CN102863217A - 一种由陶瓷先驱体制备图案化陶瓷的方法 - Google Patents
一种由陶瓷先驱体制备图案化陶瓷的方法 Download PDFInfo
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- CN102863217A CN102863217A CN2012103716599A CN201210371659A CN102863217A CN 102863217 A CN102863217 A CN 102863217A CN 2012103716599 A CN2012103716599 A CN 2012103716599A CN 201210371659 A CN201210371659 A CN 201210371659A CN 102863217 A CN102863217 A CN 102863217A
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- ceramic precursor
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- polydimethylsiloxane
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- 239000012700 ceramic precursor Substances 0.000 title claims abstract description 39
- 238000000034 method Methods 0.000 title claims abstract description 18
- 239000000919 ceramic Substances 0.000 title abstract description 14
- 239000004205 dimethyl polysiloxane Substances 0.000 claims abstract description 67
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims abstract description 67
- -1 polydimethylsiloxane Polymers 0.000 claims abstract description 22
- 238000010438 heat treatment Methods 0.000 claims abstract description 16
- 239000003999 initiator Substances 0.000 claims abstract description 10
- 238000001816 cooling Methods 0.000 claims abstract description 9
- 238000002156 mixing Methods 0.000 claims abstract description 9
- 239000007788 liquid Substances 0.000 claims abstract description 5
- 238000000059 patterning Methods 0.000 claims description 34
- 239000003795 chemical substances by application Substances 0.000 claims description 9
- 238000009413 insulation Methods 0.000 claims description 8
- 239000000203 mixture Substances 0.000 abstract description 3
- 239000000126 substance Substances 0.000 abstract description 2
- 239000003431 cross linking reagent Substances 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 238000007711 solidification Methods 0.000 abstract 1
- 230000008023 solidification Effects 0.000 abstract 1
- 229920001709 polysilazane Polymers 0.000 description 13
- 239000000243 solution Substances 0.000 description 8
- 238000003756 stirring Methods 0.000 description 8
- 238000002360 preparation method Methods 0.000 description 7
- 229920001296 polysiloxane Polymers 0.000 description 6
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 238000005260 corrosion Methods 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 238000002347 injection Methods 0.000 description 4
- 239000007924 injection Substances 0.000 description 4
- 229920003257 polycarbosilane Polymers 0.000 description 4
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 3
- 229910052802 copper Inorganic materials 0.000 description 3
- 239000010949 copper Substances 0.000 description 3
- 230000007797 corrosion Effects 0.000 description 3
- 239000012705 liquid precursor Substances 0.000 description 3
- 239000012299 nitrogen atmosphere Substances 0.000 description 3
- 238000001259 photo etching Methods 0.000 description 3
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 2
- 238000005266 casting Methods 0.000 description 2
- 238000005229 chemical vapour deposition Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 238000000206 photolithography Methods 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 239000002243 precursor Substances 0.000 description 2
- 238000000197 pyrolysis Methods 0.000 description 2
- 230000035939 shock Effects 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- VMAWODUEPLAHOE-UHFFFAOYSA-N 2,4,6,8-tetrakis(ethenyl)-2,4,6,8-tetramethyl-1,3,5,7,2,4,6,8-tetraoxatetrasilocane Chemical compound C=C[Si]1(C)O[Si](C)(C=C)O[Si](C)(C=C)O[Si](C)(C=C)O1 VMAWODUEPLAHOE-UHFFFAOYSA-N 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 238000000280 densification Methods 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- 230000003760 hair shine Effects 0.000 description 1
- 238000005459 micromachining Methods 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 238000002174 soft lithography Methods 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 238000007669 thermal treatment Methods 0.000 description 1
- 230000004304 visual acuity Effects 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
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CN201210371659.9A CN102863217B (zh) | 2012-09-27 | 2012-09-27 | 一种由陶瓷先驱体制备图案化陶瓷的方法 |
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CN201210371659.9A CN102863217B (zh) | 2012-09-27 | 2012-09-27 | 一种由陶瓷先驱体制备图案化陶瓷的方法 |
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CN102863217A true CN102863217A (zh) | 2013-01-09 |
CN102863217B CN102863217B (zh) | 2014-12-03 |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104369254A (zh) * | 2013-08-16 | 2015-02-25 | 中国科学院兰州化学物理研究所 | 一种制备三维陶瓷微器件的方法 |
CN109320248A (zh) * | 2017-07-31 | 2019-02-12 | 香港城市大学 | 用于陶瓷折纸结构四维打印的系统和方法 |
CN109970450A (zh) * | 2019-03-28 | 2019-07-05 | 天津大学 | 一种用于3d打印的光敏陶瓷液及其陶瓷件 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1999053379A1 (de) * | 1998-04-09 | 1999-10-21 | Forschungszentrum Karlsruhe Gmbh | Verfahren zur herstellung von klein- und mikroteilen aus keramik |
CN1882878A (zh) * | 2003-10-28 | 2006-12-20 | 惠普开发有限公司 | 图案化的陶瓷薄膜和其制备方法 |
CN101215156A (zh) * | 2008-01-18 | 2008-07-09 | 天津大学 | 一种硅氧碳陶瓷制品及其制备方法 |
CN102167613A (zh) * | 2011-01-11 | 2011-08-31 | 中国人民解放军国防科学技术大学 | 一种Cf/SiC复合材料有序多孔陶瓷接头的制备方法 |
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2012
- 2012-09-27 CN CN201210371659.9A patent/CN102863217B/zh active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1999053379A1 (de) * | 1998-04-09 | 1999-10-21 | Forschungszentrum Karlsruhe Gmbh | Verfahren zur herstellung von klein- und mikroteilen aus keramik |
CN1882878A (zh) * | 2003-10-28 | 2006-12-20 | 惠普开发有限公司 | 图案化的陶瓷薄膜和其制备方法 |
CN101215156A (zh) * | 2008-01-18 | 2008-07-09 | 天津大学 | 一种硅氧碳陶瓷制品及其制备方法 |
CN102167613A (zh) * | 2011-01-11 | 2011-08-31 | 中国人民解放军国防科学技术大学 | 一种Cf/SiC复合材料有序多孔陶瓷接头的制备方法 |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104369254A (zh) * | 2013-08-16 | 2015-02-25 | 中国科学院兰州化学物理研究所 | 一种制备三维陶瓷微器件的方法 |
CN109320248A (zh) * | 2017-07-31 | 2019-02-12 | 香港城市大学 | 用于陶瓷折纸结构四维打印的系统和方法 |
CN109320248B (zh) * | 2017-07-31 | 2022-05-13 | 香港城市大学 | 构造四维打印的陶瓷物体的方法 |
CN109970450A (zh) * | 2019-03-28 | 2019-07-05 | 天津大学 | 一种用于3d打印的光敏陶瓷液及其陶瓷件 |
CN109970450B (zh) * | 2019-03-28 | 2021-06-08 | 天津大学 | 一种用于3d打印的光敏陶瓷液及其陶瓷件 |
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Inventor after: Yu Yuxi Inventor after: Chen Zhaoyun Inventor after: Li Yan Inventor before: Yu Yuxi Inventor before: Chen Zhaoyun |
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Free format text: CORRECT: INVENTOR; FROM: YU YUXI CHEN ZHAOYUN TO: YU YUXI CHEN ZHAOYUN LI YAN |
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Effective date of registration: 20170711 Address after: 361000 902A and 904A, building A, industrial building, industrial zone, torch hi tech Zone (Xiangan), Fujian, Xiamen Patentee after: LVNA TECHNOLOGY Co.,Ltd. Address before: Xiamen City, Fujian Province, 361005 South Siming Road No. 422 Patentee before: Xiamen University |
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