CN102838795B - Additive resin carrier for cigarette filters and preparation method thereof - Google Patents
Additive resin carrier for cigarette filters and preparation method thereof Download PDFInfo
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- CN102838795B CN102838795B CN201210260854.4A CN201210260854A CN102838795B CN 102838795 B CN102838795 B CN 102838795B CN 201210260854 A CN201210260854 A CN 201210260854A CN 102838795 B CN102838795 B CN 102838795B
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- essence
- cigarette filter
- resin carrier
- additive resin
- filter additive
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- 229920005989 resin Polymers 0.000 title claims abstract description 57
- 239000011347 resin Substances 0.000 title claims abstract description 57
- 239000000654 additive Substances 0.000 title claims abstract description 38
- 230000000996 additive effect Effects 0.000 title claims abstract description 37
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 37
- 238000002360 preparation method Methods 0.000 title abstract description 6
- 239000003094 microcapsule Substances 0.000 claims abstract description 20
- 229920000881 Modified starch Polymers 0.000 claims abstract description 17
- 239000004368 Modified starch Substances 0.000 claims abstract description 17
- 235000019426 modified starch Nutrition 0.000 claims abstract description 17
- 238000000034 method Methods 0.000 claims abstract description 5
- 238000001125 extrusion Methods 0.000 claims abstract description 4
- 238000007493 shaping process Methods 0.000 claims abstract description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 58
- 239000011259 mixed solution Substances 0.000 claims description 25
- 239000000463 material Substances 0.000 claims description 16
- URAYPUMNDPQOKB-UHFFFAOYSA-N triacetin Chemical group CC(=O)OCC(OC(C)=O)COC(C)=O URAYPUMNDPQOKB-UHFFFAOYSA-N 0.000 claims description 14
- 238000002156 mixing Methods 0.000 claims description 11
- 229920000858 Cyclodextrin Polymers 0.000 claims description 9
- 239000004902 Softening Agent Substances 0.000 claims description 8
- 229920002472 Starch Polymers 0.000 claims description 8
- 238000001914 filtration Methods 0.000 claims description 8
- 238000005469 granulation Methods 0.000 claims description 8
- 230000003179 granulation Effects 0.000 claims description 8
- 238000000926 separation method Methods 0.000 claims description 8
- 235000019698 starch Nutrition 0.000 claims description 8
- 239000008107 starch Substances 0.000 claims description 8
- 238000005406 washing Methods 0.000 claims description 8
- 150000001875 compounds Chemical class 0.000 claims description 7
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 6
- 238000005516 engineering process Methods 0.000 claims description 5
- 239000000049 pigment Substances 0.000 claims description 5
- 230000002209 hydrophobic effect Effects 0.000 claims description 4
- 238000012986 modification Methods 0.000 claims description 4
- -1 polyethylene Polymers 0.000 claims description 4
- HFHDHCJBZVLPGP-UHFFFAOYSA-N schardinger α-dextrin Chemical compound O1C(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(O)C2O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC2C(O)C(O)C1OC2CO HFHDHCJBZVLPGP-UHFFFAOYSA-N 0.000 claims description 4
- 235000011187 glycerol Nutrition 0.000 claims description 3
- 238000004898 kneading Methods 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 230000004048 modification Effects 0.000 claims description 3
- 239000000341 volatile oil Substances 0.000 claims description 3
- 229920001353 Dextrin Polymers 0.000 claims description 2
- 239000004375 Dextrin Substances 0.000 claims description 2
- 239000004698 Polyethylene Substances 0.000 claims description 2
- 239000004743 Polypropylene Substances 0.000 claims description 2
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 2
- 238000001816 cooling Methods 0.000 claims description 2
- 238000004925 denaturation Methods 0.000 claims description 2
- 230000036425 denaturation Effects 0.000 claims description 2
- 235000019425 dextrin Nutrition 0.000 claims description 2
- 230000000694 effects Effects 0.000 claims description 2
- 229920000573 polyethylene Polymers 0.000 claims description 2
- 229920001155 polypropylene Polymers 0.000 claims description 2
- 239000003205 fragrance Substances 0.000 abstract description 6
- 230000008901 benefit Effects 0.000 abstract description 4
- 239000004014 plasticizer Substances 0.000 abstract 1
- 230000000391 smoking effect Effects 0.000 abstract 1
- 238000000465 moulding Methods 0.000 description 8
- 239000006187 pill Substances 0.000 description 6
- 239000001116 FEMA 4028 Substances 0.000 description 5
- WHGYBXFWUBPSRW-FOUAGVGXSA-N beta-cyclodextrin Chemical compound OC[C@H]([C@H]([C@@H]([C@H]1O)O)O[C@H]2O[C@@H]([C@@H](O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O3)[C@H](O)[C@H]2O)CO)O[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@@H]3O[C@@H]1CO WHGYBXFWUBPSRW-FOUAGVGXSA-N 0.000 description 5
- 235000011175 beta-cyclodextrine Nutrition 0.000 description 5
- 229960004853 betadex Drugs 0.000 description 5
- 238000011068 loading method Methods 0.000 description 5
- 239000004033 plastic Substances 0.000 description 5
- 229920003023 plastic Polymers 0.000 description 5
- 241000220317 Rosa Species 0.000 description 4
- 239000000796 flavoring agent Substances 0.000 description 4
- 235000019634 flavors Nutrition 0.000 description 4
- 239000004615 ingredient Substances 0.000 description 4
- 241000208125 Nicotiana Species 0.000 description 3
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- 235000014435 Mentha Nutrition 0.000 description 2
- 241001072983 Mentha Species 0.000 description 2
- 125000002057 carboxymethyl group Chemical group [H]OC(=O)C([H])([H])[*] 0.000 description 2
- 230000000704 physical effect Effects 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- 229920000178 Acrylic resin Polymers 0.000 description 1
- 239000004925 Acrylic resin Substances 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 244000017020 Ipomoea batatas Species 0.000 description 1
- 235000002678 Ipomoea batatas Nutrition 0.000 description 1
- 235000006679 Mentha X verticillata Nutrition 0.000 description 1
- 235000002899 Mentha suaveolens Nutrition 0.000 description 1
- 235000001636 Mentha x rotundifolia Nutrition 0.000 description 1
- 235000019082 Osmanthus Nutrition 0.000 description 1
- 241000333181 Osmanthus Species 0.000 description 1
- 244000242564 Osmanthus fragrans Species 0.000 description 1
- 235000019083 Osmanthus fragrans Nutrition 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000013467 fragmentation Methods 0.000 description 1
- 238000006062 fragmentation reaction Methods 0.000 description 1
- 150000002433 hydrophilic molecules Chemical class 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 229920000915 polyvinyl chloride Polymers 0.000 description 1
- 229920001592 potato starch Polymers 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 210000000697 sensory organ Anatomy 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 229920005992 thermoplastic resin Polymers 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
Abstract
The invention provides an additive resin carrier for cigarette filters. The additive resin carrier is prepared by: subjecting 1-8% by mass of an essence microcapsule, 20-60% by mass of modified starch, 30-70% by mass of resin, 1-3% by mass of a plasticizer and 0.01-0.05% by mass of toner to an extrusion molding process. The additive resin carrier for cigarette filters provided in the invention reserves the advantages of easy shaping and rapid as well as convenient preparation of various shapes of resin, and can fully release the additive fragrance during cigarette smoking.
Description
Technical field
The invention belongs to technical field of cigarettes, specifically refer to a kind of cigarette filter additive resin carrier and preparation method thereof.
Background technology
At present, cigarette is very extensive for the additive application of flavouring, aspect cigarette flavouring benefit taste, is playing an important role.The most general spices addition manner is to add in pipe tobacco, and additive is along with the burning of pipe tobacco is burnt simultaneously, and not only flavour ingredient exists loss, and the cracking of additive and reaction likely bring new objectionable impurities to cigarette.Therefore the interpolation of flavour ingredient is carried out at the position that, tobacco worker attempts not participating in burning at filter tip etc.And in cigarette, add add with cotton thread absorption more, its addition unstable and in filter stick skewness.In addition, also having a kind of addition manner is the mode of placing pill in can visual filter tip, and in use, human consumer, by pill fragmentation, discharges its fragrance.But this dripping pill, for moisture, temperature sensitive, stores if any improper, and the phenomenon that can deform, affects attractive in appearance.The forming process of dripping pill simultaneously, dripping pill only can be circular, and shape is comparatively single, and the complicated process of preparation of dripping pill, and molding time is longer.
Adopt thermoplastic resin material can prepare quickly and easily the different handicraft product of different shape by squeeze technology for forming.But because molding resin material temperature is high, can be due to resin material surface compact for the words of spice additive carrier by resin material, cause flavour ingredient to be difficult to retain or distribute.
Summary of the invention
The object of the invention is provides a kind of cigarette filter additive resin carrier according to the deficiencies in the prior art, and this carrier not only can fashion into arbitrary shape, and can be in sucking cigarette abundant release additives fragrance.
The present invention is achieved through the following technical solutions: a kind of cigarette filter additive resin carrier, is characterized in that: resin, the softening agent of 1-3% and the toner of 0.01-0.05% of the essence microcapsule that it is is 1-8% by mass percent, the modified starch of 20-60%, 30-70% prepare according to squeeze technology for forming.
Described essence microcapsule is that to join weight by essence be to obtain ethanol essence mixed solution after 1-8 ethanol doubly, be that 1:2-8 adds in wall material by ethanol essence mixed solution and wall material according to weight ratio, bag and 1-24 hour at 20-60 ℃, then by after throw out filtering separation, with mixed solution weight 1-2 washing with alcohol dry obtaining doubly.
Preferably, described essence is one or both mixtures in natural plant essential oils, compound essence product.
Preferably, described wall material is cyclodextrin, denaturation loop dextrin, starch or modified starch.
Preferably, described modified starch is the native starch after carboxymethylation or the modification of silicane hydrophobic molecule.
Preferably, described resin is polyethylene, polypropylene, polylactic resin.
Preferably, described softening agent is glycerine triacetate or glycerine.
Preferably, described toner is natural extract pigment or synthetic edible pigment.
Most preferred, a kind of cigarette filter additive resin carrier, is characterized in that: the essence microcapsule that it is is 5% by mass percent, 30.5% modified starch, 62.47% resin, 2% softening agent and 0.03% toner prepare according to squeeze technology for forming.Described essence microcapsule is that to join weight by essence be to obtain ethanol essence mixed solution after the ethanol of 4 times, be that 1:4 adds in wall material by ethanol essence mixed solution and wall material according to weight ratio, at 40 ℃, wrap and 12 hours, then by after throw out filtering separation, with washing with alcohol dry the obtaining of 2 times of mixed solution weight.Described essence is natural plant essential oils, and described wall material is beta-cyclodextrin, and described modified starch is the native starch after carboxymethyl-modification, and described resin is polylactic resin, and described softening agent is glycerine triacetate, and described toner is natural extract pigment.
Another object of the present invention is to provide the preparation method of above-mentioned cigarette filter additive resin carrier.
One is prepared cigarette filter additive resin carrier described in claim 1, its step comprises: the essence microcapsule that is 1-8% by mass percent, the modified starch of 20-60%, the resin of 30-70%, after the softening agent of 1-3% and the mixing of the toner of 0.01-0.05% are reinforced, be heated to 70-140 ℃ and make it to be glutinous stream mode, then under the effect of pressurization, become cross section and mouthful continuum that mould shape is similar by extruded mould, carrying out cooling and shaping is vitreous state again, obtain having the cigarette filter additive resin carrier of certain geometrical shape and size goods finally by cutting.
Preferably, first modified starch and resin are carried out to heat kneading, mixing and granulation, then add other component extrusion moulding.
Cigarette filter of the present invention had both retained resin with additive resin carrier and had easily shaped, can prepare quickly and easily the advantage of different shape, simultaneously due to the Swelling Functions of modified starch in the time extruding, can make on resin, to there is the diffusion hole that can discharge fragrance, thereby overcome resin material due to surface compact, can cause flavour ingredient to be difficult to the problem that retains or distribute as additive carrier.In addition, because essence microcapsule has certain stability, there is certain thermotolerance compared with common essence, can make cigarette just scentetd fully in sucking.And because native starch is hydrophilic compounds, with resene hydrophobic compound, consistency is poor, the mixture material physicals forming is poor, therefore the present invention by hydrophobic molecule carry out part group modified after, can have good consistency with resin material, physicals is better, easier moulding.Meanwhile, because essence chance high temperature is perishable, first modified starch and resin are carried out to heat kneading, mixing and granulation, then add other component extrusion moulding.Resin carrier of the present invention is nontoxic, cost is low and biodegradable under field conditions (factors), can be made into as required the odor type and the color that need, has the advantages such as sense organ is comfortable, environmental protection.
Embodiment
By the following specific examples further illustrate the invention:
Embodiment 1
After rose compound is joined to weight and is the ethanol of 4 times, be that 1:4 adds ethanol essence mixed solution in beta-cyclodextrin according to above-mentioned ethanol essence mixed solution and beta-cyclodextrin weight ratio, at 40 ℃, wrap and 12 hours, then after filtering separation throw out, be dried and obtain essence microcapsule 1 after dry 2-48 hour by the washing with alcohol of 2 times of mixed solution weight and in the baking oven of 30-60 ℃.
It is the carboxymethyl modified W-Gum of 30.5 parts by parts by weight, with parts by weight be 62.47 parts of polylactic resin carry out heat mediate, mixing and granulation, then adding parts by weight is that the essence microcapsule 1 of 5 parts, glycerine triacetate that parts by weight are 2 parts and parts by weight are that the rose-colored toner of 0.03 part adds in plastic extruding molding machine loading hopper, select length and width to be no more than 5mm, thickness is that the rose template of 2mm is as mouth mould, 120 ℃ of temperature, under pressure 5MPa, extrude, can obtain cigarette filter additive resin carrier 1 by 15s.
Embodiment 2
After osmanthus flower fragrance is joined to weight and is the ethanol of 8 times, be that 1:8 adds ethanol essence mixed solution in cyclodextrin according to above-mentioned ethanol essence mixed solution and cyclodextrin weight ratio, at 60 ℃, wrap and 1 hour, then after filtering separation throw out, be dried and obtain essence microcapsule 2 after dry 2-48 hour by the washing with alcohol of 1.5 times of mixed solution weight and in the baking oven of 30-60 ℃.
It is the sweet potato starch of the Phosphation modification of 60 parts by parts by weight, with parts by weight be 30.99 parts of polyvinyl resins carry out heat mediate, mixing and granulation, then adding parts by weight is that the essence microcapsule 2 of 7 parts, glycerine triacetate that parts by weight are 2 parts and parts by weight are that the yellow toner of 0.01 part adds in plastic extruding molding machine loading hopper, select length and width to be no more than 5mm, thickness is the sweet osmanthus section mould plate of 2mm, at temperature 70 C, under pressure 5MPa, extrude, can obtain cigarette filter additive resin carrier 2 by 15s.
Embodiment 3
It is after the ethanol of 1 times that the mixing essence that Mint Essence is mixed with compound essence joins weight, be that 1:4 adds ethanol essence mixed solution in starch according to above-mentioned ethanol essence mixed solution and starch weight ratio, at 20 ℃, wrap and 24 hours, then after filtering separation throw out, be dried and obtain essence microcapsule 3 after dry 2-48 hour by the washing with alcohol of 1 times of mixed solution weight and in the baking oven of 30-60 ℃.
It is the W-Gum of the lactic modified of 58.98 parts by parts by weight, with parts by weight be 30 parts of acrylic resins carry out heat mediate, mixing and granulation, then adding parts by weight is that the essence microcapsule 3 of 8 parts, glycerine triacetate that parts by weight are 3 parts and parts by weight are that the green toner of 0.02 part adds in plastic extruding molding machine loading hopper, select length and width to be no more than 5mm, thickness is the mentha leave section mould plate of 2mm, 140 ℃ of temperature, under pressure 5MPa, extrude, can obtain cigarette filter additive resin carrier 3 by 15s.
Embodiment 4
After compound essence is joined to weight and is the ethanol of 4 times, be that 1:4 adds ethanol essence mixed solution in modified starch according to above-mentioned ethanol essence mixed solution and modified starch weight ratio, at 40 ℃, wrap and 12 hours, then after filtering separation throw out, be dried and obtain essence microcapsule 4 after dry 2-48 hour by the washing with alcohol of 2 times of mixed solution weight and in the baking oven of 30-60 ℃.
It is the silane-modified W-Gum of 25.95 parts by parts by weight, with parts by weight be 70 parts of polylactic resin carry out heat mediate, mixing and granulation, then adding parts by weight is that the essence microcapsule 4 of 1 part, glycerine that parts by weight are 3 parts and parts by weight are that the green toner of 0.05 part adds in plastic extruding molding machine loading hopper, select length and width to be no more than 5mm, thickness is the mentha leave section mould plate of 2mm, 120 ℃ of temperature, under pressure 5MPa, extrude, can obtain cigarette filter additive resin carrier 4 by 15s.
Embodiment 5
After rose compound is joined to weight and is the ethanol of 4 times, be that 1:2 adds ethanol essence mixed solution in beta-cyclodextrin according to above-mentioned ethanol essence mixed solution and beta-cyclodextrin weight ratio, at 20 ℃, wrap and 24 hours, then after filtering separation throw out, be dried and obtain essence microcapsule 5 after dry 2-48 hour by the washing with alcohol of 1 times of mixed solution weight and in the baking oven of 30-60 ℃.
It is the carboxymethyl modified W-Gum of 20 parts by parts by weight, with parts by weight be 69.95 parts of polylactic resin carry out heat mediate, mixing and granulation, then adding parts by weight is that the essence microcapsule 5 of 8 parts, glycerine triacetate that parts by weight are 2 parts and parts by weight are that the rose-colored toner of 0.05 part adds in plastic extruding molding machine loading hopper, select length and width to be no more than 5mm, thickness is that the rose template of 2mm is as mouth mould, 120 ℃ of temperature, under pressure 5MPa, extrude, can obtain cigarette filter additive resin carrier 5 by 15s.
This cigarette filter can discharge the fragrance of essence additive in sucking with additive resin carrier 1-5.
Claims (10)
1. a cigarette filter additive resin carrier, is characterized in that: resin, the softening agent of 1-3% and the toner of 0.01-0.05% of the essence microcapsule that it is is 1-8% by mass percent, the modified starch of 20-60%, 30-70% prepare according to squeeze technology for forming.
2. cigarette filter additive resin carrier according to claim 1, it is characterized in that: described essence microcapsule is that to join weight by essence be to obtain ethanol essence mixed solution after 1-8 ethanol doubly, weight ratio according to ethanol essence mixed solution and wall material 1:2-8 adds ethanol essence mixed solution in wall material, inclusion 1-24 hour at 20-60 ℃, then by after throw out filtering separation, with mixed solution weight 1-2 washing with alcohol dry obtaining doubly.
3. cigarette filter additive resin carrier according to claim 2, is characterized in that: described essence is one or both mixtures in natural plant essential oils, compound essence product.
4. cigarette filter additive resin carrier according to claim 2, is characterized in that: described wall material is cyclodextrin, denaturation loop dextrin, starch or modified starch.
5. cigarette filter additive resin carrier according to claim 1, is characterized in that: described modified starch is obtained after carboxymethylation or the modification of silicane hydrophobic molecule by native starch.
6. cigarette filter additive resin carrier according to claim 1, is characterized in that: described resin is polyethylene, polypropylene, polylactic resin.
7. cigarette filter additive resin carrier according to claim 1, is characterized in that: described softening agent is glycerine triacetate or glycerine.
8. cigarette filter additive resin carrier according to claim 1, is characterized in that: described toner is natural extract pigment or synthetic edible pigment.
9. prepare the method for cigarette filter additive resin carrier described in claim 1 for one kind, its step comprises: the essence microcapsule that is 1-8% by mass percent, the modified starch of 20-60%, the resin of 30-70%, after the softening agent of 1-3% and the mixing of the toner of 0.01-0.05% are reinforced, be heated to 70-140 ℃ and make it to be glutinous stream mode, then under the effect of pressurization, become cross section and mouthful continuum that mould shape is similar by extruded mould, carrying out cooling and shaping is vitreous state again, obtain having the cigarette filter additive resin carrier of certain geometrical shape and size goods finally by cutting.
10. the method for preparing according to claim 9 cigarette filter additive resin carrier, is characterized in that: first modified starch and resin are carried out to heat kneading, mixing and granulation, then add other component extrusion moulding.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210260854.4A CN102838795B (en) | 2012-07-26 | 2012-07-26 | Additive resin carrier for cigarette filters and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210260854.4A CN102838795B (en) | 2012-07-26 | 2012-07-26 | Additive resin carrier for cigarette filters and preparation method thereof |
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| Publication Number | Publication Date |
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| CN102838795A CN102838795A (en) | 2012-12-26 |
| CN102838795B true CN102838795B (en) | 2014-05-21 |
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| CN201210260854.4A Active CN102838795B (en) | 2012-07-26 | 2012-07-26 | Additive resin carrier for cigarette filters and preparation method thereof |
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Cited By (1)
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|---|---|---|---|---|
| EP3800032A4 (en) * | 2019-06-27 | 2021-10-06 | China Tobacco Guangdong Industrial Co., Ltd. | Starch-based multi-channel airflow unit, preparation method therefor and use thereof |
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| CN103416850B (en) * | 2013-07-26 | 2015-07-29 | 北京益生汇康生物技术有限公司 | Reduce the composition and method of making the same that TPM, tar and nicotine suck |
| CN103355743A (en) * | 2013-08-14 | 2013-10-23 | 中国烟草总公司郑州烟草研究院 | Preparation and application of crop waste cigarette filter additive carrier materials |
| CN105504521B (en) * | 2016-01-29 | 2018-05-25 | 广西中烟工业有限责任公司 | A kind of preparation method for the electronics cigarette filter tip piece for capturing free radical |
| CN106221917A (en) * | 2016-08-04 | 2016-12-14 | 河北中烟工业有限责任公司 | A kind of Herba Pogostemonis essential oil preparation technology and the application in cigarette filter rod thereof |
| CN109692672A (en) * | 2018-12-29 | 2019-04-30 | 中国烟草总公司郑州烟草研究院 | A kind of cigarette filter discoloration adsorbent material and preparation method thereof, cigarette filter |
| CN110372916B (en) * | 2019-06-27 | 2021-03-12 | 广东中烟工业有限责任公司 | Starch-based cooling material and application thereof |
| CN111359553B (en) * | 2020-03-12 | 2022-04-01 | 蚌埠学院 | Preparation method of biodegradable edible pigment microcapsule |
| CN112089093A (en) * | 2020-10-13 | 2020-12-18 | 云南养瑞科技集团有限公司 | Preparation method and application of aroma-enhancing degradable plastic particles |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1686014A (en) * | 2005-06-02 | 2005-10-26 | 戴亚 | Cigarette filter tip additive and additive carrier |
| US20060130861A1 (en) * | 2004-12-22 | 2006-06-22 | Philip Morris Usa Inc. | Flavor carrier for use in smoking articles |
| CN101167601A (en) * | 2007-11-20 | 2008-04-30 | 川渝中烟工业公司 | Cigarette composite filter tip additive carrier and manufacturing method thereof |
| WO2010079141A1 (en) * | 2009-01-12 | 2010-07-15 | Sepp Steinlechner | Tobacco filter |
| CN102499477A (en) * | 2011-11-03 | 2012-06-20 | 湖南中烟工业有限责任公司 | Additive with harm reducing function for cigarette filter tip as well as preparation method and application method of additive |
-
2012
- 2012-07-26 CN CN201210260854.4A patent/CN102838795B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20060130861A1 (en) * | 2004-12-22 | 2006-06-22 | Philip Morris Usa Inc. | Flavor carrier for use in smoking articles |
| CN1686014A (en) * | 2005-06-02 | 2005-10-26 | 戴亚 | Cigarette filter tip additive and additive carrier |
| CN101167601A (en) * | 2007-11-20 | 2008-04-30 | 川渝中烟工业公司 | Cigarette composite filter tip additive carrier and manufacturing method thereof |
| WO2010079141A1 (en) * | 2009-01-12 | 2010-07-15 | Sepp Steinlechner | Tobacco filter |
| CN102499477A (en) * | 2011-11-03 | 2012-06-20 | 湖南中烟工业有限责任公司 | Additive with harm reducing function for cigarette filter tip as well as preparation method and application method of additive |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP3800032A4 (en) * | 2019-06-27 | 2021-10-06 | China Tobacco Guangdong Industrial Co., Ltd. | Starch-based multi-channel airflow unit, preparation method therefor and use thereof |
| JP7108058B2 (en) | 2019-06-27 | 2022-07-27 | チャイナ・タバコ・カントン・インダストリアル・カンパニー・リミテッド | Starch multi-channel airflow unit, manufacturing method thereof, and application |
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| CN102838795A (en) | 2012-12-26 |
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