CN102851537B - In-situ synthesis TiC particle enhanced titanium-aluminum-molybdenum-palladium alloy material and method for preparing same - Google Patents
In-situ synthesis TiC particle enhanced titanium-aluminum-molybdenum-palladium alloy material and method for preparing same Download PDFInfo
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- CN102851537B CN102851537B CN201210364855.3A CN201210364855A CN102851537B CN 102851537 B CN102851537 B CN 102851537B CN 201210364855 A CN201210364855 A CN 201210364855A CN 102851537 B CN102851537 B CN 102851537B
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- 239000000956 alloy Substances 0.000 title claims abstract description 82
- 239000002245 particle Substances 0.000 title claims abstract description 31
- 238000000034 method Methods 0.000 title claims abstract description 30
- 238000011065 in-situ storage Methods 0.000 title abstract description 14
- 230000015572 biosynthetic process Effects 0.000 title abstract description 6
- 229910001252 Pd alloy Inorganic materials 0.000 title abstract description 5
- 238000003786 synthesis reaction Methods 0.000 title abstract description 5
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims abstract description 50
- 238000005245 sintering Methods 0.000 claims abstract description 39
- 239000010936 titanium Substances 0.000 claims abstract description 34
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 30
- 229910052782 aluminium Inorganic materials 0.000 claims abstract description 25
- 229910052786 argon Inorganic materials 0.000 claims abstract description 25
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 25
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000000463 material Substances 0.000 claims abstract description 24
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims abstract description 23
- KDLHZDBZIXYQEI-UHFFFAOYSA-N palladium Substances [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 claims abstract description 22
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims abstract description 17
- 238000000498 ball milling Methods 0.000 claims abstract description 16
- 239000012535 impurity Substances 0.000 claims abstract description 11
- 239000007789 gas Substances 0.000 claims description 28
- 239000000843 powder Substances 0.000 claims description 25
- 229910052719 titanium Inorganic materials 0.000 claims description 22
- 239000004411 aluminium Substances 0.000 claims description 21
- 239000008187 granular material Substances 0.000 claims description 20
- 229910052750 molybdenum Inorganic materials 0.000 claims description 11
- 229910052760 oxygen Inorganic materials 0.000 claims description 8
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 7
- 150000001875 compounds Chemical class 0.000 claims description 7
- 239000001301 oxygen Substances 0.000 claims description 7
- 238000000465 moulding Methods 0.000 claims description 6
- 239000010439 graphite Substances 0.000 claims description 5
- 229910002804 graphite Inorganic materials 0.000 claims description 5
- 229910052763 palladium Inorganic materials 0.000 claims description 4
- 238000000227 grinding Methods 0.000 claims description 3
- 238000003825 pressing Methods 0.000 claims description 3
- 238000007873 sieving Methods 0.000 claims description 3
- 229910045601 alloy Inorganic materials 0.000 abstract description 42
- 238000006243 chemical reaction Methods 0.000 abstract description 26
- 238000005728 strengthening Methods 0.000 abstract description 22
- 239000000203 mixture Substances 0.000 abstract description 3
- 238000002844 melting Methods 0.000 abstract description 2
- 238000005299 abrasion Methods 0.000 abstract 1
- 239000006185 dispersion Substances 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- 230000001105 regulatory effect Effects 0.000 abstract 1
- 229910001069 Ti alloy Inorganic materials 0.000 description 46
- 230000000694 effects Effects 0.000 description 15
- 238000005516 engineering process Methods 0.000 description 14
- 239000011159 matrix material Substances 0.000 description 10
- 238000004663 powder metallurgy Methods 0.000 description 10
- 239000011733 molybdenum Substances 0.000 description 9
- 238000002360 preparation method Methods 0.000 description 9
- 229910001040 Beta-titanium Inorganic materials 0.000 description 7
- 239000000243 solution Substances 0.000 description 5
- 238000005452 bending Methods 0.000 description 4
- 230000007797 corrosion Effects 0.000 description 4
- 238000005260 corrosion Methods 0.000 description 4
- 229910052751 metal Inorganic materials 0.000 description 4
- 239000002184 metal Substances 0.000 description 4
- 238000005266 casting Methods 0.000 description 3
- 239000002131 composite material Substances 0.000 description 3
- 239000013078 crystal Substances 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- 238000009792 diffusion process Methods 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 229910052761 rare earth metal Inorganic materials 0.000 description 3
- 229910001404 rare earth metal oxide Inorganic materials 0.000 description 3
- 229910000838 Al alloy Inorganic materials 0.000 description 2
- 229910000883 Ti6Al4V Inorganic materials 0.000 description 2
- 238000005275 alloying Methods 0.000 description 2
- UQZIWOQVLUASCR-UHFFFAOYSA-N alumane;titanium Chemical compound [AlH3].[Ti] UQZIWOQVLUASCR-UHFFFAOYSA-N 0.000 description 2
- 238000013459 approach Methods 0.000 description 2
- 125000004429 atom Chemical group 0.000 description 2
- 238000004364 calculation method Methods 0.000 description 2
- 238000000280 densification Methods 0.000 description 2
- 230000002349 favourable effect Effects 0.000 description 2
- 238000010849 ion bombardment Methods 0.000 description 2
- 230000002045 lasting effect Effects 0.000 description 2
- 150000002910 rare earth metals Chemical class 0.000 description 2
- 230000002787 reinforcement Effects 0.000 description 2
- 239000006104 solid solution Substances 0.000 description 2
- 238000006557 surface reaction Methods 0.000 description 2
- 238000007669 thermal treatment Methods 0.000 description 2
- 229910000967 As alloy Inorganic materials 0.000 description 1
- 229910001339 C alloy Inorganic materials 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 150000001721 carbon Chemical group 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 239000010406 cathode material Substances 0.000 description 1
- 230000008602 contraction Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- YGANSGVIUGARFR-UHFFFAOYSA-N dipotassium dioxosilane oxo(oxoalumanyloxy)alumane oxygen(2-) Chemical compound [O--].[K+].[K+].O=[Si]=O.O=[Al]O[Al]=O YGANSGVIUGARFR-UHFFFAOYSA-N 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000005242 forging Methods 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 238000001513 hot isostatic pressing Methods 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 229910052746 lanthanum Inorganic materials 0.000 description 1
- FZLIPJUXYLNCLC-UHFFFAOYSA-N lanthanum atom Chemical compound [La] FZLIPJUXYLNCLC-UHFFFAOYSA-N 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000003701 mechanical milling Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 229910052627 muscovite Inorganic materials 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 238000010587 phase diagram Methods 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000001902 propagating effect Effects 0.000 description 1
- 238000007712 rapid solidification Methods 0.000 description 1
- -1 rare earth hydride Chemical class 0.000 description 1
- 230000003014 reinforcing effect Effects 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 230000002269 spontaneous effect Effects 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 230000000930 thermomechanical effect Effects 0.000 description 1
- 229910052718 tin Inorganic materials 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
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- Powder Metallurgy (AREA)
Abstract
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CN201210364855.3A CN102851537B (en) | 2012-09-27 | 2012-09-27 | In-situ synthesis TiC particle enhanced titanium-aluminum-molybdenum-palladium alloy material and method for preparing same |
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CN201210364855.3A CN102851537B (en) | 2012-09-27 | 2012-09-27 | In-situ synthesis TiC particle enhanced titanium-aluminum-molybdenum-palladium alloy material and method for preparing same |
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CN102851537A CN102851537A (en) | 2013-01-02 |
CN102851537B true CN102851537B (en) | 2014-04-02 |
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CN109530700B (en) * | 2018-12-27 | 2021-01-05 | 江苏科技大学 | In-situ endogenous nano (TiC-Al)3Ti/Al porous composite material and preparation method thereof |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101068945A (en) * | 2004-07-22 | 2007-11-07 | Fmw合成物系统公司 | Method for manufacturing titanium alloy wire with enhanced properties |
CN101850503A (en) * | 2010-05-21 | 2010-10-06 | 哈尔滨工业大学 | Preparation method of TiC granule reinforcing Ti-Al-Sn-Zr-Mo-Si high-temperature titanium alloy composite material plate |
CN102134662A (en) * | 2011-01-10 | 2011-07-27 | 哈尔滨工业大学 | Preparation method of reticular Ti5Si3 and dispersed TiC enhanced TiAl-based composite |
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- 2012-09-27 CN CN201210364855.3A patent/CN102851537B/en active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101068945A (en) * | 2004-07-22 | 2007-11-07 | Fmw合成物系统公司 | Method for manufacturing titanium alloy wire with enhanced properties |
CN101850503A (en) * | 2010-05-21 | 2010-10-06 | 哈尔滨工业大学 | Preparation method of TiC granule reinforcing Ti-Al-Sn-Zr-Mo-Si high-temperature titanium alloy composite material plate |
CN102134662A (en) * | 2011-01-10 | 2011-07-27 | 哈尔滨工业大学 | Preparation method of reticular Ti5Si3 and dispersed TiC enhanced TiAl-based composite |
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Effective date of registration: 20171103 Address after: Suzhou Changshou City City, Jiangsu province 215500 Dong Bang Huaqiang Road No. 9 Patentee after: ChangShu Hua-De Powder Metallurgy Co., Ltd. Address before: 210016, No. 5, Shun Fa Road, Gaoqiao industrial district, Dongshan street, Jiangning District, Jiangsu, Nanjing Patentee before: Nanjing University of Aeronautics and Astronautics |