CN102948660A - Trisaccharide crystal functional nutritional supplement - Google Patents
Trisaccharide crystal functional nutritional supplement Download PDFInfo
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- CN102948660A CN102948660A CN2012103838990A CN201210383899A CN102948660A CN 102948660 A CN102948660 A CN 102948660A CN 2012103838990 A CN2012103838990 A CN 2012103838990A CN 201210383899 A CN201210383899 A CN 201210383899A CN 102948660 A CN102948660 A CN 102948660A
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Abstract
The invention discloses a trisaccharide crystal functional nutritional supplement. A preparation method of a trisaccharide crystal comprises the following steps of: mixing tea flowers, corn stigma and pumpkin powders, grinding, screening, digesting, carrying out assisted extraction, concentrating, carrying out alcohol precipitation, carrying out ultrafiltration, decolorizing and carrying out freeze-drying. The natural resources including the tea flowers, the corn stigma and the pumpkin powders are efficiently utilized, waste is turned into wealth, the product added value is high, and the domestic blank can be filled up; three plant polysaccharides are extracted in a green, low-carbon and comprehensive way, and compared with a respective extraction way, the green, low-carbon and comprehensive way has the advantages of reducing labor and time, saving energy, being environment-friendly, lowering the cost and improving the labor productivity; microwaves and ultrasonic waves are united for assisted extraction, so that not only is the digestion time shortened, but also the polysaccharide dissolution rate and the trisaccharide product yield are increased; the trisaccharide crystal active polysaccharides are reasonable in proportion, complete in function, safe in quality, reliable in health maintaining and nourishing effects and capable of meeting the ever-increasing substance requirement of people in environment degradation; and the trisaccharide crystal can be prepared into various dosage forms such as soft capsules, dissolved medicines, oral liquid and the like, is good in selectivity and convenient to carry and drink and has very strong market competitiveness and wide development prospect.
Description
Technical field
The present invention relates generally to a kind of invigorant, relates in particular to the brilliant functional invigorant of a kind of trisaccharide.
Background technology
Tea Flower is the flower that the breeding tea tree just opens, and its total reducing sugar is up to the different difference of 20%-39%(kind), gal4 amino acid 11%-35%, alkaloid, polyphenol content are lower than tealeaves, and Vc content is first of the pollen; That the Tea Flower polysaccharide has is anti-oxidant, hypoglycemic, prevent and treat prostatitis, strengthens the functions such as immunity.The corn silk polysaccharide main component has galactolipin, glucose, arabinose, wood sugar and mannose; It has and improves immunity, serum cholesterol-lowering, the physiological function such as hypoglycemic.Pumpkin powder total reducing sugar＞18, the squash polyoses Main Ingredients and Appearance has D-glucose, D-galactolipin, L-arabinose, wood sugar and D-glucuronic acid, selenium polysaccharide; It has the BAs such as anticancer, antiviral, anti-inflammatory, anticoagulation, reducing blood lipid.The trisaccharide crystalline substance is soluble in water, is insoluble to organic solvent.
Tea Flower, corn stigma are often discarded by people in the prior art, the rare direct Instant Drinks of preliminary working that carry out, processing method is simple and crude, also there is in recent years institute to prepare its polysaccharide in the laboratory, but uses traditional extraction, alcohol deposition method, column chromatography, hyperfiltration, its complex process, cumbersome, yield is lower, though purity height volume containing the sample is little, can't carry out suitability for industrialized production.Especially not dark to the research of tea polysaccharide, corn silk polysaccharide, it is rarer to use.
Summary of the invention
The object of the invention is exactly in order to provide a kind of trisaccharide brilliant functional invigorant.
The present invention is achieved by the following technical solutions:
The brilliant functional invigorant of a kind of trisaccharide, be the edible preparation of being made by the raw material of following weight proportioning: trisaccharide is brilliant: edible adjuvant=1: 0.3-0.6;
The preparation method of described trisaccharide crystalline substance is:
(1) is that 1:1-2:1-2 mixes grinding in mass ratio with Tea Flower, corn stigma, pumpkin powder, crosses 60-70 mesh sieves;
(2) lixiviate: add first 7-8 times of temperature of above-mentioned compound and be 40-45 ℃ flooding, lixiviate 2-3 times;
(3) help and carry: use ultrasonic-leaching 12-15min, power is 25-26kHz; Under power 700-800W, microwave lixiviate 8-10 minutes gets extract again;
(4) concentrated: be that reduced pressure concentration said extracted liquid is concentrated into 45-50% of original volume with extract under 7.0-7.1 the condition at 40-50 ℃, PH, centrifugation goes out impurity, gets concentrate;
(5) alcohol is analysed: add 90-95% ethanol of 3-4 times of concentrate volumes, hold over night;
(6) ultrafiltration;
(7) decolouring: the polysaccharide solution PH that regulates after the ultrafiltration is 7.8-8, adds activated carbon decolorizing, and filter activity charcoal, filtered fluid be with distill water dialysis 23-24 hours, during constantly change distilled water;
(8) freeze drying, it is brilliant namely to get described trisaccharide.
Described edible adjuvant is edible sesame oil, stevioside, instant black tea powder or distilled water.
Advantage of the present invention is:
(1) efficiently utilize Tea Flower, corn stigma natural resources, turn waste into wealth, added value of product is high, may fill the domestic gaps;
(2) adopt green, low-carbon (LC), comprehensively extract three Plants polysaccharide, score is got indescribably the saving of labor, is saved time, energy-conserving and environment-protective, the saving cost is raised labour productivity;
(3) use microwave, ultrasonic combined helping to carry, both shortened extraction time, improved again polysaccharide dissolution rate and trisaccharide product yield;
(4) adopt hyperfiltration technique, exempt to use multiple solution, multiple device, simplification of flowsheet has guaranteed the stable state of active polysaccharide function, structure, composition, the purity of polysaccharide increases than conventional method, and this extraction separation and purification for plant polyose provides exemplary role;
(5) the brilliant active polysaccharide ratio of trisaccharide is reasonable, multiple functional, quality safety, and the health tonic effect is reliable, and the ever-increasing material requisite of deteriorated middle people conforms;
(6) the trisaccharide crystalline substance can be made into soft capsule, electuary, oral liquor and other types of formulations, and is better alternative, carries, drinks conveniently, has the very strong market competitiveness and development prospect.
The specific embodiment
Embodiment 1
The preparation method of trisaccharide crystalline substance is:
(1) Tea Flower, corn stigma, pumpkin powder are ground for 1:1:2 mixes in mass ratio, cross 60 mesh sieves; Perhaps pumpkin powder replaces to the sugarcane top powder as raw material.Tea Flower, corn stigma, sugarcane top powder are ground for 1:1:2 mixes in mass ratio, cross 60 mesh sieves.
(2) lixiviate: add first 8 times of temperature of above-mentioned compound and be 45 ℃ flooding, lixiviate 3 times;
(3) help and carry: use ultrasonic-leaching 12-15min, power is 25-26kHz; Under power 800W, microwave lixiviate 10 minutes gets extract again;
(4) concentrated: be that reduced pressure concentration said extracted liquid is concentrated into 50% of original volume with extract under 7.0 the condition at 50 ℃, PH, centrifugation goes out impurity, gets concentrate;
(5) alcohol is analysed: add 95% ethanol of 4 times of concentrate volumes, hold over night;
(6) ultrafiltration;
(7) decolouring: the polysaccharide solution PH that regulates after the ultrafiltration is 7.8-8, adds activated carbon decolorizing, and filter activity charcoal, filtered fluid be with distill water dialysis 23-24 hours, during constantly change distilled water;
(8) freeze drying, it is brilliant namely to get described trisaccharide.
The preparation of the brilliant soft capsule of trisaccharide:
Get the brilliant 600g of trisaccharide, add 180g sesame oil, 10g ethyl cellulose, emulsification is even, makes 1000 soft capsules, and the user eats each 2-3 3 times every day.
Embodiment 2:
The preparation of the brilliant electuary of trisaccharide:
Get the brilliant 400g of trisaccharide, allocate the instant black tea powder of 200g into, be processed into particle electuary with existing method, be distributed into packed electuary 1000 bags of every bag 6g, user's morning and evening every day each edible 1 time, each 1 bag.
Embodiment 3:
The preparation of the brilliant oral liquid of trisaccharide:
Get the brilliant 400g of trisaccharide, allocate 10 liters in the mixture of stevioside (trace) and distilled water into, make 1000 of the brilliant oral liquids of trisaccharide of every 10ml, the user drinks 3 every day, each 1.
Claims (2)
1. the brilliant functional invigorant of trisaccharide it is characterized in that the edible preparation of being made by the raw material of following weight proportioning: trisaccharide crystalline substance: edible adjuvant=1: 0.3-0.6;
The preparation method of described trisaccharide crystalline substance is:
(1) is that 1:1-2:1-2 mixes grinding in mass ratio with Tea Flower, corn stigma, pumpkin powder, crosses 60-70 mesh sieves;
(2) lixiviate: add first above-mentioned compound 7-8 times temperature and be 40-45 ℃ flooding, lixiviate 2-3 times;
(3) help and carry: use ultrasonic-leaching 12-15min, power is 25-26kHz; Under power 700-800W, microwave lixiviate 8-10 minutes gets extract again;
(4) concentrated: be that reduced pressure concentration said extracted liquid is concentrated into 45-50% of original volume with extract under 7.0-7.1 the condition at 40-50 ℃, PH, centrifugation goes out impurity, gets concentrate;
(5) alcohol is analysed: add 90-95% ethanol of 3-4 times of concentrate volumes, hold over night;
(6) ultrafiltration;
(7) decolouring: the polysaccharide solution PH that regulates after the ultrafiltration is 7.8-8, adds activated carbon decolorizing, and filter activity charcoal, filtered fluid be with distill water dialysis 23-24 hours, during constantly change distilled water;
(8) freeze drying, it is brilliant namely to get described trisaccharide.
2. the brilliant functional invigorant of trisaccharide according to claim 1 is characterized in that described edible adjuvant is edible sesame oil, stevioside, instant black tea powder or distilled water.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201210383899.0A CN102948660B (en) | 2012-10-11 | 2012-10-11 | Trisaccharide crystal functional nutritional supplement |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201210383899.0A CN102948660B (en) | 2012-10-11 | 2012-10-11 | Trisaccharide crystal functional nutritional supplement |
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| Publication Number | Publication Date |
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| CN102948660A true CN102948660A (en) | 2013-03-06 |
| CN102948660B CN102948660B (en) | 2015-06-17 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113662073A (en) * | 2021-09-08 | 2021-11-19 | 黑龙江省中医药科学院(黑龙江省中医医院) | Plant polysaccharide stomach-invigorating coffee |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101074269A (en) * | 2006-05-18 | 2007-11-21 | 徐华民 | Process for separating and extracting cucurbic active polysaccharide |
| CN101851297A (en) * | 2010-05-06 | 2010-10-06 | 安徽天品堂生态农业有限公司 | High-efficiency extraction process of polygahatous plysaccharides |
| CN102030834A (en) * | 2009-09-24 | 2011-04-27 | 上海新康制药厂 | Method for extracting and preparing camellia polysaccharide from camellia and application of camellia polysaccharide |
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2012
- 2012-10-11 CN CN201210383899.0A patent/CN102948660B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101074269A (en) * | 2006-05-18 | 2007-11-21 | 徐华民 | Process for separating and extracting cucurbic active polysaccharide |
| CN102030834A (en) * | 2009-09-24 | 2011-04-27 | 上海新康制药厂 | Method for extracting and preparing camellia polysaccharide from camellia and application of camellia polysaccharide |
| CN101851297A (en) * | 2010-05-06 | 2010-10-06 | 安徽天品堂生态农业有限公司 | High-efficiency extraction process of polygahatous plysaccharides |
Non-Patent Citations (1)
| Title |
|---|
| 周鸿立等: "玉米须多糖药理作用及提取纯化研究进展", 《吉林化工学院学报》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113662073A (en) * | 2021-09-08 | 2021-11-19 | 黑龙江省中医药科学院(黑龙江省中医医院) | Plant polysaccharide stomach-invigorating coffee |
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