CN102796454A - Nanoparticle-containing automobile polishing protective wax and its preparation method - Google Patents
Nanoparticle-containing automobile polishing protective wax and its preparation method Download PDFInfo
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- CN102796454A CN102796454A CN2012102901963A CN201210290196A CN102796454A CN 102796454 A CN102796454 A CN 102796454A CN 2012102901963 A CN2012102901963 A CN 2012102901963A CN 201210290196 A CN201210290196 A CN 201210290196A CN 102796454 A CN102796454 A CN 102796454A
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Abstract
The invention provides a nanoparticle-containing automobile polishing protective wax and its preparation method. The protective wax comprises the following components by mass: 10-20% of a high polymer synthetic wax; 5-10% of a natural resin purified wax; 5.0-10.0% of dimethyl silicon oil; 0.2-3.0% of nanoparticle powder; 60-70% of an aliphatic hydrocarbon solvent; 1.0-1.5% of a dispersing agent; and 0.5-1.0% of essence. By adding the nanoparticle material and using a special technological preparation method, the nanoparticles can be maintained in a nano-state before and after using the prepared automobile polishing protective wax, so that the product can show nano-properties. Even if the product is applied and used on an automobile surface, the product has good self-cleaning performance and hydrophobicity, can effectively resist antibacterial, prevent enzymes, defend static electricity, decompose oil stains, prevent aging, as well as keep a brilliant color and brightness on the automobile surface for a long time, thereby more effectively prolonging the service life of the automobile, and creating more economic and social benefits for people.
Description
Technical field
The present invention relates to a kind of automobile glazing protection wax, relate in particular to a kind of automobile glazing protection wax that contains nanoparticle and preparation method thereof.
Background technology
At present domestic and international widely used automobile glazing protection wax, major function is glazing and protection automobile finish, and the time of automobile finish gloss and protection is shorter; On existing automobile glazing protection cerul plinth; The technical issues that need to address are how to improve the comprehensive function of existing simoniz; Be self-cleaning, hydrophobicity, antibiotic anti-enzyme, anti-electrostatic, decomposition greasy dirt, prevent to wear out, keep the bright in luster and brightness of car surface for a long time.
Summary of the invention
The object of the present invention is to provide a kind of automobile glazing protection wax that contains nanoparticle, it has good self-cleaning, hydrophobicity, and can effectively antibiotic anti-enzyme, anti-electrostatic, decomposition greasy dirt, prevent aging and the bright in luster and brightness of maintenance car surface.
Another object of the present invention is to provide a kind of preparation method who contains the automobile glazing protection wax of nanoparticle; Make nanoparticle before product uses with after using, all keep the nanometer state through special its preparation process, thereby make product show nano-meter characteristic.
For realizing above-mentioned purpose; The present invention provides a kind of automobile glazing protection wax that contains nanoparticle; Comprise: macromolecule synthesising wax, natural resin purification wax, dimethyl silicone oil, nanoparticle powder, aliphatic solvents, dispersion agent and essence, its each constituent mass ratio is: macromolecule synthesising wax 10-20%; Natural resin purification wax 5-10%; Dimethyl silicone oil 5.0-10.0%; Nanoparticle powder 0.2-3.0%; Aliphatic solvents 60-70%; Dispersion agent 1.0-1.5%; Essence 0.5-1.0%.
The fusing point of said macromolecule synthesising wax is 80-90 ℃.
The fusing point of said natural resin purification wax is 80-90 ℃, and acid number is less than or equal to 20mgKOH/g.
Said dimethyl-silicon oil viscosity is 500-10000mm
2/ s.
Said nanoparticle powder is titanium oxide, silicon-dioxide or the PTFE powder of particle diameter less than 20nm.
The boiling range of said aliphatic solvents is 160-260 ℃.
Said dispersion agent is siliceous super wetting dispersing agent.
The present invention also provides a kind of preparation method who contains the automobile glazing protection wax of nanoparticle, may further comprise the steps:
Step 1, macromolecule synthesising wax, natural resin purification wax, dimethyl silicone oil, nanoparticle powder, aliphatic solvents, dispersion agent and essence are provided, its constituent mass ratio is: macromolecule synthesising wax 10-20%; Natural resin purification wax 5-10%; Dimethyl silicone oil 5.0-10.0%; Nanoparticle powder 0.2-3.0%; Aliphatic solvents 60-70%; Dispersion agent 1.0-1.5%; Essence 0.5-1.0%;
Step 2, the aliphatic solvents Hybrid Heating of macromolecule synthesising wax, natural resin purification wax and 70% is dissolved to even all bright, processes first solution;
Step 3, the aliphatic solvents with remaining 30%, dimethyl silicone oil, dispersant stir; Under high speed dispersion, the nanoparticle powder is slowly added then; In adition process, keep mixed solution to be being clear to translucent; Still keep high speed dispersion stable after adding finishes, process second solution until mixed solution;
Step 4, second solution slowly added to be in first solution in the high speed dispersion form mixed solution, heat and be incubated to 90-95 ℃, dispersed with stirring is the back fast cooling evenly; When temperature is reduced to 73-77 ℃, essence is added the continued that stirs cooling;
Step 5, reduce to when being higher than temperature of solidification 2-3 ℃, mixed solution is poured in the packaging vessel, reduce to room temperature naturally, and then make automobile glazing protection wax when mixeding liquid temperature.
The fusing point of said macromolecule synthesising wax is 80-90 ℃; The fusing point of said natural resin purification wax is 80-90 ℃, and acid number is less than or equal to 20mgKOH/g; Said dimethyl-silicon oil viscosity is 500-10000mm
2/ s; Said nanoparticle powder is titanium oxide, silicon-dioxide or the PTFE powder of particle diameter less than 20nm; The boiling range of said aliphatic solvents is 160-260 ℃; Said dispersion agent is siliceous super wetting dispersing agent.
Beneficial effect of the present invention: the present invention provides a kind of automobile glazing protection wax that contains nanoparticle and preparation method thereof; Through adding nanometer particle material; And use special its preparation process to make nanoparticle before prepared automobile glazing protection wax uses with after using, all keep the nanometer state; Thereby make product show nano-meter characteristic, even product has good self-cleaning, hydrophobicity after car surface is embrocated use, can effectively antibiotic anti-enzyme, anti-electrostatic, decomposition greasy dirt, prevent to wear out, keep for a long time the bright in luster and brightness of car surface; Thereby prolong motor live time more effectively, for people create more economic and social benefit.
Embodiment
Technique means and the effect thereof taked for further setting forth the present invention are described in detail below in conjunction with the preferred embodiments of the present invention.
The present invention provides a kind of automobile glazing protection wax that contains nanoparticle; Comprise: macromolecule synthesising wax, natural resin purification wax, dimethyl silicone oil, nanoparticle powder, aliphatic solvents, dispersion agent and essence, its each constituent mass ratio is: macromolecule synthesising wax 10-20%; Natural resin purification wax 5-10%; Dimethyl silicone oil 5.0-10.0%; Nanoparticle powder 0.2-3.0%; Aliphatic solvents 60-70%; Dispersion agent 1.0-1.5%; Essence 0.5-1.0%.
The fusing point of said macromolecule synthesising wax is 80-90 ℃.
The fusing point that said natural resin purification wax requires is 80-90 ℃, and acid number is less than or equal to 20mgKOH/g.
Said dimethyl-silicon oil viscosity is 500-10000mm
2/ s.
Said nanoparticle powder is titanium oxide, silicon-dioxide or the PTFE powder of particle diameter less than 20nm.
The boiling range of said aliphatic solvents is 160-260 ℃.
Said dispersion agent is siliceous super wetting dispersing agent.
The present invention also provides a kind of preparation method who contains the automobile glazing protection wax of nanoparticle, may further comprise the steps:
Step 1, macromolecule synthesising wax, natural resin purification wax, dimethyl silicone oil, nanoparticle powder, aliphatic solvents, dispersion agent and essence are provided, its constituent mass ratio is: macromolecule synthesising wax 10-20%; Natural resin purification wax 5-10%; Dimethyl silicone oil 5.0-10.0%; Nanoparticle powder 0.2-3.0%; Aliphatic solvents 60-70%; Dispersion agent 1.0-1.5%; Essence 0.5-1.0%.
Step 2, the aliphatic solvents Hybrid Heating of macromolecule synthesising wax, natural resin purification wax and 70% is dissolved to even all bright, processes first solution.
Step 3, the aliphatic solvents with remaining 30%, dimethyl silicone oil, dispersant stir; Under high speed dispersion, the nanoparticle powder is slowly added then; In adition process, keep mixed solution to be being clear to translucent; Prevent the conglomeration of nanoparticle powder, finish still high speed dispersion, process second solution to stable.
Step 4, second solution slowly added to be in first solution in the high speed dispersion form mixed solution, heat and be incubated to 90-95 ℃, dispersed with stirring is the back fast cooling evenly, when temperature is reduced to 73-77 ℃, essence is added the continued that stirs cooling.
Step 5, reduce to when being higher than temperature of solidification 2-3 ℃, mixed solution is poured in the packaging vessel, reduce to room temperature naturally, and then make automobile glazing protection wax when mixeding liquid temperature.That is,, so,, this mixing solutions is poured in the packaging vessel when the temperature of this mixing solutions is between 62-63 ℃ the time if the temperature of solidification of this mixed solution is 60 ℃.
The fusing point of said macromolecule synthesising wax is 80-90 ℃; The fusing point of said natural resin purification wax is 80-90 ℃, and acid number is less than or equal to 20mgKOH/g; Said dimethyl-silicon oil viscosity is 500-10000mm
2/ s; Said nanoparticle powder is titanium oxide, silicon-dioxide or the PTFE powder of particle diameter less than 20nm; The boiling range of said aliphatic solvents is 160-260 ℃; Said dispersion agent is siliceous super wetting dispersing agent.
The technical indicator of the automobile glazing protection wax that contains nanoparticle that the present invention makes sees table:
Table 1, the automobile glazing that contains nanoparticle is protected the technical indicator of wax
In sum; The present invention provides a kind of automobile glazing protection wax that contains nanoparticle and preparation method thereof; Through the interpolation nanometer particle material, and use special its preparation process to make nanoparticle before prepared automobile glazing protection wax uses with after using, all keep the nanometer state, thereby make product show nano-meter characteristic; Even product has good self-cleaning, hydrophobicity after car surface is embrocated use; Can effectively antibiotic anti-enzyme, anti-electrostatic, decomposition greasy dirt, prevent to wear out, keep for a long time the bright in luster and brightness of car surface, thereby prolong motor live time more effectively, for people create more economic and social benefit.
The above for the person of ordinary skill of the art, can make other various corresponding changes and distortion according to technical scheme of the present invention and technical conceive, and all these changes and distortion all should belong to the protection domain of claim of the present invention.
Claims (9)
1. an automobile glazing that contains nanoparticle is protected wax; It is characterized in that; Comprise: macromolecule synthesising wax, natural resin purification wax, dimethyl silicone oil, nanoparticle powder, aliphatic solvents, dispersion agent and essence, its each constituent mass ratio is: macromolecule synthesising wax 10-20%; Natural resin purification wax 5-10%; Dimethyl silicone oil 5.0-10.0%; Nanoparticle powder 0.2-3.0%; Aliphatic solvents 60-70%; Dispersion agent 1.0-1.5%; Essence 0.5-1.0%.
2. the automobile glazing protection wax that contains nanoparticle as claimed in claim 1 is characterized in that the fusing point of said macromolecule synthesising wax is 80-90 ℃.
3. the automobile glazing protection wax that contains nanoparticle as claimed in claim 1 is characterized in that the fusing point of said natural resin purification wax is 80-90 ℃, and acid number is less than or equal to 20mgKOH/g.
4. the automobile glazing protection wax that contains nanoparticle as claimed in claim 1 is characterized in that said dimethyl-silicon oil viscosity is 500-10000mm
2/ s.
5. the automobile glazing protection wax that contains nanoparticle as claimed in claim 1 is characterized in that said nanoparticle powder is titanium oxide, silicon-dioxide or the PTFE powder of particle diameter less than 20nm.
6. the automobile glazing protection wax that contains nanoparticle as claimed in claim 1 is characterized in that the boiling range of said aliphatic solvents is 160-260 ℃.
7. the automobile glazing protection wax that contains nanoparticle as claimed in claim 1 is characterized in that said dispersion agent is siliceous super wetting dispersing agent.
8. a preparation method who contains the automobile glazing protection wax of nanoparticle as claimed in claim 1 is characterized in that, may further comprise the steps:
Step 1, macromolecule synthesising wax, natural resin purification wax, dimethyl silicone oil, nanoparticle powder, aliphatic solvents, dispersion agent and essence are provided;
Step 2, the aliphatic solvents Hybrid Heating of macromolecule synthesising wax, natural resin purification wax and 70% is dissolved to even all bright, processes first solution;
Step 3, the aliphatic solvents with remaining 30%, dimethyl silicone oil, dispersant stir; Under high speed dispersion, the nanoparticle powder is slowly added then; In adition process, keep mixed solution to be being clear to translucent; Still keep high speed dispersion stable after adding finishes, process second solution until mixed solution;
Step 4, second solution slowly added to be in first solution in the high speed dispersion form mixed solution, heat and be incubated to 90-95 ℃, dispersed with stirring is the back fast cooling evenly; When temperature is reduced to 73-77 ℃ with the essence adding, the continued that stirs cooling;
Step 5, reduce to when being higher than temperature of solidification 2-3 ℃, mixed solution is poured in the packaging vessel, reduce to room temperature naturally, and then make automobile glazing protection wax when mixeding liquid temperature.
9. the preparation method who contains the automobile glazing protection wax of nanoparticle as claimed in claim 8 is characterized in that the fusing point of said macromolecule synthesising wax is 80-90 ℃; The fusing point of said natural resin purification wax is 80-90 ℃, and acid number is less than or equal to 20mgKOH/g; Said dimethyl-silicon oil viscosity is 500-10000mm
2/ s; Said nanoparticle powder is titanium oxide, silicon-dioxide or the PTFE powder of particle diameter less than 20nm; The boiling range of said aliphatic solvents is 160-260 ℃; Said dispersion agent is siliceous super wetting dispersing agent.
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| CN102796454B CN102796454B (en) | 2015-07-08 |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104073033A (en) * | 2014-07-06 | 2014-10-01 | 杨发祥 | High-wear-resistant high-hardness nanoscale titanium crystal coating liquid and preparation method thereof |
| CN104745010A (en) * | 2015-03-10 | 2015-07-01 | 深圳市彩虹精细化工股份有限公司 | Water-in-oil type solid automobile glazing protective wax and preparation method thereof |
| CN105153937A (en) * | 2015-08-24 | 2015-12-16 | 广州赫厉狮森汽车用品有限公司 | Total-synthesis solid wax capable of forming platinum coating film and preparation method of total-synthetic solid wax |
| CN105885439A (en) * | 2014-08-26 | 2016-08-24 | 闫立群 | Protective wax based on surface modification graphene and preparation method thereof |
| CN109266226A (en) * | 2018-08-06 | 2019-01-25 | 湖州赛德新材料科技有限公司 | A kind of automobile major wax and preparation method thereof with self-cleaning effect |
Citations (3)
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| CN1030781A (en) * | 1988-06-30 | 1989-02-01 | 上海市胜利日用化工厂 | A kind of cleaning and polishing agent |
| CN1081193A (en) * | 1992-07-09 | 1994-01-26 | 秦建国 | Multi-usage brightening agent and manufacture method thereof |
| CN101210155A (en) * | 2006-12-28 | 2008-07-02 | 财团法人工业技术研究院 | Material surface treatment composition, material and hydrophobic film prepared from the same |
-
2012
- 2012-08-15 CN CN201210290196.3A patent/CN102796454B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1030781A (en) * | 1988-06-30 | 1989-02-01 | 上海市胜利日用化工厂 | A kind of cleaning and polishing agent |
| CN1081193A (en) * | 1992-07-09 | 1994-01-26 | 秦建国 | Multi-usage brightening agent and manufacture method thereof |
| CN101210155A (en) * | 2006-12-28 | 2008-07-02 | 财团法人工业技术研究院 | Material surface treatment composition, material and hydrophobic film prepared from the same |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104073033A (en) * | 2014-07-06 | 2014-10-01 | 杨发祥 | High-wear-resistant high-hardness nanoscale titanium crystal coating liquid and preparation method thereof |
| CN105885439A (en) * | 2014-08-26 | 2016-08-24 | 闫立群 | Protective wax based on surface modification graphene and preparation method thereof |
| CN104745010A (en) * | 2015-03-10 | 2015-07-01 | 深圳市彩虹精细化工股份有限公司 | Water-in-oil type solid automobile glazing protective wax and preparation method thereof |
| CN104745010B (en) * | 2015-03-10 | 2017-03-08 | 深圳市兆新能源股份有限公司 | water-in-oil type solid vehicle glazing protection wax and preparation method thereof |
| CN105153937A (en) * | 2015-08-24 | 2015-12-16 | 广州赫厉狮森汽车用品有限公司 | Total-synthesis solid wax capable of forming platinum coating film and preparation method of total-synthetic solid wax |
| CN109266226A (en) * | 2018-08-06 | 2019-01-25 | 湖州赛德新材料科技有限公司 | A kind of automobile major wax and preparation method thereof with self-cleaning effect |
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| CN102796454B (en) | 2015-07-08 |
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Address after: Baoan District Shiyan town Shenzhen city Guangdong province 518000 house Rainbow Industrial City Patentee after: Shenzhen trillion new energy Limited by Share Ltd Address before: Baoan District Shiyan town Shenzhen city Guangdong province 518000 house Rainbow Industrial City Patentee before: Shenzhen Rainbow Fine Chemical Industry Co., Ltd. |