CN102899567B - Wear-resistant width fixing machine module and manufacturing method thereof - Google Patents
Wear-resistant width fixing machine module and manufacturing method thereof Download PDFInfo
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Abstract
The invention provides a wear-resistant width fixing machine module and a manufacturing method thereof, which belongs to the technical field of width fixing machine modules. The width fixing machine module comprises, on a basis of mass percentage, 2.5 to 2.8 of C, 1.8 to 2.4 of Si, no more than 3.5 and no less than 3.2 of C + 1/3Si, 2.2 to 2.5 of Al, 0.6 to 0.8 of Cu, 0.5 to 0.8 of Ni, 0.15 to 0.30 of Mo, 0.3 to 0.6 of Mn, 0.03 to 0.05 of Ca, 0.03 to 0.05 of Ba, 0.04 to 0.07 of Mg, 0.015 to 0.035 of Zn, 0.003 to 0.006 of B, 0.02 to 0.04 of Ti, 0.08 to 0.10 of V, 0.012 to 0.030 of N, no more than 0.035 of P and no more than 0.010 of S, with the balance being Fe. According to the invention, an electric furnace is used for production, a cold-hardening resin sand mold is used for casting, and the prepared width fixing machine module has high strength, good toughness and excellent high temperature oxidation resistance, thermal fatigue resistance and abrasion resistance.
Description
Technical field
The present invention relates to a kind of Settled breadth machine module and manufacture method thereof, particularly the wear-resisting module of a kind of large lateral pressure fixed-width pressure machine and manufacture method thereof, belong to Settled breadth machine module technical field.
Background technology
Large lateral pressure fixed width (Sizing Press is called for short SP) is an on-line width adjustment technology, has become an important new technology in modern hot rolled strip production, and it is the important new installation for slab being carried out to disposable large size side pressure.The main application of fixed-width pressure machine is that wide requirement customizes thick incoming slab width according to different production boards, be specially adapted to the few and occasion of producing again the wide production board of multiple different plate of continuously cast bloom specification, can effectively reduce former material base width specifications and continuously cast bloom width adjustment time and number of times, improve continuous caster output and productivity, reduce slab tank farm stock, simplify slab yard management and rolling scaduled, be convenient to produce in time the various width specifications band steel that meet user's needs.
Due to large lateral pressure fixed-width pressure machine pat to as if the steel billet that just taken out from process furnace, its samming reaches more than 1100 DEG C, under high loading, high temperature action condition, also will be subject to the effect that high frequency is impacted.Therefore, the working condition of fixed-width pressure machine module is extremely severe.This just requires the working lining of fixed-width pressure machine module to have good high temperature resistant fatigue property, high temperature resistant impact property, high temperature wear resistant performance, and this has proposed very harsh requirement to the over-all properties of material beyond doubt.But at present, the working face of fixed-width pressure machine module usually there will be large-area crackle.When crackle is more, if change not in time module, will on working face, there is the phenomenon of " surfacial spalling ", produce and bring major hidden danger to steel rolling.
In order to improve the work-ing life of large lateral pressure fixed-width pressure machine module, Japanese Patent JP2002194478A discloses the cast iron materials for Settled breadth machine module, its composition comprises by weight percentage: C:3.2 ~ 4.2%, Si:1.0 ~ 2.5%, Mn:0.1 ~ 0.6%, below P:0.10%, below S:0.02%, below Cr:0.15%, Mg:0.04 ~ 0.10%, Fe surplus, in described structure, more than 15% area ratio crystallization graphite, graphite granule particle diameter accounting for more than 50% more than 100 μ m in described kish of separating out, but in the cast iron materials that this patent provides, contain too much inclusion, seriously affect the performance of cast iron, especially reduce plasticity and toughness, cause being prone to crackle and peeling off in module use.Chinese patent CN102168224A also discloses a kind of Settled breadth machine module, described Settled breadth machine module is processed cast molding by spheroidal graphite cast iron, it is characterized in that: described spheroidal graphite cast iron comprises the composition of following mass percent: C:3~3.9%, Si:1.5~2.2%, Mn:0.3~0.5%, P≤0.04%, S≤0.012%, Cr < 0.3%, Ni:1.5 ~ 2.3%, Mo:0.4 ~ 0.6%, rare earth element: 0.08~0.25%, Fe surplus.This invention provides in module material and contains more expensive nickel, molybdenum element, also has the deficiency of the low and poor toughness of intensity.Chinese patent CN202061891U also discloses a kind of Settled breadth machine module, and the working face of its back side module is made up of three inclined-planes and a curved surface; The first inclined-plane and horizontal angle of cut α
120 ° of <, the second inclined-plane and horizontal angle of cut α
213 ° of <, the second inclined-plane and curved surface are tangent, the 3rd inclined-plane and horizontal angle of cut α
3be 12 °, the 3rd inclined-plane and curved surface are tangent.The first slope level length: the second slope level length: curved surface horizontal length: the 3rd slope level length ratio is 12:22:23:11.Owing to having changed the shape of back side module working face, the equilibrium that makes it to be conducive to metal flow momentum is consistent, can be according to temperature difference in the width of plate slab direction of coming out of the stove, the curved surface form of adjusting module one side working face flexibly, thereby effectively control the slab lateral bending after constant width machine side pressure, both can greatly simplify production technique, can reduce again lateral bending defect, improve the quality of products.Chinese patent CN201791735U also discloses a kind of hot rolling unit slab press working module, particularly large lateral pressure constant width machine module.A kind of hot rolling unit sizing press module (1), its working face (2) comprises a plane (22) and three inclined-planes (21), (23) and (24), longitudinally on the working face of module, processes two taking mid-depth line as symmetrical V-shaped groove.Along module longitudinally on arbitrary transverse section (A-A) on working face curve by the first straight line (25), first horizontal V-shaped line (26), middle part straight line (27), second horizontal V-shaped line (28) and the 3rd straight line (29) formation.First sizing press curved surface module of the present invention strengthens the draught to metal side limit, middle part on the thickness direction of slab, and be less than centre portions near the metal lateral pressure amount of upper and lower surface, reduce slab side down tilt amount on surface up and down in side pressure process and the horizontal operation of rolling, the final generation that reduces the defects such as steel edge portion fine rule, the lumber recovery of raising belt steel product.In order to improve the work-ing life of module, (the Wang Guanghuan of Shanghai Communications University, the development of the compound module of fixed-width side press and application, Shanghai Communications University's academic dissertation, 2009) also propose to adopt Ni-Cr-Mo-W nickel-base welding rod heap to be welded in the working face of fixed-width pressure machine module, reach the object that extends module life, but adopt overlaying method to manufacture fixed-width pressure machine module, there is the poor and low deficiency of wear resistance of uniformity of hardness in overlay cladding, and overlay cladding is prone to cracking and peels off in using.
Summary of the invention
The object of the invention is the problems that exist in using for existing Settled breadth machine module, propose to adopt the low-carbon Ductile Iron that obdurability is good to manufacture Settled breadth machine module, on low-carbon Ductile Iron basis, suitably add copper, aluminium, nickel, the alloying elements such as molybdenum, improve intensity and the hardness of magnesium iron, and adopt copper-magnesium alloy nodulizing agent and the nodularization of nickel magnesium alloy nodulizing agent, improve magnesium iron nodularization effect, in addition, also add a small amount of calcium, barium, zinc, titanium, boron, vanadium, the micro alloying elements such as nitrogen, refinement magnesium iron solidified structure, improve toughness and the thermal fatigue resistance of Settled breadth machine module, promote increasing substantially of Settled breadth machine module work-ing life.
Object of the present invention can realize by following measures:
The chemical composition of Settled breadth machine module of the present invention is (massfraction %): 2.5 ~ 2.8C, 1.8 ~ 2.4Si, 3.2≤C+1/3Si≤3.5,2.2 ~ 2.5Al, 0.6 ~ 0.8Cu, 0.5 ~ 0.8Ni, 0.15 ~ 0.30Mo, 0.3 ~ 0.6Mn, 0.03 ~ 0.05Ca, 0.03 ~ 0.05Ba, 0.04 ~ 0.07Mg, 0.015 ~ 0.035Zn, 0.003 ~ 0.006B, 0.02 ~ 0.04Ti, 0.08 ~ 0.10V, 0.012 ~ 0.030N, P≤0.035, S≤0.010, Fe surplus.
Settled breadth machine module electrosmelting of the present invention, its manufacturing technology steps is:
1. by ordinary scrap steel, carburelant and the fusing of molybdenum-iron Hybrid Heating, molten iron adds ferrosilicon and ferromanganese after melting clearly, after stokehold adjusting component is qualified, temperature is risen to 1560~1580 DEG C, after adding aluminium and calsibar alloy, come out of the stove, molten iron is come out of the stove, and to add quality in process be that the come out of the stove ferrosilicon of molten iron total mass 0.70~0.85% carries out current-following inoculation processing, and wherein Silicon in Ferrosilicon mass content used is 75~80%;
2. copper-magnesium alloy nodulizing agent, nickel magnesium alloy nodulizing agent, ferro-boron, metallic zinc, VN alloy and ferrotianium are crushed to the fritter that granularity is 8~12mm, dry after 3~5h through 200~250 DEG C, be placed in casting ladle bottom, with pouring method in bag, molten iron carried out to spheroidizing and composite inoculating processing;
3. use cold setresin sand molding Settled breadth machine module, paintcast alcohol-base paint, adopts step molten iron 2. to pour into a mould, 1410~1430 DEG C of molten steel pouring temperatures;
4. pour into a mould the air cooling Settled breadth machine module of unpacking after 15~20h, spruing, cleaning undesirable root, overlap, burr;
5. Settled breadth machine module is heated to 920~950 DEG C with stove, insulation 6~8h, then air-cooled to temperature lower than after 300 DEG C, be heated to 530~580 DEG C back into stove, insulation 12~15h, then air cooling, to room temperature, is finally refined to specified dimension and precision.
The performance of alloy material is determined by metallographic structure, and certain tissue depends on chemical composition and thermal treatment process, and chemical composition of the present invention is to determine like this:
Carbon and silicon: carbon and silicon are to ensure that magnesium iron has the important element of good mechanical properties and good castability, carbon and silicone content are too low, cast iron melting difficulty, and castability is poor, carbon and silicone content are too high, Graphite in Cast Iron quantity is too much, causes the mechanical property of cast iron, and especially intensity and toughness obviously decline, according to the working conditions of Settled breadth machine module, determine that suitable carbon content is 2.5 ~ 2.8%, silicone content is 1.8 ~ 2.4%, and 3.2%≤C+1/3Si≤3.5%.
Aluminium: aluminium is mainly dissolved in matrix, obviously improves antioxidant property, hot strength and the wear resistance of matrix, and add-on is very few, raising impact on magnesium iron performance is little, and add-on is too much, easily produces oxide inclusion, damage on the contrary the performance of magnesium iron, suitable aluminium content is 2.2 ~ 2.5%.
Copper and mickel: adding copper and mickel in magnesium iron is mainly in order to improve hardening capacity, also there is positive effect to improving magnesium iron intensity, add-on is too much, when particularly nickel add-on is too much, in normalized structure, retained austenite is too much, reduce on the contrary the intensity of magnesium iron, and nickel is expensive, suitable copper content is 0.6 ~ 0.8%, and suitable nickel content is 0.5 ~ 0.8%.
Molybdenum: add appropriate molybdenum in magnesium iron, there is crystal grain thinning, improve the effect of magnesium iron obdurability, in addition, molybdenum can also reduce the temper brittleness of magnesium iron, but molybdenum add-on is too much, in magnesium iron, be prone to carbide, and the appearance of carbide can greatly damage intensity and the toughness of magnesium iron, suitable molybdenum content should be controlled at 0.15 ~ 0.30%.
Manganese: add appropriate manganese mainly to play desoxydatoin in magnesium iron, and manganese is also improved the effect of magnesium iron intensity, but manganese reduces the high temperature oxidation resistance of magnesium iron, suitable manganese content should be controlled at 0.3 ~ 0.6%.
Calcium and barium: the Main Function that adds calcium and barium in magnesium iron is deoxidation, desulfurization, in addition, calcium and barium are also improved the effect of inclusion morphology and distribution, promote increasing substantially of magnesium iron mechanical property and thermal fatigue property, suitable calcium add-on should be controlled at 0.03 ~ 0.05%, and suitable barium add-on should be controlled at 0.03 ~ 0.05%.
Magnesium: it is to promote spheroidization of graphite that magnesium adds the Main Function of molten iron, but magnesium is to promote whitening element, and add-on is too much, is prone to the carbide of fragility in cast iron, intensity and the toughness of infringement magnesium iron, suitable magnesium add-on should be controlled at 0.04 ~ 0.07%.
Boron: boron solid solution, in matrix, obviously improves matrix hardening capacity, still, boron add-on is too much, is prone to the Fe of fragility in magnesium iron
3(B, C) carbon-boron compound, causes magnesium iron mechanical property significantly to reduce, and suitable boron add-on should be controlled at 0.003 ~ 0.006%.
Zinc: add appropriate zinc to there is good deoxidation, sweetening effectiveness in magnesium iron, zinc reduces molten iron condensate depression in addition, promote the effect of magnesium iron solidified structure refinement, be conducive to increasing substantially of magnesium iron performance, add-on is too much, in magnesium iron, be prone to the carbide of fragility, be unfavorable on the contrary the improvement of magnesium iron performance, suitable zinc add-on should be controlled at 0.015 ~ 0.035%.
Titanium, vanadium, nitrogen: add appropriate titanium in magnesium iron, vanadium, nitrogen, mainly in order to form dystectic TiN, VN particle, these refractory grain, can play external nucleation, promote that magnesium iron solidifies refinement, cause the intensity of Settled breadth machine module and toughness and thermal fatigue property and wear resistance obviously to improve, but titanium, vanadium, nitrogen add-on is too much, dystectic TiN, the easy alligatoring of VN particle, reduce on the contrary the performance of Settled breadth machine module, suitable vanadium add-on should be controlled at 0.08 ~ 0.10%, suitable titanium add-on should be controlled at 0.02 ~ 0.04%, suitable nitrogen add-on should be controlled at 0.012 ~ 0.030%.
Sulphur and phosphorus: sulphur and phosphorus are inevitable trace impurities in molten iron, the performance of grievous injury magnesium iron, should strictly control its residual quantity, in order to obtain high performance Settled breadth machine module, its sulphur content is limited in below 0.010%, its phosphorus content is limited in below 0.035%.
In addition, magnesium iron of the present invention, in nodularization process, adopts copper-magnesium alloy nodulizing agent and nickel magnesium alloy nodulizing agent to carry out nodularization, has overcome the deficiency of common pure magnesium nodularization poor stability and common magnesium-rare earth nodularization weak effect, make magnesium iron stable performance, be conducive to the safe handling of Settled breadth machine module.
Effect of the present invention:
(1) Settled breadth machine module of manufacturing with the present invention, production technique is easy, and in metallographic structure, the nodularization rate of graphite is greater than 95%.
(2) the Settled breadth machine module inclusion of manufacturing with the present invention is few, and inclusion total amount is down to below 0.45%.
(3) the Settled breadth machine module solidified structure of manufacturing with the present invention is tiny, has high strength and high tenacity, and wherein tensile strength is greater than 750MPa, and yield strength is greater than 450MPa, and unit elongation is greater than 4.0%, ballistic work (α
kV) being greater than 5J, hardness reaches 260~280HB.
(4) have fabulous resistance to high temperature oxidation and thermal fatigue resistance with the Settled breadth machine module of manufacture of the present invention, also have good wear resistance, for hot rolling constant width machine, its each steel transportation amount exceedes 100,000 tons, and repairs cutting output at every turn and be less than 16mm.
Embodiment
Below in conjunction with embodiment, the invention will be further described:
Embodiment 1:
Adopt 5 tons of line frequency furnace melting Settled breadth machine module materials, the manufacturing technology steps of Settled breadth machine module is:
1. by ordinary scrap steel, carburelant and the fusing of molybdenum-iron Hybrid Heating, molten iron adds ferrosilicon and ferromanganese after melting clearly, after stokehold adjusting component is qualified, temperature is risen to 1562 DEG C, after adding aluminium and calsibar alloy, come out of the stove, molten iron is come out of the stove, and to add quality in process be that the ferrosilicon that the siliceous quality of molten iron total mass 0.70% is 79.3% of coming out of the stove carries out current-following inoculation processing.
2. copper-magnesium alloy nodulizing agent, nickel magnesium alloy nodulizing agent, ferro-boron, metallic zinc, VN alloy and ferrotianium are crushed to the fritter that granularity is 8~12mm, dry after 5h through 200 DEG C, be placed in casting ladle bottom, with pouring method in bag, molten iron carried out to spheroidizing and composite inoculating processing.
3. use cold setresin sand molding Settled breadth machine module, paintcast alcohol-base paint, adopts step molten iron 2. to pour into a mould, 1412 DEG C of molten steel pouring temperatures;
4. pour into a mould the air cooling Settled breadth machine module of unpacking after 20h, spruing, cleaning undesirable root, overlap, burr;
5. Settled breadth machine module is heated to 920 DEG C with stove, and insulation 8h is then air-cooled during to 280 DEG C of temperature, is heated to 580 DEG C back into stove, insulation 15h, and then air cooling, to room temperature, is finally refined to specified dimension and precision.The composition of Settled breadth machine module is in table 1, and the performance of Settled breadth machine module is in table 2.
Embodiment 2:
Adopt 5 tons of line frequency furnace melting Settled breadth machine module materials, the manufacturing technology steps of Settled breadth machine module is:
1. by ordinary scrap steel, carburelant and the fusing of molybdenum-iron Hybrid Heating, molten iron adds ferrosilicon and ferromanganese after melting clearly, after stokehold adjusting component is qualified, temperature is risen to 1579 DEG C, after adding aluminium and calsibar alloy, come out of the stove, molten iron is come out of the stove, and to add quality in process be that the ferrosilicon that the siliceous quality of molten iron total mass 0.85% is 75.8% of coming out of the stove carries out current-following inoculation processing.
2. copper-magnesium alloy nodulizing agent, nickel magnesium alloy nodulizing agent, ferro-boron, metallic zinc, VN alloy and ferrotianium are crushed to the fritter that granularity is 8~12mm, dry after 3h through 250 DEG C, be placed in casting ladle bottom, with pouring method in bag, molten iron carried out to spheroidizing and composite inoculating processing.
3. use cold setresin sand molding Settled breadth machine module, paintcast alcohol-base paint, adopts step molten iron 2. to pour into a mould, 1428 DEG C of molten steel pouring temperatures;
4. pour into a mould the air cooling Settled breadth machine module of unpacking after 15h, spruing, cleaning undesirable root, overlap, burr;
5. Settled breadth machine module is heated to 950 DEG C with stove, and insulation 6h is then air-cooled during to 260 DEG C of temperature, is heated to 530 DEG C back into stove, insulation 15h, and then air cooling, to room temperature, is finally refined to specified dimension and precision.The composition of Settled breadth machine module is in table 1, and the performance of Settled breadth machine module is in table 2.
Embodiment 3:
Adopt 5 tons of line frequency furnace melting Settled breadth machine module materials, the manufacturing technology steps of Settled breadth machine module is:
1. by ordinary scrap steel, carburelant and the fusing of molybdenum-iron Hybrid Heating, molten iron adds ferrosilicon and ferromanganese after melting clearly, after stokehold adjusting component is qualified, temperature is risen to 1571 DEG C, after adding aluminium and calsibar alloy, come out of the stove, molten iron is come out of the stove, and to add quality in process be that the ferrosilicon that the siliceous quality of molten iron total mass 0.75% is 75.8% of coming out of the stove carries out current-following inoculation processing.
2. copper-magnesium alloy nodulizing agent, nickel magnesium alloy nodulizing agent, ferro-boron, metallic zinc, VN alloy and ferrotianium are crushed to the fritter that granularity is 8~12mm, dry after 4h through 220 DEG C, be placed in casting ladle bottom, with pouring method in bag, molten iron carried out to spheroidizing and composite inoculating processing.
3. use cold setresin sand molding Settled breadth machine module, paintcast alcohol-base paint, adopts step molten iron 2. to pour into a mould, 1419 DEG C of molten steel pouring temperatures;
4. pour into a mould the air cooling Settled breadth machine module of unpacking after 18h, spruing, cleaning undesirable root, overlap, burr;
5. Settled breadth machine module is heated to 940 DEG C with stove, and insulation 7h is then air-cooled during to 268 DEG C of temperature, is heated to 560 DEG C back into stove, insulation 14h, and then air cooling, to room temperature, is finally refined to specified dimension and precision.The composition of Settled breadth machine module is in table 1, and the performance of Settled breadth machine module is in table 2.
The composition (massfraction, %) of table 1 Settled breadth machine module
The mechanical property of table 2 Settled breadth machine module
Settled breadth machine module of the present invention has been successfully applied on hot rolling slab sizing press, because Settled breadth machine module nodularization rate of the present invention is high, inclusion is few, fine microstructures, not only hardness is high, and obdurability, high temperature oxidation resistance, thermal fatigue resistance and wear resistance are good, can be because abnormal cracks causes inefficacy in use, for hot rolling slab sizing press, its each steel transportation amount exceedes 100,000 tons, and repairs cutting output at every turn and be less than 16mm.Apply product of the present invention, can improve hot rolling slab sizing press working efficiency, alleviate labor strength, also can avoid the unstable in production process, and can economize on resources, reduce production costs, there is good economic and social benefit.
Claims (2)
1. a manufacture method for wear-resisting Settled breadth machine module, is characterized in that, the chemical composition of Settled breadth machine module is: 2.5 ~ 2.8C, 1.8 ~ 2.4Si, 3.2≤C+1/3Si≤3.5,2.2 ~ 2.5Al, 0.6 ~ 0.8Cu, 0.5 ~ 0.8Ni, 0.15 ~ 0.30Mo, 0.3 ~ 0.6Mn, 0.03 ~ 0.05Ca, 0.03 ~ 0.05Ba, 0.04 ~ 0.07Mg, 0.015 ~ 0.035Zn, 0.003 ~ 0.006B, 0.02 ~ 0.04Ti, 0.08 ~ 0.10V, 0.012 ~ 0.030N, P≤0.035, S≤0.010, Fe surplus, above-mentioned is massfraction %;
Its preparation method comprises the following steps:
1. by ordinary scrap steel, carburelant and the fusing of molybdenum-iron Hybrid Heating, molten iron adds ferrosilicon and ferromanganese after melting clearly, after stokehold adjusting component is qualified, temperature is risen to 1560~1580 DEG C, after adding aluminium and calsibar alloy, come out of the stove, molten iron is come out of the stove, and to add quality in process be that the come out of the stove ferrosilicon of molten iron total mass 0.70~0.85% carries out current-following inoculation processing, and wherein Silicon in Ferrosilicon mass content used is 75~80%;
2. copper-magnesium alloy nodulizing agent, nickel magnesium alloy nodulizing agent, ferro-boron, metallic zinc, VN alloy and ferrotianium are crushed to the fritter that granularity is 8~12mm, dry after 3~5h through 200~250 DEG C, be placed in casting ladle bottom, with pouring method in bag, molten iron carried out to spheroidizing and composite inoculating processing;
3. use cold setresin sand molding Settled breadth machine module, paintcast alcohol-base paint, adopts step molten iron 2. to pour into a mould, 1410~1430 DEG C of molten steel pouring temperatures;
4. pour into a mould the air cooling Settled breadth machine module of unpacking after 15~20h, spruing, cleaning undesirable root, overlap, burr;
5. Settled breadth machine module is heated to 920~950 DEG C with stove, insulation 6~8h, then air-cooled to temperature lower than after 300 DEG C, be heated to 530~580 DEG C back into stove, insulation 12~15h, then air cooling, to room temperature, is finally refined to specified dimension and precision.
2. the wear-resisting Settled breadth machine module of one of preparing in accordance with the method for claim 1.
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JP2002194478A (en) * | 2000-12-25 | 2002-07-10 | Kogi Corp | Cast iron material for sizing press die |
CN102168224A (en) * | 2011-05-26 | 2011-08-31 | 上海东新冶金技术工程有限公司 | Sizing press module |
CN102615108A (en) * | 2012-04-09 | 2012-08-01 | 北京工业大学 | Centrifugal casting high-speed steel composite roll and manufacture method thereof |
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JP2002194478A (en) * | 2000-12-25 | 2002-07-10 | Kogi Corp | Cast iron material for sizing press die |
CN102168224A (en) * | 2011-05-26 | 2011-08-31 | 上海东新冶金技术工程有限公司 | Sizing press module |
CN102615108A (en) * | 2012-04-09 | 2012-08-01 | 北京工业大学 | Centrifugal casting high-speed steel composite roll and manufacture method thereof |
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