CN102851538B - In situ synthesis TiC particle-reinforced Ti-Al-Mo-Mn alloy material and preparation method thereof - Google Patents
In situ synthesis TiC particle-reinforced Ti-Al-Mo-Mn alloy material and preparation method thereof Download PDFInfo
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- CN102851538B CN102851538B CN201210364856.8A CN201210364856A CN102851538B CN 102851538 B CN102851538 B CN 102851538B CN 201210364856 A CN201210364856 A CN 201210364856A CN 102851538 B CN102851538 B CN 102851538B
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- 239000000956 alloy Substances 0.000 title claims abstract description 81
- 238000011065 in-situ storage Methods 0.000 title abstract description 13
- 238000002360 preparation method Methods 0.000 title abstract description 11
- 230000015572 biosynthetic process Effects 0.000 title abstract description 5
- 238000003786 synthesis reaction Methods 0.000 title abstract description 5
- 229910017309 Mo—Mn Inorganic materials 0.000 title abstract 2
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims abstract description 50
- 238000005245 sintering Methods 0.000 claims abstract description 40
- 239000010936 titanium Substances 0.000 claims abstract description 34
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 30
- 239000002245 particle Substances 0.000 claims abstract description 27
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 26
- 229910052782 aluminium Inorganic materials 0.000 claims abstract description 25
- 229910052786 argon Inorganic materials 0.000 claims abstract description 25
- 239000000463 material Substances 0.000 claims abstract description 25
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims abstract description 24
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims abstract description 23
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims abstract description 20
- 238000000498 ball milling Methods 0.000 claims abstract description 17
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims abstract description 15
- 239000011572 manganese Substances 0.000 claims abstract description 15
- 229910052750 molybdenum Inorganic materials 0.000 claims abstract description 15
- 239000012535 impurity Substances 0.000 claims abstract description 11
- 229910052748 manganese Inorganic materials 0.000 claims abstract description 9
- 238000000465 moulding Methods 0.000 claims abstract description 7
- 239000000843 powder Substances 0.000 claims description 29
- 239000007789 gas Substances 0.000 claims description 28
- 238000000034 method Methods 0.000 claims description 27
- 229910052719 titanium Inorganic materials 0.000 claims description 22
- 239000004411 aluminium Substances 0.000 claims description 21
- 239000008187 granular material Substances 0.000 claims description 20
- 229910000914 Mn alloy Inorganic materials 0.000 claims description 17
- -1 titanium-aluminium-molybdenum-manganese Chemical compound 0.000 claims description 15
- 229910052760 oxygen Inorganic materials 0.000 claims description 8
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 7
- 150000001875 compounds Chemical class 0.000 claims description 7
- 239000001301 oxygen Substances 0.000 claims description 7
- 239000010439 graphite Substances 0.000 claims description 5
- 229910002804 graphite Inorganic materials 0.000 claims description 5
- 238000000227 grinding Methods 0.000 claims description 3
- 238000003825 pressing Methods 0.000 claims description 3
- 238000007873 sieving Methods 0.000 claims description 3
- 229910045601 alloy Inorganic materials 0.000 abstract description 40
- 238000005728 strengthening Methods 0.000 abstract description 22
- 239000011159 matrix material Substances 0.000 abstract description 11
- 239000006104 solid solution Substances 0.000 abstract description 3
- 238000002844 melting Methods 0.000 abstract description 2
- 230000008018 melting Effects 0.000 abstract description 2
- 239000000203 mixture Substances 0.000 abstract description 2
- 230000002457 bidirectional effect Effects 0.000 abstract 1
- 238000012216 screening Methods 0.000 abstract 1
- 238000005303 weighing Methods 0.000 abstract 1
- 229910001069 Ti alloy Inorganic materials 0.000 description 46
- 238000006243 chemical reaction Methods 0.000 description 26
- 230000000694 effects Effects 0.000 description 17
- 238000005516 engineering process Methods 0.000 description 14
- 239000011733 molybdenum Substances 0.000 description 12
- 238000004663 powder metallurgy Methods 0.000 description 10
- 229910001040 Beta-titanium Inorganic materials 0.000 description 7
- 239000000243 solution Substances 0.000 description 5
- 238000005452 bending Methods 0.000 description 4
- 229910052751 metal Inorganic materials 0.000 description 4
- 239000002184 metal Substances 0.000 description 4
- 238000005266 casting Methods 0.000 description 3
- 239000002131 composite material Substances 0.000 description 3
- 239000013078 crystal Substances 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- 238000009792 diffusion process Methods 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 229910052761 rare earth metal Inorganic materials 0.000 description 3
- 229910001404 rare earth metal oxide Inorganic materials 0.000 description 3
- 229910001182 Mo alloy Inorganic materials 0.000 description 2
- 229910000883 Ti6Al4V Inorganic materials 0.000 description 2
- 238000005275 alloying Methods 0.000 description 2
- 238000013459 approach Methods 0.000 description 2
- 125000004429 atom Chemical group 0.000 description 2
- 238000004364 calculation method Methods 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 238000000280 densification Methods 0.000 description 2
- 230000002349 favourable effect Effects 0.000 description 2
- 238000010849 ion bombardment Methods 0.000 description 2
- 230000002045 lasting effect Effects 0.000 description 2
- 150000002910 rare earth metals Chemical class 0.000 description 2
- 230000002787 reinforcement Effects 0.000 description 2
- 238000006557 surface reaction Methods 0.000 description 2
- 238000007669 thermal treatment Methods 0.000 description 2
- 229910000838 Al alloy Inorganic materials 0.000 description 1
- 229910000967 As alloy Inorganic materials 0.000 description 1
- 229910001339 C alloy Inorganic materials 0.000 description 1
- 229910000846 In alloy Inorganic materials 0.000 description 1
- UQZIWOQVLUASCR-UHFFFAOYSA-N alumane;titanium Chemical compound [AlH3].[Ti] UQZIWOQVLUASCR-UHFFFAOYSA-N 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 150000001721 carbon Chemical group 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 239000010406 cathode material Substances 0.000 description 1
- 230000008602 contraction Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- YGANSGVIUGARFR-UHFFFAOYSA-N dipotassium dioxosilane oxo(oxoalumanyloxy)alumane oxygen(2-) Chemical compound [O--].[K+].[K+].O=[Si]=O.O=[Al]O[Al]=O YGANSGVIUGARFR-UHFFFAOYSA-N 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000005242 forging Methods 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 238000001513 hot isostatic pressing Methods 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 229910052746 lanthanum Inorganic materials 0.000 description 1
- FZLIPJUXYLNCLC-UHFFFAOYSA-N lanthanum atom Chemical compound [La] FZLIPJUXYLNCLC-UHFFFAOYSA-N 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000003701 mechanical milling Methods 0.000 description 1
- 229910052627 muscovite Inorganic materials 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 238000010587 phase diagram Methods 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000001902 propagating effect Effects 0.000 description 1
- 238000007712 rapid solidification Methods 0.000 description 1
- 230000003014 reinforcing effect Effects 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 230000002269 spontaneous effect Effects 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 230000000930 thermomechanical effect Effects 0.000 description 1
- 229910052718 tin Inorganic materials 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
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CN201210364856.8A CN102851538B (en) | 2012-09-27 | 2012-09-27 | In situ synthesis TiC particle-reinforced Ti-Al-Mo-Mn alloy material and preparation method thereof |
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CN201210364856.8A CN102851538B (en) | 2012-09-27 | 2012-09-27 | In situ synthesis TiC particle-reinforced Ti-Al-Mo-Mn alloy material and preparation method thereof |
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CN102851538B true CN102851538B (en) | 2014-04-02 |
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CN109530700B (en) * | 2018-12-27 | 2021-01-05 | 江苏科技大学 | In-situ endogenous nano (TiC-Al)3Ti/Al porous composite material and preparation method thereof |
CN111451502B (en) * | 2020-04-10 | 2021-08-17 | 西北工业大学 | Partition regulation and control method for in-situ synthesized TiC-reinforced titanium-based composite material in additive manufacturing |
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2012
- 2012-09-27 CN CN201210364856.8A patent/CN102851538B/en active Active
Non-Patent Citations (8)
Title |
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E.Abey-Gautier et al..Microstrual Formation in Ti alloys:In-Situ Characterization of Phase Transformation Kinetics.《JOM》.2007,第54-58页. |
Microstrual Formation in Ti alloys:In-Situ Characterization of Phase Transformation Kinetics;E.Abey-Gautier et al.;《JOM》;20070131;第54-58页 * |
Microstructure of in-situ TiC particle reinforced titanium alloy matrix composites;Zhang Erlin et al.;《Trans. Nonferrous Met. Soc. China》;20001231;第10卷(第6期);第764-768页 * |
Zhang Erlin et al..Microstructure of in-situ TiC particle reinforced titanium alloy matrix composites.《Trans. Nonferrous Met. Soc. China》.2000,第10卷(第6期),第764-768页. |
杨滨等.熔铸-原位反应喷射沉积形成TiC/Ti-5Mo-5V-2Cr-3Al复合材料围观组织和力学性能.《北京科技大学学报》.2003,第25卷(第4期),第332-336页. |
熔铸-原位反应喷射沉积形成TiC/Ti-5Mo-5V-2Cr-3Al复合材料围观组织和力学性能;杨滨等;《北京科技大学学报》;20030831;第25卷(第4期);第332-336页 * |
空心阴极烧结原位合成TiC/Ti基复合材料的工艺研究;胡超杰;《中国优秀硕士论文全文数据库 工程科技I辑》;20110615;B020-53 * |
胡超杰.空心阴极烧结原位合成TiC/Ti基复合材料的工艺研究.《中国优秀硕士论文全文数据库 工程科技I辑》.2011,B020-53. |
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Effective date of registration: 20160406 Address after: 225511, Jiangsu, Taizhou province Jiangyan Qiaotou town industrial concentration area Patentee after: JIANGSU SHENGYANG FIRE DOOR INDUSTRY CO., LTD. Address before: 210016, No. 5, Shun Fa Road, Gaoqiao industrial district, Dongshan street, Jiangning District, Jiangsu, Nanjing Patentee before: Nanjing University of Aeronautics and Astronautics |