5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain the first decocting liquid of solid contents 13%; Get described bletilla and angelica powder, add 1.1 times of decoctings and boil 6.8h, filter, concentrate with reverse osmosis membrane, obtain the second decocting liquid of solid contents 32%-35%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor.
The preparation method of Korean pine active carbon powder is: the soil sample to the pine Proterozoic detects, and requiring lead, arsenic, mercury content is zero; Pine is experienced drying, pre-charing, charing, calcining and cooling successively, control combustion is warming up to 900-950 ℃ and be incubated 40-60min with the speed of 5-10 ℃/min, and then be warming up to 1600-1700 ℃ and be incubated 2-8h with the speed of 5-10 ℃/min, then the speed with 18-20 ℃/min is cooled to 300-350 ℃, cools to room temperature with the furnace again; Powder crushing process.
Ensuing edible Korean pine active carbon part preparation method is with embodiment one.
Embodiment five
With embodiment four, the preparation method of different is Korean pine active carbon powder is: the soil sample to the pine Proterozoic detects, and it is zero requiring lead, arsenic, mercury content; Pine is experienced drying, pre-charing, charing, calcining and cooling successively, control combustion is warming up to 950-1000 ℃ and be incubated 60-80min with the speed of 10-15 ℃/min, and then be warming up to 1700-1800 ℃ and be incubated 2-8h with the speed of 10-15 ℃/min, then the speed with 20-25 ℃/min is cooled to 350-400 ℃, cools to room temperature with the furnace again; Powder crushing process.
Ensuing edible Korean pine active carbon part preparation method is with embodiment two.
This specific embodiment only is explanation of the invention; it is not limitation of the present invention; those skilled in the art can make the modification that does not have creative contribution to present embodiment as required after reading this specification, but as long as all are subject to the protection of Patent Law in claim scope of the present invention.
Claims (10)
1. eat the production method of powdered carbon, it is characterized in that may further comprise the steps:
The preparation of A, decoction liquor: take by weighing by weight oatmeal 5-10 part, Semen sesami nigrum 3-5 part, soybean 5-10 part, bletilla 4-6 part, angelica powder 3-5 part, get described oatmeal, Semen sesami nigrum and soybean, add 3-5 times of decocting and boil 4-5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain the first decocting liquid of solid contents 5%-20%; Get described bletilla and angelica powder, add 1-2 times of decocting and boil 6-7h, filter, concentrate with reverse osmosis membrane, obtain the second decocting liquid of solid contents 30%-40%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor;
The preparation of B, edible powdered carbon: take by weighing by weight particle diameter and be 600-1100 purpose powdered carbon 40-60 part, millet powder 15-20 part, peppermint oil 0.5-1.8 part, rhizome of chuanxiong powder 3-5 part, tea juice 40-50 part and mix with steps A gained decoction liquor, then carrying out microwave vacuum processes, send in the microwave vacuum tank after specifically all substances being mixed, then vacuumize process to vacuum for-0.09MPa～-0.06MPa; Carry out microwave treatment, microwave frequency is 245MHz～400MHz again, and microwave treatment time is 0.5～1min.
2. the production method of edible powdered carbon according to claim 1, it is characterized in that: the preparation of described decoction liquor is to get described oatmeal, Semen sesami nigrum and soybean, adds 3-5 times of decocting and boils 4-5h, filters, filtered solution is concentrated with reverse osmosis membrane, obtain the first decocting liquid of solid contents 13%; Get described bletilla and angelica powder, add 1-2 times of decocting and boil 6-7h, filter, concentrate with reverse osmosis membrane, obtain the second decocting liquid of solid contents 32-35%; Then merge the first decocting liquid and the second decocting liquid.
3. the production method of edible powdered carbon according to claim 1, it is characterized in that: described edible powdered carbon preparation takes by weighing by weight 50 parts of particle diameter 800-1000 purpose powdered carbons, 18 parts of millet powder, 1 part of peppermint oil, 4 parts in rhizome of chuanxiong powder, 45 parts in tea juice and mixes with steps A gained decoction liquor, then carries out the microwave vacuum processing.
4. the production method of edible powdered carbon according to claim 1, it is characterized in that: the preparation method of described tea juice is:
(1), first witch hazel and tealeaves are cleaned, pulverize, press the weight ratio of 1:4-9 and mix witch hazel and tealeaves, add in the deionized water fully immersion 2-3 hour, then pour in the countercurrent extraction machine and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in the coarse filtration liquid, obtain preliminary filtered fluid;
(2), preliminary filtered fluid is carried out ultra-filtration filters, again ultrafiltration is seen through liquid and concentrate with reverse osmosis membrane, obtain the first concentrate of solid contents 5%-20%; Half of getting the first concentrate carried out Vacuum Concentration, and obtaining solid contents is the second concentrate of 30%-35%; Remaining the first concentrate and the second concentrate are mixed to get tea juice.
5. the production method of each described edible powdered carbon according to claim 1-4 is characterized in that: it is to send in the microwave vacuum tank after all substances are mixed that described microwave vacuum is processed, and then vacuumizes to process to vacuum to be-0.07Pa; Carry out microwave treatment, microwave frequency is 300MHz again, and microwave treatment time is 0.5～1min.
6. the production method of each described edible powdered carbon according to claim 1-4, it is characterized in that: described powdered carbon is bamboo charcoal powder.
7. the production method of edible powdered carbon according to claim 6, it is characterized in that: the preparation method of described bamboo charcoal powder is:
(1) soil sample of bamboo wood Proterozoic is detected, requiring lead, arsenic, mercury content is zero;
(2) bamboo wood is experienced successively drying, pre-charing, charing, calcining and cooling, control combustion is warming up to 700-750 ℃ and be incubated 40-80min with the speed of 5-15 ℃/min, and then be warming up to 1000-1500 ℃ and be incubated 2-8h with the speed of 5-15 ℃/min, then the speed with 18-25 ℃/min is cooled to 300-400 ℃, cools to room temperature with the furnace again and obtains bamboo charcoal;
(3) powder crushing process.
8. the production method of edible powdered carbon according to claim 6, it is characterized in that: also comprise activation process before the described powder crushing process: the Potassium Oxalate Solution that the bamboo charcoal that obtains and mass fraction are 8-10% is 1:3-4 mixing submergence 3-5h in mass ratio, then be neutral with washed with de-ionized water to pH value, drying.
9. the production method of each described edible powdered carbon according to claim 1-4, it is characterized in that: described powdered carbon is the Korean pine active carbon powder.
10. the production method of edible powdered carbon according to claim 9, it is characterized in that: the preparation method of described Korean pine active carbon powder is:
(1) soil sample of pine Proterozoic is detected, requiring lead, arsenic, mercury content is zero;
(2) pine is experienced successively drying, pre-charing, charing, calcining and cooling, control combustion is warming up to 900-1000 ℃ and be incubated 40-80min with the speed of 5-15 ℃/min, and then be warming up to 1600-1800 ℃ and be incubated 2-8h with the speed of 5-15 ℃/min, then the speed with 18-25 ℃/min is cooled to 300-400 ℃, cools to room temperature with the furnace again;
(3) powder crushing process.
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Cited By (2)
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| CN103349251A (en) * | 2013-07-31 | 2013-10-16 | 宁夏天瑞产业集团现代农业有限公司 | Bamboo carbon crispy yam ball and manufacture method thereof |
| CN105476004A (en) * | 2015-12-03 | 2016-04-13 | 铜仁市金农绿色农业科技有限公司 | Dendrobium officinale lozenge and preparation method thereof |
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| CN103349251A (en) * | 2013-07-31 | 2013-10-16 | 宁夏天瑞产业集团现代农业有限公司 | Bamboo carbon crispy yam ball and manufacture method thereof |
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| CN105476004A (en) * | 2015-12-03 | 2016-04-13 | 铜仁市金农绿色农业科技有限公司 | Dendrobium officinale lozenge and preparation method thereof |
| CN105476004B (en) * | 2015-12-03 | 2018-05-25 | 铜仁市金农绿色农业科技有限公司 | A kind of dendrobium candidum lozenge and preparation method thereof |
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