CN102807926B - Preparation method of water aqua bearing cleaning agent - Google Patents
Preparation method of water aqua bearing cleaning agent Download PDFInfo
- Publication number
- CN102807926B CN102807926B CN201210315146.6A CN201210315146A CN102807926B CN 102807926 B CN102807926 B CN 102807926B CN 201210315146 A CN201210315146 A CN 201210315146A CN 102807926 B CN102807926 B CN 102807926B
- Authority
- CN
- China
- Prior art keywords
- cleaning agent
- bearing
- aqueous cleaning
- bearing aqueous
- present
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)
- Detergent Compositions (AREA)
Abstract
The invention provides a use method of a water aqua bearing cleaning agent, and relates to a use method of a cleaning agent. In order to resolve the problems that the cleaning cost increases due to that the existing cleaning agents are used with a 5% use concentration according to the existing water aqua bearing cleaning agent. The use method comprises: mixing uniformly the water aqua bearing cleaning agent and water according to a volume ratio of 2:98, obtaining a solution with a 2% volume concentration, and then cleaning. The water aqua bearing cleaning agent is mainly used for cleaning bearing semi-finished products and finished product bearings in bearing processing processes.
Description
Technical field
The present invention relates to a kind of using method of clean-out system.
Background technology
Matting is very important operation in Production of bearing process, is not only one of extremely important link of the antirust work of bearing, is also one of link improving accurate low noise bearing quality.The dirt kind being often attached on semi-manufactured bearing and finished surface has a lot, has salt, dust, smear metal, abrasive material, lapping paste, rubbing paste, cuttings liquid, hand perspiration and various oil, fat, wax etc., wherein has water misciblely, also has non-water-soluble.If these dirts do not clean up and stick on bearing products surface, will cause or accelerated corrosion, not only impact is processed, is assembled, and can have a strong impact on quality and the work-ing life of product.
The cleaning of the cleaning in bearing machining process and semi-manufactured bearing, finished product is generally adopted in two ways: 1. petroleum solvent cleans (being oil wash), comprises the cleaning of gasoline, kerosene, solar oil; 2. contain the aqueous cleaning (i.e. washing) of tensio-active agent.Oil wash exists cost high, inflammable, poisonous, and for shortcomings such as solid matter (as dust, salt) etc. are difficult for removing.The feature of washing is: with low cost, consumption is few, washability is strong, non-toxic and safe, cleaning are relatively simple.But washing need will be grown with the time when the product of cleaning tape sealed anti-rust oil, the clean-out system therefore using in existing Production of bearing process can not have the problem that cleaning performance is good, cost is low and life cycle is long concurrently.
Summary of the invention
The present invention seeks to solve the clean-out system using in existing Production of bearing process and can not have the problem that cleaning performance is good, cost is low and life cycle is long concurrently, and a kind of using method of bearing aqueous cleaning agent is provided.
A kind of bearing aqueous cleaning agent is mixed by 6.5%～7.5% primary alconol AEO-9,4.5%～5.5% polyoxyethylene nonylphenol ether, 6.5%～7.5% dodecyl diglycollic amide, 8%～9% oleic acid, 21%～21.5% trolamine, 7.5%～8.5% Sodium Nitrite and 40.5%～46% deionized water by mass percentage.
A preparation method for bearing aqueous cleaning agent, specifically completes according to the following steps: one, prepare raw material: take first by mass percentage 6.5%～7.5% primary alconol AEO-9,4.5%～5.5% polyoxyethylene nonylphenol ether, 6.5%～7.5% dodecyl diglycollic amide, 8%～9% oleic acid, 21%～21.5% trolamine, 7.5%～8.5% Sodium Nitrite and 40.5%～46% deionized water; Two, preparation degreasing composition: 6.5%～7.5% the dodecyl diglycollic amide that 4.5%～5.5% the polyoxyethylene nonylphenol ether that 6.5%～7.5% primary alconol AEO-9, the step 1 that step 1 is taken takes and step 1 take is uniformly mixed, and obtains degreasing composition; Three, prepare antirust composition: in temperature, be that 21%～21.5% the trolamine that 8%～9% the oleic acid that at 50 ℃～55 ℃, step 1 taken and step 1 take is uniformly mixed, obtain antirust composition; Four, mix: in 40.5%～46% the deionized water that 7.5%～8.5% the Sodium Nitrite first step 1 being taken is dissolved in that step 1 takes completely, then the antirust composition that adds degreasing composition prepared by step 2 and step 3 to prepare, obtains bearing aqueous cleaning agent after stirring and evenly mixing.
Advantage of the present invention: the bearing aqueous cleaning agent degreasing power that, prepared by the present invention is very excellent wide in range, can clean the dirt that is often attached to semi-manufactured bearing and finished surface, improves the surface clearness of semi-manufactured bearing and finished product, improves bearing surface quality; Two, the bearing aqueous cleaning agent that prepared by the present invention contains rust cleaning composition, therefore eliminates the corrosion hidden danger of product, has good rustless property, guarantees to be issued to non-corroding in 24 hours in the situation of not using rust-preventive agent; Although three foams can increase the degreasing power of aqueous cleaning agent, but overgenerous foam is unfavorable for bearing cleaning and produces, so bearing aqueous cleaning agent prepared by the present invention has low bubble performance, has both guaranteed the degreasing power of aqueous cleaning agent, and be conducive to bearing cleaning production; Four, the bearing aqueous cleaning agent that prepared by the present invention does not have cloud point between 15 ℃～100 ℃, is beneficial to bearing cleaning and produces; The pH value of the bearing aqueous cleaning agent that five, prepared by the present invention, between 8～9.5, is beneficial to bearing (ferrous metal) protection against corrosion; Six, the bearing aqueous cleaning agent solubleness that prepared by the present invention is good, dissolves rapidly the easy bearing cleaning that is beneficial to of preparation and produces; Seven, the bearing aqueous cleaning agent that prepared by the present invention is tasteless, non-stimulated, is beneficial to safety of workers production operation; Eight, the bearing aqueous cleaning agent life cycle that prepared by the present invention is long, can reach one month; Nine, the bearing aqueous cleaning agent preparation process that prepared by the present invention is easy, and the raw material cheapness of employing, so cost is low.
Bearing aqueous cleaning agent prepared by the present invention is mainly used in semi-manufactured bearing and the bearing finished products in the bearing cleaning course of processing.
Embodiment
Embodiment one: present embodiment is that a kind of bearing aqueous cleaning agent is mixed by 6.5%～7.5% primary alconol AEO-9,4.5%～5.5% polyoxyethylene nonylphenol ether, 6.5%～7.5% dodecyl diglycollic amide, 8%～9% oleic acid, 21%～21.5% trolamine, 7.5%～8.5% Sodium Nitrite and 40.5%～46% deionized water by mass percentage.
Primary alconol AEO-9 described in present embodiment is that the polymerization degree is 9 primary aliphatic alcohols Soxylat A 25-7.
The using method of the bearing aqueous cleaning agent described in present embodiment: be that 2:98 mixes the bearing aqueous cleaning agent described in present embodiment with water by the bearing aqueous cleaning agent described in present embodiment and water volume ratio, obtain 2% volumetric concentration solution, then clean, very convenient simple.
Bearing aqueous cleaning agent prepared by the present invention is mainly used in semi-manufactured bearing and the bearing finished products in the bearing cleaning course of processing.
Bearing aqueous cleaning agent degreasing power described in present embodiment is very excellent wide in range, the dirt that is often attached to semi-manufactured bearing and finished surface can be cleaned, and improves the surface clearness of semi-manufactured bearing and finished product, improves bearing surface quality.
Bearing aqueous cleaning agent described in present embodiment contains rust cleaning composition, therefore eliminates the corrosion hidden danger of product, has good rustless property, guarantees to be issued to non-corroding in 24 hours in the situation of not using rust-preventive agent.
Although foam can increase the degreasing power of aqueous cleaning agent, but overgenerous foam is unfavorable for bearing cleaning and produces, so the bearing aqueous cleaning agent described in present embodiment has low bubble performance, has both guaranteed the degreasing power of aqueous cleaning agent, and be conducive to bearing cleaning production.
Bearing aqueous cleaning agent described in present embodiment does not have cloud point, is beneficial to bearing cleaning and produces.
The pH value of the bearing aqueous cleaning agent described in present embodiment, between 8～9.5, is beneficial to bearing (ferrous metal) protection against corrosion.
Bearing aqueous cleaning agent solubleness described in present embodiment is good, dissolves rapidly the easy bearing cleaning that is beneficial to of preparation and produces
Bearing aqueous cleaning agent described in present embodiment is tasteless, non-stimulated, is beneficial to safety of workers production operation.
Bearing aqueous cleaning agent life cycle described in present embodiment is long, can reach one month.
Embodiment two: the difference of present embodiment and embodiment one is: described bearing aqueous cleaning agent is mixed by 7% primary alconol AEO-9,5% polyoxyethylene nonylphenol ether, 7% dodecyl diglycollic amide, 8.5% oleic acid, 21.25% trolamine, 8% Sodium Nitrite and 43.25% deionized water by mass percentage.Other embodiments one are identical.
Embodiment three: present embodiment is a kind of preparation method of bearing aqueous cleaning agent, specifically completes according to the following steps: one, prepare raw material: take first by mass percentage 6.5%～7.5% primary alconol AEO-9,4.5%～5.5% polyoxyethylene nonylphenol ether, 6.5%～7.5% dodecyl diglycollic amide, 8%～9% oleic acid, 21%～21.5% trolamine, 7.5%～8.5% Sodium Nitrite and 40.5%～46% deionized water; Two, preparation degreasing composition: 6.5%～7.5% the dodecyl diglycollic amide that 4.5%～5.5% the polyoxyethylene nonylphenol ether that 6.5%～7.5% primary alconol AEO-9, the step 1 that step 1 is taken takes and step 1 take is uniformly mixed, and obtains degreasing composition; Three, prepare antirust composition: in temperature, be that 21%～21.5% the trolamine that 8%～9% the oleic acid that at 50 ℃～55 ℃, step 1 taken and step 1 take is uniformly mixed, obtain antirust composition; Four, mix: in 40.5%～46% the deionized water that 7.5%～8.5% the Sodium Nitrite first step 1 being taken is dissolved in that step 1 takes completely, then the antirust composition that adds degreasing composition prepared by step 2 and step 3 to prepare, obtains bearing aqueous cleaning agent after stirring and evenly mixing.
Primary alconol AEO-9 described in present embodiment is that the polymerization degree is 9 primary aliphatic alcohols Soxylat A 25-7.
The using method of the bearing aqueous cleaning agent described in present embodiment: be that 2:98 mixes the bearing aqueous cleaning agent described in present embodiment with water by the bearing aqueous cleaning agent described in present embodiment and water volume ratio, obtain 2% volumetric concentration solution, then clean, very convenient simple.
Bearing aqueous cleaning agent prepared by the present invention is mainly used in semi-manufactured bearing and the bearing finished products in the bearing cleaning course of processing.
Bearing aqueous cleaning agent degreasing power prepared by present embodiment is very excellent wide in range, the dirt that is often attached to semi-manufactured bearing and finished surface can be cleaned, and improves the surface clearness of semi-manufactured bearing and finished product, improves bearing surface quality.
Bearing aqueous cleaning agent prepared by present embodiment contains rust cleaning composition, therefore eliminates the corrosion hidden danger of product, has good rustless property, guarantees to be issued to non-corroding in 24 hours in the situation of not using rust-preventive agent.
Although foam can increase the degreasing power of aqueous cleaning agent, but overgenerous foam is unfavorable for bearing cleaning and produces, so bearing aqueous cleaning agent prepared by present embodiment has low bubble performance, has both guaranteed the degreasing power of aqueous cleaning agent, and be conducive to bearing cleaning production.
Bearing aqueous cleaning agent prepared by present embodiment does not have cloud point, is beneficial to bearing cleaning and produces.
The pH value of bearing aqueous cleaning agent prepared by present embodiment, between 8～9.5, is beneficial to bearing (ferrous metal) protection against corrosion; .
Bearing aqueous cleaning agent solubleness prepared by present embodiment is good, dissolves rapidly the easy bearing cleaning that is beneficial to of preparation and produces.
Bearing aqueous cleaning agent prepared by present embodiment is tasteless, non-stimulated, is beneficial to safety of workers production operation.
Bearing aqueous cleaning agent life cycle prepared by present embodiment is long, can reach one month.
Bearing aqueous cleaning agent preparation process prepared by present embodiment is easy, and the raw material cheapness of employing, so cost is low.
Embodiment four: the difference of present embodiment and embodiment three is: take first by mass percentage 7% primary alconol AEO-9,5% polyoxyethylene nonylphenol ether, 7% dodecyl diglycollic amide, 8.5% oleic acid, 21.25% trolamine, 8% Sodium Nitrite and 43.25% deionized water in step 1.Other embodiments three are identical.
Adopt following verification experimental verification effect of the present invention:
Test one: a kind of preparation method of bearing aqueous cleaning agent, specifically completes according to the following steps: one, prepare raw material: take first by mass percentage 7% primary alconol AEO-9,5% polyoxyethylene nonylphenol ether, 7% dodecyl diglycollic amide, 8.5% oleic acid, 21.25% trolamine, 8% Sodium Nitrite and 43.25% deionized water; Two, preparation degreasing composition: 7% the dodecyl diglycollic amide that 5% the polyoxyethylene nonylphenol ether that 7% primary alconol AEO-9, the step 1 that step 1 is taken takes and step 1 take is uniformly mixed, and obtains degreasing composition; Three, prepare antirust composition: in temperature, be that 21.25% the trolamine that 8.5% the oleic acid that at 53 ℃, step 1 taken and step 1 take is uniformly mixed, obtain antirust composition; Four, mix: in 43.25% the deionized water that 8% the Sodium Nitrite first step 1 being taken is dissolved in that step 1 takes completely, then the antirust composition that adds degreasing composition prepared by step 2 and step 3 to prepare, obtains bearing aqueous cleaning agent after stirring and evenly mixing.
The described primary alconol AEO-9 of this test is that the polymerization degree is 9 primary aliphatic alcohols Soxylat A 25-7.
The bearing aqueous cleaning agent of this test preparation is from the appearance the transparent uniform liquid of sundown, non-stimulated peculiar smell.
Known by the test of pH value, the bearing aqueous cleaning agent pH of this test preparation is 8.7.
Known by specific weight determine (d420), the proportion (d420) of the bearing aqueous cleaning agent of this test preparation is 1.02.
First by the bearing aqueous cleaning agent described in present embodiment and water volume ratio, be that 2:98 mixes the bearing aqueous cleaning agent described in present embodiment with water, obtain 2% volumetric concentration solution, then 2% volumetric concentration solution is carried out to solution surface tension test known, open for 37.65mN/m on the surface of 2% volumetric concentration solution.
First by the bearing aqueous cleaning agent described in present embodiment and water volume ratio, be that 2:98 mixes the bearing aqueous cleaning agent described in present embodiment with water, obtain 2% volumetric concentration solution, then 2% volumetric concentration solution is carried out to cleaning efficiency test known, it is 97% that 2% volumetric concentration solution cleaning efficiency is surveyed.
By dissolution rate, test knownly, the bearing aqueous cleaning agent dissolution rate of this test preparation is instant.
By antifoam performance, test knownly, the antifoam performance of the bearing aqueous cleaning agent of this test preparation is good.
Known by cloud point test, the bearing aqueous cleaning agent of this test preparation is warming up to 100 ℃ of processes and does not become turbid from 15 ℃, the bearing aqueous cleaning agent that is this test preparation does not have cloud point between 15 ℃～100 ℃, so the bearing aqueous cleaning agent of this test preparation can be for warm wash.
Adopt the bearing aqueous cleaning agent of this test preparation to carry out rust-preventing characteristic test, first by the bearing aqueous cleaning agent described in present embodiment and water volume ratio, be that 2:98 mixes the bearing aqueous cleaning agent described in present embodiment with water, obtain 2% volumetric concentration solution, draw 2% volumetric concentration solution with minim pipette, by plum blossom form, splash into five on one-level grey cast iron test piece polished face, every diameter is about 4mm～5mm.Then test piece is placed on moisture eliminator dividing plate to (noting not plug-hole), the dryer door of closing, is placed in the thermostat container of constant temperature to 35 ± 2 ℃, and long run test is taken out the test piece of one-level grey cast iron after 4h, observes, and reaches A level rustless.
Adopt the bearing aqueous cleaning agent of this test preparation to carry out corrosion test, first by the bearing aqueous cleaning agent described in present embodiment and water volume ratio, be that 2:98 mixes the bearing aqueous cleaning agent described in present embodiment with water, obtain 2% volumetric concentration solution, then the 45# steel disc of preparation, copper sheet, LY12 aluminium flake are dipped in respectively in 2% volumetric concentration solution entirely, add a cover respectively lens, be displaced in the thermostat container of constant temperature to 55 ℃ ± 2 ℃, long run test is to steel disc 24h, copper sheet 4h, LY12 aluminium flake 4h, then take out test piece and observe, all qualified.
Claims (1)
1. a using method for bearing aqueous cleaning agent, is characterized in that the using method of bearing aqueous cleaning agent completes according to the following steps:
By bearing aqueous cleaning agent and water volume ratio, be that 2:98 mixes bearing aqueous cleaning agent with water, obtain 2% volumetric concentration solution, then clean; Described bearing aqueous cleaning agent completes according to the following steps: one, prepare raw material: take first by mass percentage 7% primary alconol AEO-9,5% polyoxyethylene nonylphenol ether, 7% dodecyl diglycollic amide, 8.5% oleic acid, 21.25% trolamine, 8% Sodium Nitrite and 43.25% deionized water; Two, preparation degreasing composition: 7% the dodecyl diglycollic amide that 5% the polyoxyethylene nonylphenol ether that 7% primary alconol AEO-9, the step 1 that step 1 is taken takes and step 1 take is uniformly mixed, and obtains degreasing composition; Three, prepare antirust composition: in temperature, be that 21.25% the trolamine that 8.5% the oleic acid that at 53 ℃, step 1 taken and step 1 take is uniformly mixed, obtain antirust composition; Four, mix: in 43.25% the deionized water that 8% the Sodium Nitrite first step 1 being taken is dissolved in that step 1 takes completely, then the antirust composition that adds degreasing composition prepared by step 2 and step 3 to prepare, obtains bearing aqueous cleaning agent after stirring and evenly mixing; Wherein said primary alconol AEO-9 is that the polymerization degree is 9 primary aliphatic alcohols Soxylat A 25-7.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210315146.6A CN102807926B (en) | 2012-08-30 | 2012-08-30 | Preparation method of water aqua bearing cleaning agent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210315146.6A CN102807926B (en) | 2012-08-30 | 2012-08-30 | Preparation method of water aqua bearing cleaning agent |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102807926A CN102807926A (en) | 2012-12-05 |
| CN102807926B true CN102807926B (en) | 2014-04-23 |
Family
ID=47231798
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210315146.6A Active CN102807926B (en) | 2012-08-30 | 2012-08-30 | Preparation method of water aqua bearing cleaning agent |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102807926B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107365640A (en) * | 2016-05-12 | 2017-11-21 | 无锡市久嘉科技有限公司 | A kind of water base bearing cleaning agent of safety and environmental protection and its preparation method and application |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1504550A (en) * | 2002-12-04 | 2004-06-16 | 山西大学 | Water base lubricant for drawing metallic fiber material and preparing process thereof |
| CN101270478A (en) * | 2008-04-25 | 2008-09-24 | 浙江大学 | Metal cleaning agent |
| CN101748007A (en) * | 2008-12-10 | 2010-06-23 | 中国科学院过程工程研究所 | Method for preparing degreaser |
| CN102242369A (en) * | 2011-07-05 | 2011-11-16 | 白马轴承技术(洛阳)有限公司 | Metal bearing water-based cleaning agent and preparation method and application thereof |
-
2012
- 2012-08-30 CN CN201210315146.6A patent/CN102807926B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1504550A (en) * | 2002-12-04 | 2004-06-16 | 山西大学 | Water base lubricant for drawing metallic fiber material and preparing process thereof |
| CN101270478A (en) * | 2008-04-25 | 2008-09-24 | 浙江大学 | Metal cleaning agent |
| CN101748007A (en) * | 2008-12-10 | 2010-06-23 | 中国科学院过程工程研究所 | Method for preparing degreaser |
| CN102242369A (en) * | 2011-07-05 | 2011-11-16 | 白马轴承技术(洛阳)有限公司 | Metal bearing water-based cleaning agent and preparation method and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102807926A (en) | 2012-12-05 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103757640B (en) | A kind of micro-emulsion type water-based metal antirust liquid | |
| CN103590044B (en) | A kind of metal polish | |
| CN102747380B (en) | Environmentally-friendly cleaning agent and preparation method thereof | |
| CN104947112B (en) | A kind of preparation of environment-friendly metal polishing fluid | |
| CN102877082B (en) | Wax solvent for cleaning magnesium alloy or aluminum alloy workpiece | |
| CN103409741B (en) | A kind of multifunctional treating liquid for surface of iron or steel and its preparation method and application | |
| CN102925908B (en) | Water-based normal-temperature rustproof spray cleaning agent and preparation method thereof | |
| CN109136940A (en) | Low bubble cleaning agent of a kind of environment-friendly type high performance ferrous metal antirust and preparation method thereof | |
| CN104726884A (en) | Environment-friendly water-based metal cleaner | |
| CN102953071A (en) | Highly-efficiently degreasing and rust-removal surface treating agent for metal | |
| CN104313614A (en) | Low-foam detergent and preparation method thereof | |
| CN104372362B (en) | Aluminum alkali-washing corrosion inhibitor, and preparation method and application thereof | |
| CN103668155B (en) | A kind of method of passivating solution and passivation ferrous metal surface thereof | |
| CN102807926B (en) | Preparation method of water aqua bearing cleaning agent | |
| CN105018913A (en) | Rust prevention liquid for metal surfaces | |
| CN103409761A (en) | Metal rust removal solution and its preparation method | |
| CN104388936A (en) | Low-foam antirust polishing agent and its preparation method | |
| CN103911226A (en) | Smoke ventilator cleaning compound and preparation method thereof | |
| RU2387704C1 (en) | Detergent for cleaning containers and metal surfaces | |
| CN113564605B (en) | Environment-friendly organic engine test solution | |
| CN105239067B (en) | A kind of environment-friendly metal high temperature quenching antirust agent and preparation method thereof | |
| CN104264169A (en) | Special cleaning agent for metal part and preparation method thereof | |
| CN108486585A (en) | A kind of highly effective antirust metal cleaner and preparation method thereof | |
| CN103882464B (en) | A kind of steel surface clean-out system and application thereof | |
| CN106467972A (en) | A kind of rustless steel cleansing cream and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |