CN102908464B - Radix tetrastigme micro mist and its preparation method and application - Google Patents
Radix tetrastigme micro mist and its preparation method and application Download PDFInfo
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Abstract
The extraction preparation method who the present invention relates to a kind of radix tetrastigme, relates in particular to a kind of radix tetrastigme micro mist and its preparation method and application. Radix tetrastigme micro mist, the preparation method of this radix tetrastigme micro mist comprises following step: 1) raw material is according to weight ratio radix tetrastigme blade 60% ~ 90%, the aerial stem of plant 8% ~ 35%, radix tetrastigme 0.5% ~ 5% ratio, by radix tetrastigme blade, the aerial stem of plant, flower, with clear water clean, after centrifugal dehydration; 2) add 5% ~ 20% the clear water that accounts for above-mentioned raw materials gross weight through filtering, disinfecting, polishing is broken, crosses 150-200 order, the tissue fibers in centrifugal removal slurries again; 3) by the radix tetrastigme slurries after centrifugal, carry out solution spray and be dried, atomization drying at 90-95 DEG C of temperature, obtains radix tetrastigme powder; 4) radix tetrastigme powder is carried out to vacuum packaging, stand-by. The invention has the advantages that: explained hereafter operation is simple, drug effect is high, active ingredient retains high.
Description
Technical field
The extraction preparation method who the present invention relates to a kind of radix tetrastigme, relates in particular to a kind of radix tetrastigme micro mist and its preparation method and application.
Background technology
Radix tetrastigme (TetrastigmahemsleyanumDielsetGilg) is vitaceae, has another name called gold thread hoist, the flat rattan of three leaves, stone mouse, little flat rattan, stone monkey, soil through ball, three leaves pair. The main place of production in Southwestern China portion and Anhui, Zhejiang, Jiangxi, Fujian, Hubei, Hunan, Guangdong, Guangxi.
Radix tetrastigme is with stem tuber and all herbal medicine, and radix tetrastigme has magical medicinal effects, has the immunity of raising, antiviral, enhancing liver function, is usually used in clinically treating hyperpyretic convulsion, and rheumatism is ached, and irregular menstruation is coughed and breathed heavily phlegm, pharyngalgia scrofula, the diseases such as carbuncle furunculosis. To pneumonia, scrofula, hepatitis, the severe infections diseases such as gastritis, cervicitis, septicemia have obvious curative effects. The diseases such as Several Kinds of Malignancy and hypertension, heart disease, diabetes, neurasthenia are all had to extensive and good therapeutic action.
Modern medicine study shows: radix tetrastigme all has good therapeutic action to most primary carcinoma, metastatic carcinoma etc., all bad reactions that chemotherapy of tumors is brought, as low in appetite, vomiting, feel sick, epilation and leucocyte minimizing etc. all improve significantly, patients with terminal is had to alleviating pain effect, and it can also improve the immunologic function of human body effectively; And radix tetrastigme tool wide spectrum (being suitable for various solid tumors and non-patients with solid tumor takes), efficiently (can improve rapidly carcinous heating, pain, chest ascites, leucocyte decline, apocleisis, the cachexia symptom such as weak, rapid-action, clinical total effective rate is high), nontoxic (is pure natural plant extract, without any side effects through testing), have no drug resistance (can be comprehensive, the inhibition tumour of too many levels, many target spots, completely different from the CDCC of chemotherapeutics, the not anti-medicine situation of clinical application occurs).
Chinese invention patent (application number: 200810120750.7 applyings date: 2008-09-11) disclose a kind of from radix tetrastigme the technique of high efficiency extraction flavone compound. Its technological process is: raw material radix tetrastigme, air-dry, chopping, adds water to extract in ultrasonic extractor, and extract is concentrated into certain volume, then carries out adsorption bleaching with active carbon. Then utilize cavitation suspension extraction separator, first be extracted with ethyl acetate, reclaim ethyl acetate, by aqueous solution part chloroform extraction, reclaim chloroform, by aqueous solution partial concentration to without organic reagent taste, by macroporous absorbent resin, water and 50% ethanol elution successively, collects 50% ethanol eluate, reclaim solvent to dry, obtain radix tetrastigme extract.
At present, radix tetrastigme plantation generally at least needs more than 4 years could gather in the crops, and the exploitation of radix tetrastigme product mainly concentrates on underground medicinal rhizome part, a large amount of radix tetrastigme leaf, the exploitation of stem on the ground after how the Cultivate administration phase of 4 years increases grower's income and excavate. Research finds, radix tetrastigme leaf, stem, spends and has equally good medicinal efficacy, contains abundant radix tetrastigme flavones, gallic acid, Kaempferol composition, and just pharmaceutical ingredient content is about 70% left and right of underground medicinal part. But almost 100% radix tetrastigme leaf, stem, flower etc. are all discarded on planting base or mountain, do not utilize, cause the great wasting of resources.
Summary of the invention
For radix tetrastigme leaf is carried out to deep processing and fine finishining, turn waste into wealth, exploitation radix tetrastigme leaf resource, increases farmers' income and meets consumers in general's demand. First object of the present invention is to provide a kind of radix tetrastigme micro mist, and second object of the present invention is to provide the preparation method of above-mentioned radix tetrastigme micro mist, and the 3rd object of the present invention is to provide the application of above-mentioned radix tetrastigme micro mist. The present invention is a kind of product taking radix tetrastigme leaf as main component, containing composition products such as abundant radix tetrastigme flavones, gallic acid, Kaempferols, there is effective inhibition tumor cell propagation, promote apoptosis of tumor cells, the antitumor action that tool is good, and nontoxic secondary work, be easy to absorb, good for health, can be used as the raw material of multiple product.
In order to realize first above-mentioned object, the present invention has adopted following technical scheme:
Radix tetrastigme micro mist, the preparation method of this radix tetrastigme micro mist comprises following step:
1) raw material is according to weight ratio radix tetrastigme blade 60% ~ 90%, the aerial stem of plant 8% ~ 35%, radix tetrastigme 0.5% ~ 5% ratio, by radix tetrastigme blade, the aerial stem of plant, flower, with clear water clean, after centrifugal dehydration;
2) add 5% ~ 20% the clear water that accounts for above-mentioned raw materials gross weight through filtering, disinfecting, polishing is broken, crosses 150-200 order, the tissue fibers in centrifugal removal slurries again;
3) by the radix tetrastigme slurries after centrifugal, carry out solution spray and be dried, atomization drying at 90-95 DEG C of temperature, obtains radix tetrastigme powder;
4) radix tetrastigme powder is carried out to vacuum packaging, stand-by.
As preferably, above-mentioned step 1) Raw is radix tetrastigme blade 70% ~ 80%, the aerial stem of plant 18% ~ 29%, radix tetrastigme 1% ~ 3%.
In order to realize second above-mentioned object, the present invention has adopted following technical scheme:
The preparation method of radix tetrastigme micro mist, this preparation method comprises following step:
1) raw material is according to weight ratio radix tetrastigme blade 60% ~ 90%, the aerial stem of plant 8% ~ 35%, radix tetrastigme 0.5% ~ 5% ratio, by radix tetrastigme blade, the aerial stem of plant, flower, with clear water clean, after centrifugal dehydration;
2) add 5% ~ 20% the clear water that accounts for above-mentioned raw materials gross weight through filtering, disinfecting, polishing is broken, crosses 150-200 order, the tissue fibers in centrifugal removal slurries again;
3) by the radix tetrastigme slurries after centrifugal, carry out solution spray and be dried, atomization drying at 90-95 DEG C of temperature, obtains radix tetrastigme powder;
4) radix tetrastigme powder is carried out to vacuum packaging, stand-by.
As preferably, above-mentioned step 1) Raw is radix tetrastigme blade 70% ~ 80%, the aerial stem of plant 18% ~ 29%, radix tetrastigme 1% ~ 3%.
As preferably, above-mentioned step 2) in the addition of clear water be radix tetrastigme blade gross weight 8% ~ 12%.
In order to realize the 3rd above-mentioned object, the present invention has adopted following technical scheme:
The fabricated product of radix tetrastigme micro mist, this fabricated product can be instant tea, buccal tablet, food additives, health products or medicine.
The present invention is owing to having adopted above-mentioned technical scheme, this explained hereafter operation is simple, drug effect is high, active ingredient retains high, the radix tetrastigme micro mist making is a kind of product taking radix tetrastigme leaf as main component, containing composition products such as abundant radix tetrastigme flavones, gallic acid, Kaempferols, has effective inhibition tumor cell propagation, promote apoptosis of tumor cells, the antitumor action that tool is good, and nontoxic secondary work, be easy to absorb, good for health, can be used as the raw material of multiple product.
Detailed description of the invention
Below in conjunction with the specific embodiment of the present invention is made a detailed explanation.
Radix tetrastigme micro mist, the preparation method of this radix tetrastigme micro mist comprises following step:
1) pluck and clean: all can pluck the whole year, fresh radix tetrastigme blade, stem, flower are picked, according to weight ratio radix tetrastigme blade (70% ~ 80%), stem (29% ~ 18%), radix tetrastigme (1% ~ 2%) ratio proportioning, then with filter, disinfected mountain spring water by radix tetrastigme blade, rattan, take dust, earth is rinsed well, then centrifugal dehydration;
2) polishing is broken: in the raw material such as the radix tetrastigme leaf through cleaning, stem, flower, add the mountain spring water that accounts for the gross weight 10%-12% such as radix tetrastigme leaf, rattan, flower through filtering, disinfecting, polish broken, rear 150-200 mesh filter screen is excessively centrifugal, filters the tissue fibers of removing wherein;
3) by radix tetrastigme slurries centrifugal, after filtering, carry out solution spray dry, atomization drying temperature is controlled at 90-95 DEG C, final radix tetrastigme powder;
4) dried radix tetrastigme powder is carried out to vacuum packaging, stand-by.
The above-mentioned radix tetrastigme micro mist that makes can be used as various radix tetrastigme processed goods (instant tea, buccal tablet, food additives, health products, medicine etc.) main raw material(s).
Claims (7)
1. radix tetrastigme micro mist, is characterized in that the preparation method of this radix tetrastigme micro mist comprises following step:
1) raw material is according to weight ratio radix tetrastigme blade 60% ~ 90%, the aerial stem of plant 8% ~ 35%, radix tetrastigme 0.5% ~ 5% ratio, by radix tetrastigme blade, the aerial stem of plant, flower, with clear water clean, after centrifugal dehydration;
2) add 5% ~ 20% the clear water that accounts for above-mentioned raw materials gross weight through filtering, disinfecting, polishing is broken, crosses 150-200 order, the tissue fibers in centrifugal removal slurries again;
3) by the radix tetrastigme slurries after centrifugal, carry out solution spray and be dried, atomization drying at 90-95 DEG C of temperature, obtains radix tetrastigme powder;
4) radix tetrastigme powder is carried out to vacuum packaging, stand-by.
2. radix tetrastigme micro mist according to claim 1, is characterized in that step 1) Raw is radix tetrastigme blade 70% ~ 80%, the aerial stem of plant 18% ~ 29%, radix tetrastigme 1% ~ 3%.
3. the preparation method of radix tetrastigme micro mist, is characterized in that this preparation method comprises following step:
1) raw material is according to weight ratio radix tetrastigme blade 60% ~ 90%, the aerial stem of plant 8% ~ 35%, radix tetrastigme 0.5% ~ 5% ratio, by radix tetrastigme blade, the aerial stem of plant, flower, with clear water clean, after centrifugal dehydration;
2) add 5% ~ 20% the clear water that accounts for above-mentioned raw materials gross weight through filtering, disinfecting, polishing is broken, crosses 150-200 order, the tissue fibers in centrifugal removal slurries again;
3) by the radix tetrastigme slurries after centrifugal, carry out solution spray and be dried, atomization drying at 90-95 DEG C of temperature, obtains radix tetrastigme powder;
4) radix tetrastigme powder is carried out to vacuum packaging, stand-by.
4. the preparation method of radix tetrastigme micro mist according to claim 3, is characterized in that step 1) Raw is radix tetrastigme blade 70% ~ 80%, the aerial stem of plant 18% ~ 29%, radix tetrastigme 1% ~ 3%.
5. the preparation method of radix tetrastigme micro mist according to claim 3, is characterized in that step 2) in the addition of clear water be radix tetrastigme blade gross weight 8% ~ 12%.
6. the fabricated product of the radix tetrastigme micro mist described in employing claim 1 or 2, is characterized in that: this fabricated product is food additives, health products or medicine.
7. the fabricated product of the radix tetrastigme micro mist described in employing claim 1 or 2, is characterized in that: this fabricated product is instant tea, buccal tablet.
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| CN103127314A (en) * | 2013-02-25 | 2013-06-05 | 胡馨尹 | Hemsley rockvine root tuber used for treating cancer fever |
| CN103169815A (en) * | 2013-04-09 | 2013-06-26 | 丽水市莲都区绿谷三叶青珍稀植物研究所 | Radix tetrastigme lozenge and preparation method thereof |
| CN103623036B (en) * | 2013-09-13 | 2016-02-17 | 浙江中医药大学中药饮片有限公司 | Radix tetrastigme direct oral herbal medicine and preparation method thereof |
| CN104431199A (en) * | 2014-12-22 | 2015-03-25 | 吴绍平 | Health radix tetrastigme tea and preparation method thereof |
| CN106072529A (en) * | 2016-06-18 | 2016-11-09 | 程龙凤 | A kind of processing method of Cerasus humilis Bunge Radix Apioris Fortunei (Radix Lespedezae Buergeri) nutrient tablet |
| CN109303819A (en) * | 2018-11-24 | 2019-02-05 | 郎国忠 | A kind of processing technology of radix tetrastigme |
| CN109566809A (en) * | 2018-12-24 | 2019-04-05 | 宁波市昱博药业有限公司 | A kind of preparation method of radix tetrastigme nutrition and health care jasmine tea |
| CN114470073A (en) * | 2022-03-15 | 2022-05-13 | 朱建国 | Radix tetrastigme fried carbon powder agent for treating digestive tract ulcer |
| CN114569660A (en) * | 2022-03-21 | 2022-06-03 | 朱建国 | Radix tetrastigme spray for resisting bacteria and diminishing inflammation |
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Effective date of registration: 20210916 Address after: 323000 workshop 2, floor 2, block B, building 1, No. 268, Shiniu Road, nanmingshan street, Liandu District, Lishui City, Zhejiang Province Patentee after: Zhejiang Zhongxing Biomedical Technology Co.,Ltd. Address before: 323000 no.827, Liyang street, Liandu District, Lishui City, Zhejiang Province Patentee before: LISHUI LIANDU LVGU SANYEQING RARE PLANT INSTITUTE |