CN102899732A - Anti-ultraviolet hairpiece and preparation process thereof - Google Patents
Anti-ultraviolet hairpiece and preparation process thereof Download PDFInfo
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- CN102899732A CN102899732A CN2012104394732A CN201210439473A CN102899732A CN 102899732 A CN102899732 A CN 102899732A CN 2012104394732 A CN2012104394732 A CN 2012104394732A CN 201210439473 A CN201210439473 A CN 201210439473A CN 102899732 A CN102899732 A CN 102899732A
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Abstract
The invention discloses an anti-ultraviolet hairpiece. According to the anti-ultraviolet hairpiece, after being added, an ultraviolet absorber can absorb high-energy ultraviolet rays selectively, so that the ultraviolet rays are changed into harmless energy to be released or consumed. A method for preparing the anti-ultraviolet hairpiece comprises the following steps of: the preparation of the hairpiece and perming and dyeing, wherein a method for preparing the hairpiece comprises the following steps of: adding the ultraviolet absorber into a natural polymer stock solution or a fiber-forming polymer stock solution for emulsifying; preparing primary hairpiece fibers by a solution spinning method; and immersing the hairpiece in organosilicone finishing agent emulsion, padding and baking; and performing self-crosslinking on surfaces of the hairpiece fibers to form a film or reacting with groups in the hairpiece fibers to form a film, so that anti-ultraviolet synthetic fiber hairpiece is prepared. The hairpiece is subjected to perming, sizing and dyeing by utilizing a curling sizing device.
Description
Technical field
The present invention relates to a kind of wig, be specifically related to a kind of wig and preparation technology thereof of antiultraviolet.
Background technology
In general, wig mainly is natural material and the thicker synthetic fiber preparations such as human hair, animal hair with material.The wig class that uses the natural material such as human hair to make is higher, but the problem that faces at present that there is lack of raw materials is expensive.And the wig that uses the synthetic fiber such as polyester fiber, polyamide fiber, polypropylene fibre and polyvinyl chloride fibre to make, feel, gloss and serviceability are relatively poor, belong to low-grade product.Always underway with the research that improves synthetic fiber wig class by adding different functional stuffings.
Macromolecular material because of ultraviolet effect, produces autoxidation under daylight and fluorescence, cause the degraded of polymer and deteriorated, and outward appearance and mechanical performance are degenerated.Therefore, antiultraviolet also is nowadays to be badly in need of the large problem that solves in the wig technique.
Summary of the invention
The objective of the invention is provides a kind of wig of antiultraviolet for overcoming above-mentioned the deficiencies in the prior art, optionally absorbs this high-octane ultraviolet ray after adding ultra-violet absorber, makes it to become harmless energy and discharges or consume.
For achieving the above object, the present invention adopts following technical proposals:
A kind of preparation technology of wig of antiultraviolet comprises the preparation process of wig and scalds and dyes step.
The preparation process of described wig is as follows:
Ultra-violet absorber is added to emulsification in natural polymer stoste or the fibre-forming polymer stoste, make nascent wig fiber through the solution spinning process again, then successively through silicone finish agent emulsion dipping, pad with baking process process wig fiber surface self-crosslinking film forming or with the wig fiber in the radical reaction film forming, namely prepare the synthetic fiber wig of antiultraviolet.
Described ultra-violet absorber be in salicylate class, benzophenone class, benzotriazole, group-substituted acrylonitrile, the triazines any or several.
Mass fraction at synthetic fiber wig middle-ultraviolet lamp absorbent is 10 ~ 30%, natural macromolecular material or fibre-forming polymer quality of materials Fractional domination are 95 ~ 50%, and described natural polymer stoste refers to that mass concentration is 5 ~ 30% cellulose solution, chitosan solution or sodium alginate soln; Described fibre-forming polymer stoste refers to that mass concentration is 5 ~ 30% polyacrylonitrile solution, acrylonitrile-metachloroethylene copolymer solution, polyvinyl chloride or poly-vinyl alcohol solution; Described silicone finish agent emulsion has poly-(dimethyl) siloxane microemulsion of different modified groups for more than one, and the organic silicone finishing agent mass fraction is that 1 ~ 50% described impregnation technology refers in 10 ~ 60 ℃ described silicone finish agent emulsion in the silicone finish agent emulsion, impregnation process wig 10 ~ 120min, described baking process refers under 100 ~ 150 ℃, cures and processes wig 1 ~ 30min; The diameter of described synthetic fiber wig is 20 ~ 200 μ m.
The boiling hot step of dying of described wig is as follows:
(1) utilize the curling, shaping device that wig is scalded volume and heat treatment;
(2) processing of will dyeing through the wig that step (1) is processed.
Dyeing described in the step (2) is: the wig of drying is immersed in the coloring agent, soak 45 ~ 90min, water is rinsed post-drying well.
The invention has the beneficial effects as follows, realized a kind of antiultraviolet wig preparation and scald and to dye integrated production, preparation technology is simple, production efficiency is high, is suitable for suitability for industrialized production.And, have good ultraviolet resistance, both prolonged the service life of wig, also improved the person's that wears the wig comfortableness, improved class and the quality of synthetic fiber wigs.
The specific embodiment
The present invention will be further elaborated below in conjunction with embodiment, should be noted that following explanation only is in order to explain the present invention, its content not to be limited.
Embodiment 1:
It is emulsification in 5% the cellulose solution that 10kg salicyl ester phenyl ester is added to the 100kg mass concentration, make nascent wig fiber through the solution spinning process again, then be silicone finish agent emulsion impregnation process wig 10 ~ 120min of 1% through 10 ~ 60 ℃ mass fraction, then pad and under 100 ~ 150 ℃, cure and process wig 1 ~ 30min; Wig fiber surface self-crosslinking film forming or with the wig fiber in the radical reaction film forming, namely prepare the synthetic fiber wig of antiultraviolet, diameter is 20 ~ 200 μ m.
Utilize the curling, shaping device that wig is scalded volume and heat treatment;
With the processing of dyeing of above-mentioned wig: the wig of drying is immersed in the coloring agent, soak 45 ~ 90min, water is rinsed post-drying well.
Embodiment 2:
It is emulsification in 10% the polyacrylonitrile solution that the 20kg Ultraviolet Absorber UV-P is added to the 100kg mass concentration, make nascent wig fiber through the solution spinning process again, then be silicone finish agent emulsion impregnation process wig 10 ~ 120min of 1% through 10 ~ 60 ℃ mass fraction, then pad and under 100 ~ 150 ℃, cure and process wig 1 ~ 30min; Wig fiber surface self-crosslinking film forming or with the wig fiber in the radical reaction film forming, namely prepare the synthetic fiber wig of antiultraviolet, diameter is 20 ~ 200 μ m.
Utilize the curling, shaping device that wig is scalded volume and heat treatment;
With the processing of dyeing of above-mentioned wig: the wig of drying is immersed in the coloring agent, soak 45 ~ 90min, water is rinsed post-drying well.
Embodiment 3:
It is emulsification in 8% the chitosan solution that 30kg light stabilizer GW-540 is added to the 100kg mass concentration, make nascent wig fiber through the solution spinning process again, then be silicone finish agent emulsion impregnation process wig 10 ~ 120min of 1% through 10 ~ 60 ℃ mass fraction, then pad and under 100 ~ 150 ℃, cure and process wig 1 ~ 30min; Wig fiber surface self-crosslinking film forming or with the wig fiber in the radical reaction film forming, namely prepare the synthetic fiber wig of antiultraviolet, diameter is 20 ~ 200 μ m.
Utilize the curling, shaping device that wig is scalded volume and heat treatment;
With the processing of dyeing of above-mentioned wig: the wig of drying is immersed in the coloring agent, soak 45 ~ 90min, water is rinsed post-drying well.
Embodiment 4:
It is emulsification in 6% the sodium alginate soln that 10kg ultra-violet absorber RMB is added to the 100kg mass concentration, make nascent wig fiber through the solution spinning process again, then be silicone finish agent emulsion impregnation process wig 10 ~ 120min of 1% through 10 ~ 60 ℃ mass fraction, then pad and under 100 ~ 150 ℃, cure and process wig 1 ~ 30min; Wig fiber surface self-crosslinking film forming or with the wig fiber in the radical reaction film forming, namely prepare the synthetic fiber wig of antiultraviolet, diameter is 20 ~ 200 μ m.
Utilize the curling, shaping device that wig is scalded volume and heat treatment;
With the processing of dyeing of above-mentioned wig: the wig of drying is immersed in the coloring agent, soak 45 ~ 90min, water is rinsed post-drying well.
Embodiment 5:
It is emulsification in 5% acrylonitrile-metachloroethylene copolymer solution that 20kg ultra-violet absorber UVP-327 is added to the 100kg mass concentration, make nascent wig fiber through the solution spinning process again, then be silicone finish agent emulsion impregnation process wig 10 ~ 120min of 1% through 10 ~ 60 ℃ mass fraction, then pad and under 100 ~ 150 ℃, cure and process wig 1 ~ 30min; Wig fiber surface self-crosslinking film forming or with the wig fiber in the radical reaction film forming, namely prepare the synthetic fiber wig of antiultraviolet, diameter is 20 ~ 200 μ m.
Utilize the curling, shaping device that wig is scalded volume and heat treatment;
With the processing of dyeing of above-mentioned wig: the wig of drying is immersed in the coloring agent, soak 45 ~ 90min, water is rinsed post-drying well.
Although above-mentioned the specific embodiment of the present invention is described; but be not limiting the scope of the invention; on the basis of technical scheme of the present invention, those skilled in the art do not need to pay various modifications that creative work can make or distortion still in protection scope of the present invention.
Claims (6)
1. the preparation technology of the wig of an antiultraviolet is characterized in that, comprises the preparation process of wig and scald dying step.
2. the preparation technology of the wig of a kind of antiultraviolet according to claim 1 is characterized in that, the preparation process of described wig is as follows:
Ultra-violet absorber is added to emulsification in natural polymer stoste or the fibre-forming polymer stoste, make nascent wig fiber through the solution spinning process again, then successively through silicone finish agent emulsion dipping, pad with baking process process wig fiber surface self-crosslinking film forming or with the wig fiber in the radical reaction film forming, namely prepare the synthetic fiber wig of antiultraviolet.
3. the preparation technology of the wig of a kind of antiultraviolet according to claim 2 is characterized in that, described ultra-violet absorber be in salicylate class, benzophenone class, benzotriazole, group-substituted acrylonitrile, the triazines any or several.
4. the preparation technology of the wig of a kind of antiultraviolet according to claim 2, it is characterized in that, mass fraction at synthetic fiber wig middle-ultraviolet lamp absorbent is 10 ~ 30%, natural macromolecular material or fibre-forming polymer quality of materials Fractional domination are 95 ~ 50%, and described natural polymer stoste refers to that mass concentration is 5 ~ 30% cellulose solution, chitosan solution or sodium alginate soln; Described fibre-forming polymer stoste refers to that mass concentration is 5 ~ 30% polyacrylonitrile solution, acrylonitrile-metachloroethylene copolymer solution, polyvinyl chloride or poly-vinyl alcohol solution; Described silicone finish agent emulsion has poly-(dimethyl) siloxane microemulsion of different modified groups for more than one, and the organic silicone finishing agent mass fraction is 1 ~ 50% in the silicone finish agent emulsion, described impregnation technology refers in 10 ~ 60 ℃ described silicone finish agent emulsion, impregnation process wig 10 ~ 120min, described baking process refers under 100 ~ 150 ℃, cures and processes wig 1 ~ 30min; The diameter of described synthetic fiber wig is 20 ~ 200 μ m.
5. the preparation technology of the wig of a kind of antiultraviolet according to claim 1 is characterized in that, the boiling hot step of dying of described wig is as follows:
(1) utilize the curling, shaping device that wig is scalded volume and heat treatment;
(2) processing of will dyeing through the wig that step (1) is processed.
6. the preparation technology of the wig of a kind of antiultraviolet according to claim 5 is characterized in that, dyeing described in the step (2) is: the wig of drying is immersed in the coloring agent, soak 45 ~ 90min, water is rinsed post-drying well.
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| Application Number | Priority Date | Filing Date | Title |
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| CN2012104394732A CN102899732A (en) | 2012-11-07 | 2012-11-07 | Anti-ultraviolet hairpiece and preparation process thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012104394732A CN102899732A (en) | 2012-11-07 | 2012-11-07 | Anti-ultraviolet hairpiece and preparation process thereof |
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| CN102899732A true CN102899732A (en) | 2013-01-30 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104328664A (en) * | 2014-10-30 | 2015-02-04 | 北京中纺化工股份有限公司 | Compound function fabric and preparation method thereof |
| WO2022209289A1 (en) * | 2021-03-29 | 2022-10-06 | デンカ株式会社 | Artificial hair fibers |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101563003A (en) * | 2006-12-22 | 2009-10-21 | 纳幕尔杜邦公司 | Opaque colored and white monofilaments having stability to prolonged exposure to uv light |
| WO2010134561A1 (en) * | 2009-05-22 | 2010-11-25 | 株式会社ユニヘアー | Fiber for artificial hair and method for producing same |
| CN102560736A (en) * | 2011-12-19 | 2012-07-11 | 上海瑞贝卡纤维材料科技有限公司 | Polyvinyl chloride fibers for hair and method |
| CN102605626A (en) * | 2012-01-18 | 2012-07-25 | 天津工业大学 | Preparation method of synthetic fiber wig |
-
2012
- 2012-11-07 CN CN2012104394732A patent/CN102899732A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101563003A (en) * | 2006-12-22 | 2009-10-21 | 纳幕尔杜邦公司 | Opaque colored and white monofilaments having stability to prolonged exposure to uv light |
| WO2010134561A1 (en) * | 2009-05-22 | 2010-11-25 | 株式会社ユニヘアー | Fiber for artificial hair and method for producing same |
| CN102560736A (en) * | 2011-12-19 | 2012-07-11 | 上海瑞贝卡纤维材料科技有限公司 | Polyvinyl chloride fibers for hair and method |
| CN102605626A (en) * | 2012-01-18 | 2012-07-25 | 天津工业大学 | Preparation method of synthetic fiber wig |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104328664A (en) * | 2014-10-30 | 2015-02-04 | 北京中纺化工股份有限公司 | Compound function fabric and preparation method thereof |
| CN104328664B (en) * | 2014-10-30 | 2016-02-17 | 北京中纺化工股份有限公司 | A kind of composite functional fabric and preparation method thereof |
| WO2022209289A1 (en) * | 2021-03-29 | 2022-10-06 | デンカ株式会社 | Artificial hair fibers |
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Application publication date: 20130130 |