CN102895129B - Composition for smoothing out wrinkles on skin and firming skin - Google Patents
Composition for smoothing out wrinkles on skin and firming skin Download PDFInfo
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- CN102895129B CN102895129B CN201210459570.8A CN201210459570A CN102895129B CN 102895129 B CN102895129 B CN 102895129B CN 201210459570 A CN201210459570 A CN 201210459570A CN 102895129 B CN102895129 B CN 102895129B
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Abstract
The invention discloses a composition for smoothing out wrinkles on the skin and firming the skin, and aims to provide a composition (SOPC-H for short) which can effectively clear away free radicals produced by the skin of a human body, improves the activity of elastic collagen in the skin, firms the skin and improves the elasticity of the skin. The composition is characterized by consisting of the following components in percentage by weight: 30-70 percent of super procyanidins and 30-70 percent of hydrolyzed hazelnut protein. The composition belongs to the technical field of skin care products.
Description
Technical field
The present invention discloses a kind of compositions (being called for short SOPC-H), specifically, is a kind of compositions of compacting for skin plain weave, belongs to technical field of skin care.
Background technology
The reason of skin aging has: (1) intrinsic factor, heredity, neuroendocrine system and dermis thickness etc.(2) extrinsic factor 1. excessive ultraviolet radiation can destroy elastic fiber and the collagen fiber of corium, make fiber occur fracture, cutis laxa, there is wrinkle.2. skin pore blocks, and affects fat secretion and exchange of moisture, causes xerosis cutis, wrinkle, acne, freckle.(3), when in vivotoxin excretion situation body, toxin expelling organ is as cisco unity malfunctions such as intestinal, kidney, lungs, toxin can not excrete out in time, will carry out toxin expelling by skin, occurs acne, skin allergy, long speckle.(4) first the nutrient in the maintenance body of the nutriture of human body and skin is to guarantee the after one's own heart supply of Liver and kidney brain lung of life-critical organ, and unnecessary nutrient offers non-vital organ again as uses such as skins.When human nutrition situation is poor, nutrient is not enough, the nutrition of skin often can not be guaranteed.If do not noted skin inherence and external maintenance, also can accelerate the aging of skin at ordinary times.
The performance of skin aging is thinning of skin, lax, and sebum secretion reduces, xerosis cutis, coarse, wrinkle, long speckle.People is to after 25 years old, and the production capacity of elastin laminin just starts to die down, and the elastin laminin in skin is just constantly passage also, and skin starts to relax, have the catabiosis such as microgroove.So the plain weave that compacts, increasing skin elasticity is one of main means that resist skin aging.
Skin care item and clean skin product are one of the article of everyday use that must use every day of modern female.Chinese women likes skin-tightening level and smooth, and most of women is the product of the wrinkle of using over, the skin that compacts.And a part of women is because of pachylosis, lax and other reasons, also can use and claim special skin care item or the skin-cleaning articles that contain medical components, safety causes anxiety.
Summary of the invention
The present invention utilizes the combination of super procyanidin (SOPC) and hydrolysis hazelnut albumen, strengthens removing the free radical that human body skin produces, and strengthens the activity of skin Elastic collagen protein, reaches the skin that compacts, and significantly increases the effect of skin elasticity.
Technical scheme of the present invention is such: the compositions that should compact for skin plain weave, consists of than the component of component following quality: the hydrolysis hazelnut albumen of the super procyanidin of 30%-70% and 30%-70%, each component sum is 100%.
The above-mentioned compositions of compacting for skin plain weave, the following quality of said composition forms than the component of component: the hydrolysis hazelnut albumen of the super procyanidin of 40%-60% and 40%-60%, each component sum is 100%.
The above-mentioned compositions of compacting for skin plain weave, described super procyanidin extracts from French malaga, is a kind of oligomer procyanidin, and structural formula is formula 1:
Formula 1
The above-mentioned compositions of compacting for skin plain weave, described hydrolysis hazelnut protein CAS is numbered 100209-45-8.
Compared with prior art, compositions provided by the invention to free radical resisting, avoids collagen protein and elasticity collagen protein in skin to come to harm by SOPC, and opposing is old and feeble, suppresses the appearance of microgroove; Synthesizing of hydrolysis hazelnut albumen stimulation collagen and elasticity collagen protein, improves the protein content in skin, keeps skin health flexible, resist skin aging, prevent loosely, improve skin elasticity, level and smooth microgroove effect is remarkable, and both scientific composition have the effect of the skin that well compacts.
The specific embodiment
Below in conjunction with the specific embodiment, technical scheme of the present invention is described in further detail, but does not form any limitation of the invention.
Embodiment 1
Take super procyanidin (SOPC) powder 10g, be placed in 250mL beaker, add 90g distilled water, stir, until dissolve completely.With middle density filter paper filtering, obtain the SOPC solution of clear, temporary standby.
Take hydrolysis hazelnut protein 10 g, be placed in 250mL beaker, add 90g distilled water, stir, until dissolve completely.With middle density filter paper filtering, obtain milky hydrolysis hazelnut protein solution, temporary standby.Wherein, hydrolysis hazelnut albumen is provided by French SOLABIA
Get SOPC solution 30g and directly mix with hydrolysis hazelnut protein solution 70g, obtain super procyanidin (SOPC)/hydrolysis hazelnut protein composition (SOPC-H) of 30%:70%, solid content is 10%.
Embodiment 2
Take super procyanidin (SOPC) powder 10g, be placed in 250mL beaker, add 90g distilled water, stir, until dissolve completely.With middle density filter paper filtering, obtain the SOPC solution of clear, temporary standby.
Take hydrolysis hazelnut protein 10 g, be placed in 250mL beaker, add 90g distilled water, stir, until dissolve completely.With middle density filter paper filtering, obtain the hydrolysis hazelnut protein solution of clear, temporary standby.
Get SOPC solution 40g and directly mix with hydrolysis hazelnut protein solution 60g, obtain super procyanidin (SOPC)/hydrolysis hazelnut protein composition (SOPC-H) of 40%:60%, solid content is 10%.
Embodiment 3
Take super procyanidin (SOPC) powder 20g, be placed in 250mL beaker.Take again hydrolysis hazelnut protein 20 g, join in same beaker.In beaker, add 60g distilled water, stir, until dissolve completely.With middle density filter paper filtering, obtain milky super procyanidin (SOPC)/hydrolysis hazelnut protein composition (SOPC-H), solid content is 10%, wherein the ratio of two kinds of materials is 50%:50%.
Embodiment 4
Take super procyanidin (SOPC) powder 10g, be placed in 250mL beaker, add 90g distilled water, stir, until dissolve completely.With middle density filter paper filtering, obtain the SOPC solution of clear, temporary standby.
Take hydrolysis hazelnut protein 10 g, be placed in 250mL beaker, add 90g distilled water, stir, until dissolve completely.With middle density filter paper filtering, obtain the hydrolysis hazelnut protein solution of clear, temporary standby.
Get SOPC solution 60g and directly mix with hydrolysis hazelnut protein solution 40g, obtain super procyanidin (SOPC)/hydrolysis hazelnut protein composition (SOPC-H) of 60%:40%, solid content is 10%.
Embodiment 5
Take super procyanidin (SOPC) powder 10g, be placed in 250mL beaker, add 90g distilled water, stir, until dissolve completely.With middle density filter paper filtering, obtain the SOPC solution of clear, temporary standby.
Take hydrolysis hazelnut protein 10 g, be placed in 250mL beaker, add 90g distilled water, stir, until dissolve completely.With middle density filter paper filtering, obtain the hydrolysis hazelnut protein solution of clear, temporary standby.
Get SOPC solution 70g and directly mix with hydrolysis hazelnut protein solution 30g, obtain super procyanidin (SOPC)/hydrolysis hazelnut protein composition (SOPC-H) of 70%:30%, solid content is 10%.
This SOPC-H can be used as the skin plain weave active matter that compacts, for preparing cream frost emulsion class skin care item.
While specifically using, room temperature adds in the SOPC-L compositions and basic emulsion of 1-5%, and emulsifying is even.
Preparation basic emulsion, fill a prescription as following table 1:
Table 1
Compound method: A heat phase is to 80-85 ℃, and B heat phase is to 80-85 ℃, and A is added to B phase, and emulsifying homogeneous is even.Under stirring, be cooled to 45 ℃, add C phase, homogenizing is even, as basic emulsion.
Principle of the present invention:
Super procyanidin is to extract and obtain material from French VITIS VINIFERA Fructus Vitis viniferae, English name is Super Oligomeric Proantho Cyanidins(SOPC), being a kind of oligomer procyanidin that has special molecular structure, is the current generally acknowledged the most effective Natural antioxidant procyanidin of removing people interior free yl OPC a kind of in the world.Super procyanidin (SOPC) is a kind of high-efficiency antioxidant agent, is the most potent free radical scavenger found so far, has very strong activity in vivo.
Hydrolysis hazelnut albumen is the hydrolysis hazelnut oligopeptide of high bioactivity and aminoacid etc., promotes horn cell breeding, promotes fibroblast breeding, promotes cell metabolism, promotes the synthetic of collagen.Use can the recombinate effect of sebum barrier of hydrolysis hazelnut albumen, promote the synthetic of epidermis sebum.
(2) select suitable hydrolysis hazelnut albumen as raw material.The hydrolysis hazelnut albumen of choice for use of the present invention is provided by French SOLABIA company, and wherein hazelnut derives from hazel tree.Hazel tree is machaka, hermaphroditism, and fruit, hazelnut or Semen coryli heterophyllae, is filbert, and shell is hard, edible.It contains abundant vitamin B1, B2, C, E, protein and carbohydrate.In every 100 grams of Semen coryli heterophyllaes, the potassium that contains 618 milligrams, the phosphorus of 354 milligrams, the calcium of 287 milligrams, the thiamine of 46 milligrams, also has the mineral such as niacin and ferrum.Hydrolysis crylin is rich in aminoacid, contracting amino acid (glutamic acid, arginine, aspartic acid and praline) and glucose, galactose etc.
Hydrolysis hazelnut protein I NCI name: hydrolysis hazelnut albumen
No. CAS: 100209-45-8
PH(potentiometry) 5.0-7.0
Dry extract (100-105 ℃, 4 hours) 55 ± 10g/L
Total nitrogen content (Kjeldahl): 4 ± 1g/L
Nitrogen content in amino (Soerensen): 0.9 ± 0.4g/L
Total glucides content (phynol method): 13 ± 4g/L
The compact mechanism of action of skin of the present invention is: super procyanidin (SOPC) can exchange an electronics with free radical, and the free radical of removing with wish has approximate oxidation-reduction potential, and in the compound of generation, electronics is stablized by delocalization.Owing to there being a plurality of phenolic hydroxyl groups on SOPC, they can be combined with living radical, generate stable compound.The snperoxiaized metal ion of SOPC chelating, participates in antioxidative synergism, by stopping free chain reaction, and Scavenger of ROS, the detrimental effect of elimination radical pair body tissue and organ.Therefore SOPC can keep the young state of skin, reduces wrinkle of skin.And the main component of hydrolysis hazelnut albumen is oligopeptide and the aminoacid of high bioactivity, there is promotion cell metabolism, accelerate the synthetic of collagen.Both are used in combination, and cooperatively interact from inside to outside, and coordinative role, reaches the significant plain weave skin effect that compacts.
Experimental example 1
Choosing 10 canthus has the volunteer of crows-feet, two one group of people, being divided into 5 groups tries out, smear containing the emulsion in embodiment 1 to 5, smear every day twice as follows, 1 Zhou Houhui produces effect, canthus microgroove obviously shoals after 2 weeks, after 4 weeks, deep layer stricture of vagina also obviously shoals, and wherein the user effect of 50%:50% solution is the most obvious.
Experimental example 2
SOPC-H improves old and feeble sign experiment
Containing the emulsion of SOPC-H2%, improve old and feeble sign experiment (SOPC quality: hydrolysis hazelnut albumen quality=1:1)
Experimental design:
42 volunteers' skin plain weave clinical trial;
2%SOPC-H emulsion and blank formula contrast;
Compositions is to use twice every day, uses continuously half face test 8 weeks;
Before experiment starts, have within three days, nurse one's health the phase in advance, after three days, do benchmark and measure;
For the wrinkle of surveying outside canthus, do the digital image analysis of silica gel pour mask; Super close-up photography is done microgroove and fold evaluation
CUTOMETER measures skin elasticity.After 8 weeks, contrast with blank formula, emulsion containing quality 2%SOPC-H (SOPC quality: hydrolysis hazelnut albumen quality=1:1) has every effect of improving, and the silica gel pour mask of wrinkle outside canthus is analyzed and shown, the formula that contains 2%SOPC-H has the effect of improving skin smooth degree.
Embodiment 3
SOPC-H emulsion is improved skin elasticity experiment
Containing 2%SOPC-H SOPC quality (: hydrolysis hazelnut albumen quality=1:1) emulsion, improve skin elasticity
5 women testers (28-35 year)
Test article: adding content is 1%SOPC-H emulsion
Test zone: the inner side of left forearm
Control zone: the inner side of right forearm
Test period: 4 week
Test article frequency of utilization: twice of every day
Test event: skin elasticity-CK-MC750 skin elasticity protos test suite PROTOS
Method of testing: use the probe of diameter 2mm to be approximately the region of 3mm with the vacuum suction diameter of 0.045MPa.The 1.5N that exerts pressure on skin that probe can continue, measures and does not use fixative.In order to keep measuring the concordance of skin, during measurement, use masterplate holder, patient turns to head to measure buccal offside, so that probe can keep vertical with buccal skin, slightly exerts oneself in order to avoid probe slides simultaneously.Attract skin within 2 seconds, then to loosen 2 seconds.So circulation 5 times while measuring the fatigability of skin, total Measuring Time is 20 seconds.Result adopts time deformation curve and area to describe.At the 0th, 1,2 and 4 week, measure the elasticity number of skin, get 5 people's average elasticity numerical value as result.Result of the test shows to improve skin elasticity and have good effect containing 2% SOPC-H emulsion, and data are as table 2:
Table 2
| Time | 0 week | 1 week | 2 weeks | 3 weeks | 4 weeks |
| Mean values | 17 | 17.8 | 18.3 | 18.7 | 18.9 |
Use separately containing 1% SOPC emulsion and improve skin elasticity containing 1% hydrolysis hazelnut protein emulsion all to produce effect, data are as table 3:
Table 3
| Time | 0 week | 1 week | 2 weeks | 3 weeks | 4 weeks |
| 1%SOPC mean values | 17 | 17.3 | 17.5 | 17.6 | 17.7 |
| 1% hydrolysis hazelnut albumen mean values | 17.1 | 17.3 | 17.5 | 17.6 | 17.7 |
Claims (5)
1. a compositions of compacting for skin plain weave, is characterized in that, said composition consists of than the component of component following quality: the hydrolysis hazelnut albumen of the super procyanidin of 30%-70% and 30%-70%, each component sum is 100%.
2. compositions of compacting for skin plain weave according to claim 1, is characterized in that, said composition consists of than the component of component following quality: the hydrolysis hazelnut albumen of the super procyanidin of 40%-60% and 40%-60%, each component sum is 100%.
3. compositions of compacting for skin plain weave according to claim 1 and 2, is characterized in that, described super procyanidin extracts from French VITIS VINIFERA Fructus Vitis viniferae, is a kind of oligomer procyanidin.
4. compositions of compacting for skin plain weave according to claim 1 and 2, is characterized in that, the structural formula of described super procyanidin is formula 1:
Formula 1.
5. compositions of compacting for skin plain weave according to claim 1 and 2, is characterized in that, described hydrolysis hazelnut protein CAS is numbered 100209-45-8.
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| CN105852124A (en) * | 2016-04-11 | 2016-08-17 | 林映津 | Preparation method of anthocyanin-containing collagen |
| CN108294999A (en) * | 2018-04-13 | 2018-07-20 | 李海珍 | A kind of composition and preparation method thereof for skin care |
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| EP1541158A1 (en) * | 2003-12-04 | 2005-06-15 | Cognis Deutschland GmbH & Co. KG | Antioxydant composition for oral or topical administration |
| EP1541040A1 (en) * | 2003-12-04 | 2005-06-15 | Cognis Iberia S.L | Composition for oral administration (VI) comprising an extract or active agents of Medicago sativa |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1541158A1 (en) * | 2003-12-04 | 2005-06-15 | Cognis Deutschland GmbH & Co. KG | Antioxydant composition for oral or topical administration |
| EP1541040A1 (en) * | 2003-12-04 | 2005-06-15 | Cognis Iberia S.L | Composition for oral administration (VI) comprising an extract or active agents of Medicago sativa |
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