CN102795945A - Special sulfur-resin double-membrane humic-acid controlled release fertilizer suitable for culturing garlic with mulching film - Google Patents

Special sulfur-resin double-membrane humic-acid controlled release fertilizer suitable for culturing garlic with mulching film Download PDF

Info

Publication number
CN102795945A
CN102795945A CN2012102630745A CN201210263074A CN102795945A CN 102795945 A CN102795945 A CN 102795945A CN 2012102630745 A CN2012102630745 A CN 2012102630745A CN 201210263074 A CN201210263074 A CN 201210263074A CN 102795945 A CN102795945 A CN 102795945A
Authority
CN
China
Prior art keywords
release
fertilizer
sulfur
garlic
slow
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN2012102630745A
Other languages
Chinese (zh)
Inventor
丁方军
谷端银
陈士更
孟庆羽
吴钦泉
付乃峰
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SHANDONG AGRUNIV FERT SCITECH CO Ltd
Original Assignee
SHANDONG AGRUNIV FERT SCITECH CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SHANDONG AGRUNIV FERT SCITECH CO Ltd filed Critical SHANDONG AGRUNIV FERT SCITECH CO Ltd
Priority to CN2012102630745A priority Critical patent/CN102795945A/en
Publication of CN102795945A publication Critical patent/CN102795945A/en
Pending legal-status Critical Current

Links

Landscapes

  • Fertilizers (AREA)

Abstract

The invention discloses a special sulfur-resin double-membrane humic-acid controlled release fertilizer suitable for culturing garlic with a mulching film. The fertilizer is characterized by being prepared from the following ingredients by mass percent: 130%-165% of resin-coated urea, 135%-150% of sulfur-coated urea, 120%-170% of diammonium phosphate, 290%-380% of potassium sulphate, 220%-240% of humic-acid controlled release compound fertilizers and 10%-15% of zinc sulfate. Compared with the prior art, the special sulfur-resin double-membrane humic-acid controlled release fertilizer for culturing the garlic is produced in a compounded manner by utilizing the nutrient releasing characteristic of a sulfur-coated and resin-coated fertilizer and the slow release synergy effect of humic acid on nutrients according to the nutrient absorption principle of the garlic, and a certain amount of medium and trace elements are compounded in the fertilizer, so that the interdependence between release and control of nutrients is achieved, and good fertilizing and absorbing effects are ensured.

Description

A kind of two film humic acids slow-release or control-release fertilizers of the special-purpose sulfur and resin of film-mulching cultivation garlic that are suitable for
Technical field
The present invention relates to a kind of slow/controlled release fertilizer technology field that belongs to, specifically is a kind of two film humic acids slow-release or control-release fertilizers of the special-purpose sulfur and resin of film-mulching cultivation garlic that are suitable for.
Background technology
Garlic is a Liliaceae allium biennial herb plant, and special sharp flavor is arranged, and is requisite seasonings and the important export vegetables of earning foreign exchange in the daily life.
The Shandong garlic mainly concentrates on by the end of September to the early October sowing, and the membrane covering open country is survived the winter, and gather in the crops to early June next year by the end of May.Common composite fertilizer fertilizer efficiency is fast, and when base fertilizer applied, the garlic seedling was little, absorbs the fertilizer ability, and fertilizer is prone to the loss loss, is difficult to satisfy the nutrient demand of garlic growing period, and temperature and ground temperature are lower in the winter time.Therefore when the film-mulching cultivation garlic, provide a kind of and can increase production, can improve again the long-acting slow-releasing and controlled-releasing of quality fertile very necessary.
Be main to use readily avaiable fertilizer during current garlic produces; The membrane covering of extensively adopting has strengthened the difficulty of topdressing again; Part garlic farmers are for the saving of labor; At seeding time with nitrogenous fertilizer 60%~80%, all the disposable base of phosphorus potash fertilizer is executed (all the other nitrogenous fertilizer spring in next year topdress use), but this and do not meet the nutrition absorption characteristic of garlic; Readily avaiable fertilizer decomposes soon in addition, difficulty is made this traditional fertilizing method very easily cause available nutrient a large amount of losses in the winter time by soil fixing, thereby reduces utilization rate of fertilizer.
The controlled release fertilizer nutrient discharges steadily, can artificially control its release period (2-3) according to the crop nutrition content absorption characteristics.In common controlled release fertilizer, mix the controlled release Bulk Blending Fertilizer that the quick-acting chemical fertilizer of part are processed, controlled release is fertile to be supplied the fertile persistent general feature except that possessing, and has also solved the low excessively problem of traditional controlled release nutrient release amount in fertile early stage.In addition, the minimizing of coating quantity has also reduced cost, more is prone to accepted by garlic farmers.
Summary of the invention
For addressing the above problem; The present invention provides a kind of two film humic acids slow-release or control-release fertilizers of the special-purpose sulfur and resin of film-mulching cultivation garlic that are suitable for, and the present invention utilizes the Nutrient Release of sulphur, the two membrane envelope fertilizer of resin, and humic acids is to the sustained-release synergistic effect of nutrient; Law of nutritive absorption according to garlic carries out the two film humic acids slow-release or control-release fertilizers of the special-purpose sulfur and resin of composite production garlic simultaneously; And composite a certain amount of middle trace element, the slow control of nutrient is Ji mutually, guarantees good fertilising and assimilation effect.
For achieving the above object, the present invention adopts following technical scheme:
A kind of two film humic acids slow-release or control-release fertilizers of the special-purpose sulfur and resin of film-mulching cultivation garlic that are suitable for, said fertilizer components and weight proportion are following:
Resin coated urea 130-15;
Sulfur coated urea 135-150;
Diammonium phosphate 120-170;
Vitriolate of tartar 290-380;
Humic acid slow release composite fertilizer 220-240;
Zinc sulfate 10-15.
Further, said fertilizer components and weight proportion are following:
Resin coated urea 130;
Sulfur coated urea 140;
Diammonium phosphate 120;
Vitriolate of tartar 380;
Humic acid slow release composite fertilizer 220;
Zinc sulfate 10.
The two film humic acids slow-release or control-release fertilizers of above-mentioned sulfur and resin, in the said components:
In the said components:
The resin coated urea model is 44-0-0, nitrogen content >=44%;
The sulfur coated urea model is 35-0-0, nitrogen content >=35%, and sulphur content is 25%;
Diammonium phosphate is a granule type, and the mass percentage content of nitrogen, Vanadium Pentoxide in FLAKES is respectively 18%, 46%;
Vitriolate of tartar is a granule type, and potassium oxide content is 50%;
Zinc sulfate adopts commercially available agricultural Zinc Sulphate Heptahydrate crystal, and zinc content is 21~22%, sulphur content >=10%;
The mass percentage content of nitrogen, Vanadium Pentoxide in FLAKES, potassium oxide is in the humic acid slow release composite fertilizer: 14%~16%, 7~9%, 16~18%, and humic acids content >=10%.
Above-mentioned humic acid slow release composite fertilizer, the mass percentage content of nitrogen, Vanadium Pentoxide in FLAKES, potassium oxide is respectively 15%, 8%, 17%.
Said component raw material particle diameter is 2-4mm.
Excellent results of the present invention is following:
1. quick-acting, slow, long-acting combining; Satisfy the garlic nutrient demand in vegetative period; Especially satisfied the nutrient demand of garlic under the shed cultivation condition: diammonium phosphate, vitriolate of tartar can provide the quick-acting npk nutrients of garlic early growth; Sulphur and resin coated urea provide the nitrogen nutrient of different release periods, and the nutrient demand of garlic whole growth phase is satisfied in the npk nutrient that humic acid slow release the is fertile release of releiving.
2. nutrient reasonable ratio is fit to the nutrient uptake feature of garlic, and composite a certain amount of in trace element (sulphur, zinc); And contain the synergy nutrient, stimulate plant growth and improve the humic acids composition of quality; The slow control of nutrient is Ji mutually, improves specific absorption and plant recovery of nutrient, improves quality of agricultural product.
3. can effectively promote plant growth, can play the effect of improving the soil of preserve moisture and fertility again, production-increasing function is remarkable, and raising the output can reach about 10%.
4. significantly improve soluble proteins and VC content in the garlic, improve garlic quality and mouthfeel.
Below in conjunction with embodiment the present invention is further specified.
Embodiment
A kind of two film humic acids slow-release or control-release fertilizers of the special-purpose sulfur and resin of film-mulching cultivation garlic that are suitable for comprise following component: resin coated urea, sulfur coated urea, diammonium phosphate, vitriolate of tartar, humic acid slow release composite fertilizer, zinc sulfate.
Used above-mentioned raw materials is the commercially available prod in following examples, and wherein the sulfur coated urea product type is (35-0-0, S >=25%); The resin coated urea product type is (44-0-0); Humic acid slow release complex fertilizer product model is (15-8-17 contains humic acids >=10%); Above raw material has all been produced by Shandong NongDa Fertilizer Science Co., Ltd and has sold, and the numeral in its bracket is the mass percentage content of nitrogen, Vanadium Pentoxide in FLAKES, potassium oxide, is the conventional sign in this area.
The content of nitrogen, Vanadium Pentoxide in FLAKES is respectively 18%, 46% in the diammonium phosphate;
Potassium oxide content is 50% in the vitriolate of tartar;
Zinc sulfate adopts commercially available Zinc Sulphate Heptahydrate crystal, and zinc content is 21~22%, sulphur content >=10%.
The particle diameter of above-mentioned all raw materials is all in 2~4 millimeters scopes.
Embodiment one
Embodiment 1: be suitable for the two film humic acids slow-release or control-release fertilizers of the special-purpose sulphur resin of film-mulching cultivation garlic, total nutrient: the content of nitrogen, Vanadium Pentoxide in FLAKES, potassium oxide is respectively 16%, 7%, 22%, is mass percent.The raw materials quality component is following:
Resin coated urea 130
Sulfur coated urea 140
Diammonium phosphate 120
Vitriolate of tartar 380
Humic acid slow release composite fertilizer 220
Zinc sulfate 10
Above-mentioned each raw material is put into stirrer together stirred 5~10 minutes, fully mixing promptly gets.Then with the fertilizer that mixes send into metering, wrapping machine measures, packs.
Embodiment 2: be suitable for the two film humic acids slow-release or control-release fertilizers of the special-purpose sulphur resin of film-mulching cultivation garlic, total nutrient: the content of nitrogen, Vanadium Pentoxide in FLAKES, potassium oxide is respectively 17%, 9%, 19%, is mass percent.Feed composition is following:
Resin coated urea 130
Sulfur coated urea 135
Diammonium phosphate 170
Vitriolate of tartar 310
Humic acid slow release composite fertilizer 240
Zinc sulfate 15
Above-mentioned each raw material is put into stirrer together stirred 5~10 minutes, fully mixing promptly gets.Then with the fertilizer that mixes send into metering, wrapping machine measures, packs.
Embodiment 3: be suitable for the two film humic acids slow-release or control-release fertilizers of the special-purpose sulphur resin of film-mulching cultivation garlic, total nutrient: the content of nitrogen, Vanadium Pentoxide in FLAKES, potassium oxide is respectively 18%, 7%, 20%, is mass percent.Feed composition is following:
Resin coated urea 160
Sulfur coated urea 150
Diammonium phosphate 130
Vitriolate of tartar 325
Humic acid slow release composite fertilizer 225
Zinc sulfate 10
Above-mentioned each raw material is put into stirrer together stirred 5~10 minutes, fully mixing promptly gets.Then with the fertilizer that mixes send into metering, wrapping machine measures, packs.
Embodiment 4: be suitable for the two film humic acids slow-release or control-release fertilizers of the special-purpose sulphur resin of film-mulching cultivation garlic, total nutrient: the content of nitrogen, Vanadium Pentoxide in FLAKES, potassium oxide is respectively 18%, 9%, 18%, is mass percent.Feed composition is following:
Resin coated urea 165
Sulfur coated urea 140
Diammonium phosphate 160
Vitriolate of tartar 290
Humic acid slow release composite fertilizer 235
Zinc sulfate 10
Above-mentioned each raw material is put into stirrer together stirred 5~10 minutes, fully mixing promptly gets.Then with the fertilizer that mixes send into metering, wrapping machine measures, packs.
Embodiment 5: be suitable for the two film humic acids slow-release or control-release fertilizers of the special-purpose sulphur resin of film-mulching cultivation garlic,
Resin coated urea 130;
Sulfur coated urea 140;
Diammonium phosphate 120;
Vitriolate of tartar 380;
Humic acid slow release composite fertilizer 220;
Zinc sulfate 10.
Above-mentioned each raw material is put into stirrer together stirred 5~10 minutes, fully mixing promptly gets.Then with the fertilizer that mixes send into metering, wrapping machine measures, packs.
Comparative Examples: the general composite fertilizer of common vitriolate of tartar (total nutrient content 45%)+common urea (nitrogen content 46%).
The effect of above embodiment 1~5 and Comparative Examples is following:
Supplying the examination garlic cultivar is the Jinxiang garlic, and soil is cinnamon soil, the adjacent identical cultivation of areal.By equal total fertilization amount, 810 kilograms of common compound potassium sulfate fertilizers of per hectare in the Comparative Examples, 90 kilograms of urea; The fertilizer amount of the two film humic acids slow-release or control-release fertilizers of special-purpose sulphur resin is 1200 kilograms of per hectares.
Among the embodiment all special-purpose control-release fertilizers be before the garlic sowing, once to apply in the plot of planting, with the seedling of planting after the mixing with soil, during garlic is carried out routine irrigation.Compound potassium sulfate fertilizer and urea mix back 40% with the same time of special-purpose control-release fertilizer, use with method in the Comparative Examples, do to topdress for remaining 60% minute 2 times to use, and fertilizing method is fertilizer to be dissolved the back use with watering
Figure 32803DEST_PATH_IMAGE002

Claims (5)

1. one kind is suitable for the two film humic acids slow-release or control-release fertilizers of the special-purpose sulfur and resin of film-mulching cultivation garlic, it is characterized in that said fertilizer components and weight proportion are following:
Resin coated urea 130-15;
Sulfur coated urea 135-150;
Diammonium phosphate 120-170;
Vitriolate of tartar 290-380;
Humic acid slow release composite fertilizer 220-240;
Zinc sulfate 10-15.
2. slow-release or control-release fertilizer according to claim 1 is characterized in that, said fertilizer components and weight proportion are following:
Resin coated urea 130;
Sulfur coated urea 140;
Diammonium phosphate 120;
Vitriolate of tartar 380;
Humic acid slow release composite fertilizer 220;
Zinc sulfate 10.
3. the two film humic acids slow-release or control-release fertilizers of sulfur and resin according to claim 1 and 2 is characterized in that,
In the said components:
The resin coated urea model is 44-0-0, nitrogen content >=44%;
The sulfur coated urea model is 35-0-0, nitrogen content >=35%, and sulphur content is 25%;
Diammonium phosphate is a granule type, and the mass percentage content of nitrogen, Vanadium Pentoxide in FLAKES is respectively 18%, 46%;
Vitriolate of tartar is a granule type, and potassium oxide content is 50%;
Zinc sulfate adopts commercially available agricultural Zinc Sulphate Heptahydrate crystal, and zinc content is 21~22%, sulphur content >=10%;
The mass percentage content of nitrogen, Vanadium Pentoxide in FLAKES, potassium oxide is in the humic acid slow release composite fertilizer: 14%~16%, 7~9%, 16~18%, and humic acids content >=10%.
4. slow-release or control-release fertilizer according to claim 3 is characterized in that, above-mentioned humic acid slow release composite fertilizer, and the mass percentage content of nitrogen, Vanadium Pentoxide in FLAKES, potassium oxide is respectively 15%, 8%, 17%.
5. slow-release or control-release fertilizer according to claim 1 and 2 is characterized in that, said component raw material particle diameter is 2-4mm.
CN2012102630745A 2012-07-27 2012-07-27 Special sulfur-resin double-membrane humic-acid controlled release fertilizer suitable for culturing garlic with mulching film Pending CN102795945A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2012102630745A CN102795945A (en) 2012-07-27 2012-07-27 Special sulfur-resin double-membrane humic-acid controlled release fertilizer suitable for culturing garlic with mulching film

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2012102630745A CN102795945A (en) 2012-07-27 2012-07-27 Special sulfur-resin double-membrane humic-acid controlled release fertilizer suitable for culturing garlic with mulching film

Publications (1)

Publication Number Publication Date
CN102795945A true CN102795945A (en) 2012-11-28

Family

ID=47195287

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2012102630745A Pending CN102795945A (en) 2012-07-27 2012-07-27 Special sulfur-resin double-membrane humic-acid controlled release fertilizer suitable for culturing garlic with mulching film

Country Status (1)

Country Link
CN (1) CN102795945A (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103232306A (en) * 2013-05-23 2013-08-07 史丹利化肥股份有限公司 Method for preparing special fertilizer containing sulfur element for efficiently controlled release garlic
CN104692936A (en) * 2015-02-13 2015-06-10 杨树东 Fertilizer capable of improving yield of garlic
CN108383664A (en) * 2018-05-15 2018-08-10 王文杰 A kind of slow-release Radix Astragali mixing fertilizer specially
CN108947726A (en) * 2018-07-27 2018-12-07 山东省农业科学院生物技术研究中心 Fertilizer special for peanuts and preparation method thereof
CN109400391A (en) * 2018-12-27 2019-03-01 山东农大腐植酸高效利用工程技术研发有限公司 A kind of dedicated humic acid type Controlled-release nitrogen potash fertilizer material of crop

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101182259A (en) * 2007-10-31 2008-05-21 山东金正大生态工程股份有限公司 Special controlled-release fertilizer for sulfur, resin film coated ginger, garlic and manufacturing method therefor
CN101870624A (en) * 2010-06-13 2010-10-27 山东金正大生态工程股份有限公司 Rice special controlled-release fertilizer applied once in processes of rice transplantation and seedling culture and preparation method thereof
CN101891550A (en) * 2010-07-26 2010-11-24 菏泽金正大生态工程有限公司 Synchronous nutrient controlled release fertilizer special for cotton and application thereof
US20110218102A1 (en) * 2006-02-08 2011-09-08 The Andersons, Inc. Dispersable potash granule
CN102249818A (en) * 2011-05-16 2011-11-23 菏泽金正大生态工程有限公司 Organic-inorganic controlled-release fertilizer special for isatidis root and preparation method and application thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20110218102A1 (en) * 2006-02-08 2011-09-08 The Andersons, Inc. Dispersable potash granule
CN101182259A (en) * 2007-10-31 2008-05-21 山东金正大生态工程股份有限公司 Special controlled-release fertilizer for sulfur, resin film coated ginger, garlic and manufacturing method therefor
CN101870624A (en) * 2010-06-13 2010-10-27 山东金正大生态工程股份有限公司 Rice special controlled-release fertilizer applied once in processes of rice transplantation and seedling culture and preparation method thereof
CN101891550A (en) * 2010-07-26 2010-11-24 菏泽金正大生态工程有限公司 Synchronous nutrient controlled release fertilizer special for cotton and application thereof
CN102249818A (en) * 2011-05-16 2011-11-23 菏泽金正大生态工程有限公司 Organic-inorganic controlled-release fertilizer special for isatidis root and preparation method and application thereof

Non-Patent Citations (5)

* Cited by examiner, † Cited by third party
Title
刘中良等: "水培条件下硫对大蒜营养品质和鲜重的影响", 《中国农学通报》, vol. 26, no. 10, 31 December 2010 (2010-12-31), pages 207 - 211 *
张自坤等: "控释掺混肥对大蒜根际土壤微生物的影响", 《中国农学通报》, vol. 26, no. 9, 31 December 2010 (2010-12-31), pages 226 - 229 *
杨凤娟等: "硫对大蒜生理生化指标及营养品质的影响", 《应用生态学报》, vol. 15, no. 11, 31 December 2004 (2004-12-31), pages 2095 - 2098 *
闫冰洁: "硫对大蒜产量和品质的影响", 《中国优秀硕士学位论文全文数据库•农业科技辑》, no. 12, 31 December 2006 (2006-12-31) *
齐建建等: "控释掺混肥对大蒜鳞茎产量、品质和氮素利用率的影响", 《中国蔬菜》, no. 8, 31 December 2009 (2009-12-31), pages 42 - 47 *

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103232306A (en) * 2013-05-23 2013-08-07 史丹利化肥股份有限公司 Method for preparing special fertilizer containing sulfur element for efficiently controlled release garlic
CN103232306B (en) * 2013-05-23 2014-08-20 史丹利化肥股份有限公司 Method for preparing special fertilizer containing sulfur element for efficiently controlled release garlic
CN104692936A (en) * 2015-02-13 2015-06-10 杨树东 Fertilizer capable of improving yield of garlic
CN108383664A (en) * 2018-05-15 2018-08-10 王文杰 A kind of slow-release Radix Astragali mixing fertilizer specially
CN108947726A (en) * 2018-07-27 2018-12-07 山东省农业科学院生物技术研究中心 Fertilizer special for peanuts and preparation method thereof
CN109400391A (en) * 2018-12-27 2019-03-01 山东农大腐植酸高效利用工程技术研发有限公司 A kind of dedicated humic acid type Controlled-release nitrogen potash fertilizer material of crop

Similar Documents

Publication Publication Date Title
CN102267827B (en) Pollution-free high-efficiency special fertilizer for walnut
CN102795929A (en) Polymer-sulfur double coated humic acid sustained and controlled-release fertilizer dedicated for wheat
CN105198619B (en) A kind of fertilizer specially for peanut and preparation method thereof made between corn, peanut
CN106146146A (en) A kind of Special foliage fertilizer for wheat
CN101953249B (en) Fertilization method for protected tomato overwinter long-season cultivation
CN104671991A (en) Special slow-released water-soluble fertilizer for american ginseng and preparation method thereof
CN102816010A (en) Seed nursing fertilizer, method for preparing same and application of nursing fertilizer
CN115024147B (en) Fertilizing method for improving high-quality fruit rate of red crisp pears
CN102795945A (en) Special sulfur-resin double-membrane humic-acid controlled release fertilizer suitable for culturing garlic with mulching film
CN108947631A (en) A kind of promoting root growth mentions seedling functional form solid water-soluble fertilizer and the preparation method and application thereof
CN103159558A (en) Novel long-lasting special fertilizer for sugarcane and preparation method thereof
CN102795926A (en) Special sulfur and resin double-coated humic acid controlled-release fertilizer suitable for corn
CN102503702A (en) Organic potassium fertilizer for improving potassium utilization ratio and fertilizer efficiency slow release and preparation method thereof
CN103694060A (en) Corn special fertilizer under corn peanut intercropping condition and preparation method thereof
CN103641589A (en) Fertilizer special for corn and production method thereof
CN103539509A (en) Compound controlled-release fertilizer special for spring corns and production method thereof
CN102757290A (en) Polypeptide fertilizer and preparation method thereof for wheat
CN102603410B (en) Nitrogen fertilizer combination containing fulvic acid
CN106396802A (en) Composite amino acid chelated trace element water-soluble fertilizer and preparation method thereof
CN103910580B (en) Common fertilizer special for sesbania in medium and low-yield fields in Huang-Huai-Hai region
CN102795928A (en) Special sulfur and resin double-coated humic acid controlled-release fertilizer suitable for culturing potatoes in arched shed
CN100478313C (en) Special multi-nutrient control-release fertilizer for cauliflower and preparation method thereof
CN105967962A (en) Summer corn synchronous nutrition formula fertilizer
CN106242681A (en) A kind of compound fertilizer improving sugarcane yield and preparation method thereof
CN103772057B (en) A kind of chelated microelements fertilizer

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C02 Deemed withdrawal of patent application after publication (patent law 2001)
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20121128