CN102720062A - Preparation method of selvedge sizing agent - Google Patents
Preparation method of selvedge sizing agent Download PDFInfo
- Publication number
- CN102720062A CN102720062A CN2012101955330A CN201210195533A CN102720062A CN 102720062 A CN102720062 A CN 102720062A CN 2012101955330 A CN2012101955330 A CN 2012101955330A CN 201210195533 A CN201210195533 A CN 201210195533A CN 102720062 A CN102720062 A CN 102720062A
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- China
- Prior art keywords
- preparation
- selvedge
- sizing agent
- agent
- stirring
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 238000004513 sizing Methods 0.000 title abstract 5
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 35
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 claims abstract description 21
- 229920003023 plastic Polymers 0.000 claims abstract description 18
- 239000004033 plastic Substances 0.000 claims abstract description 18
- 238000003756 stirring Methods 0.000 claims abstract description 17
- 239000011347 resin Substances 0.000 claims abstract description 14
- 229920005989 resin Polymers 0.000 claims abstract description 14
- XMNIXWIUMCBBBL-UHFFFAOYSA-N 2-(2-phenylpropan-2-ylperoxy)propan-2-ylbenzene Chemical compound C=1C=CC=CC=1C(C)(C)OOC(C)(C)C1=CC=CC=C1 XMNIXWIUMCBBBL-UHFFFAOYSA-N 0.000 claims abstract description 9
- HGAZMNJKRQFZKS-UHFFFAOYSA-N chloroethene;ethenyl acetate Chemical compound ClC=C.CC(=O)OC=C HGAZMNJKRQFZKS-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000002270 dispersing agent Substances 0.000 claims abstract description 8
- 238000001914 filtration Methods 0.000 claims abstract description 4
- 239000004793 Polystyrene Substances 0.000 claims description 8
- 229920002223 polystyrene Polymers 0.000 claims description 8
- 238000004519 manufacturing process Methods 0.000 abstract description 5
- 238000000034 method Methods 0.000 abstract description 4
- 239000002994 raw material Substances 0.000 abstract description 4
- 239000002699 waste material Substances 0.000 abstract description 3
- 239000006260 foam Substances 0.000 abstract 3
- 229920006248 expandable polystyrene Polymers 0.000 abstract 2
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 18
- 239000004744 fabric Substances 0.000 description 5
- 239000003570 air Substances 0.000 description 3
- 231100000614 poison Toxicity 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 229920001893 acrylonitrile styrene Polymers 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000005022 packaging material Substances 0.000 description 2
- 230000007096 poisonous effect Effects 0.000 description 2
- SCUZVMOVTVSBLE-UHFFFAOYSA-N prop-2-enenitrile;styrene Chemical compound C=CC#N.C=CC1=CC=CC=C1 SCUZVMOVTVSBLE-UHFFFAOYSA-N 0.000 description 2
- 238000004064 recycling Methods 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000012080 ambient air Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000002788 crimping Methods 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000013467 fragmentation Methods 0.000 description 1
- 238000006062 fragmentation reaction Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 239000002341 toxic gas Substances 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 229920002554 vinyl polymer Polymers 0.000 description 1
- ORGHESHFQPYLAO-UHFFFAOYSA-N vinyl radical Chemical class C=[CH] ORGHESHFQPYLAO-UHFFFAOYSA-N 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
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Abstract
The invention discloses a preparation method of a selvedge sizing agent. The method comprises the following steps of: adding butanone, dispersing agent vinyl chloride-vinyl acetate resin and hardening agent dicumyl peroxide in a stirring barrel, and stirring uniformly; adding expandable polystyrene foam plastic in the stirring process; after charging, and continuously stirring for 20-45 minutes at 10-30 DEG C at a stirring speed of 500-1,000rpm; and filtering to obtain the selvedge sizing agent. 60-120g of the dispersing agent vinyl chloride-vinyl acetate resin, 4-6g of the hardening agent dicumyl peroxide and 300-330g of the expandable polystyrene foam plastic are added into each kilogram of butanone. Through the invention, the prepared selvedge sizing agent can completely replace the traditional selvedge sizing agent in production practice, and the preparation cost is remarkably lowered; and since the recycled foam plastic is used as a raw material, the cost is lowered, thus the preparation method disclosed by the invention turns waste into wealth and has obvious economic and social benefits.
Description
Technical field
The invention belongs to field of textiles, particularly a kind of preparation method of selvedge setting agent.
Background technology
The selvedge setting agent is the raw material that industrial knitted cloth is used for fixing selvedge when cuing open the width of cloth, plays typing, prevents the effect of crimping,
In industrial circle extensive uses such as dyeing and finishing, process hides.Traditional selvedge setting agent acrylonitrile-styrene copolymerized resin (AS) resin and toluene of adopting are allocated more, and about 3.5 ten thousand yuan/ton of AS resin market price costs an arm and a leg, and makes cost improve greatly; Toluene belongs to the bio-toxicity organic solvent, produce and use in contaminated environment not only, and have a strong impact on producers' health.
Summary of the invention
The object of the present invention is to provide a kind of preparation method of selvedge setting agent, reduce in manufacturing of traditional selvedge setting agent and the use, reduce production costs simultaneously the pollution of air.
To achieve these goals; Technical scheme provided by the invention is: a kind of preparation method of selvedge setting agent; Butanone (MEK), dispersant vinyl chloride-vinyl acetate resin and curing agent cumyl peroxide are added in the agitator; Stir and it was mixed in 3 ~ 5 minutes, progressively add polystyrene foamed plastics then while stirring; After reinforced the completion, continue to stir 20 ~ 45 minutes at 10 ~ 30 ℃, speed of agitator is 500 ~ 1000 rev/mins.Reaction finishes, and promptly obtains the selvedge setting agent after the filtration.If ambient air temperature is lower than 10 ℃, should take the measure of heat tracing.
Every 1kg butanone adds dispersant vinyl chloride-vinyl acetate resin 60 ~ 120g, curing agent cumyl peroxide 4 ~ 6g, polystyrene foamed plastics 300 ~ 330g.
Add vinyl chloride-vinyl acetate resin (VINYL) in the preparation process, regulate solution viscosity, and the cohesive force of increase and base cloth, add cumyl peroxide (DCP), strengthen the non-deformability of selvedge under 180 ℃ of environment.
Said filtration adopts 200 mesh filter screens to filter.
The polystyrene foamed plastics (EPS) that the present invention adopts can be the foamed plastics that reclaims.
Beneficial effect: the inventive method is a major ingredient with polystyrene foamed plastics (EPS); Polystyrene foamed plastics can be to reclaim foamed plastics; Replace the acrylonitrile-styrene copolymerized resin of expensive propylene, be substituted with the lower butanone of bio-toxicity and poison solvent toluene.The selvedge setting agent of preparation can tolerate 180 ℃ high temperature, in production practices, can substitute traditional selvedge setting agent fully and use, and cost of manufacture declines to a great extent, and adopting the foamed plastics that reclaims is raw material, is a practicality invention of turning waste into wealth.Have tangible economic benefit and social benefit.
Economic and Efficiency Analysis:
Tradition selvedge setting agent is a main material with AS resin and poisonous chemical solvent toluene, the about 12.8 yuan/KG of cost; This law is produced the about 8.9 yuan/KG of selvedge setting agent cost.Cut open width of cloth knitted cloth 400 myriametres year with our company, 30 tons of calculating of selvedge setting agent consumption, cost-saved 13.65 ten thousand yuan.The present invention is if be generalized to relevant industries, and economic benefits are more remarkable.
Social benefit is analyzed:
Because of poisonous chemical solvent toluene in traditional selvedge setting agent can in use all evaporate in the air, use the lower butanone of toxicity instead and then can effectively avoid the pollution of toluene surrounding air.
EPS is widely used in the internal layer packaging of electric equipment as modal amortizing packaging material, and after the use of equipment Kaifeng, packaging material lack effectively to be recycled.Can discharge black smoke poison gas again because of being difficult to degraded under its natural environment, burning, and be difficult to handle.The present invention is the effective trial to the recycling of waste plastic, meets the recycling economy thinking of current sustainable development.
Description of drawings
Fig. 1 is the preparation flow figure of selvedge setting agent provided by the invention.
The specific embodiment
Below in conjunction with accompanying drawing the present invention is done explanation further.
Embodiment 1:
The preparation method of selvedge setting agent, concrete steps are following:
1, in agitator, adds butanone 50KG, add 0.2 kilogram of dispersant vinyl chloride-vinyl acetate resin 3KG and curing agent cumyl peroxide then, stir.
3, stir on one side, Yi Bian add 16.5 kilograms polystyrene foamed plastics.
4. after reinforced the completion,, continue to stir 20 minutes down at 30 ℃ with the agitator sealing.
5, open the bleeder valve of agitator below, filter, obtain the selvedge setting agent with 200 mesh filter screens.
Embodiment 2:
The preparation method of selvedge setting agent, concrete steps are following:
1, the foamed plastics EPS that adopt to reclaim is as raw material, to the foamed plastics that reclaims sort, fragmentation, remove foreign material, the back that drains away the water is subsequent use.
2, in agitator, add butanone 50KG, add 0.3 kilogram of dispersant vinyl chloride-vinyl acetate resin 6KG and curing agent cumyl peroxide then, stir.
3, stir on one side, Yi Bian progressively add 15 kilograms recovery foamed plastics.
4. after reinforced the completion,, continue to stir 45 minutes at 10 ℃ with the agitator sealing.
5, open the bleeder valve of agitator below, filter, obtain the selvedge setting agent with 200 mesh filter screens.
Claims (3)
1. the preparation method of a selvedge setting agent; It is characterized in that: butanone, dispersant vinyl chloride-vinyl acetate resin and curing agent cumyl peroxide are added in the agitator; Stir and it was mixed in 3 ~ 5 minutes, add polystyrene foamed plastics then while stirring; After reinforced the completion, continue to stir 20 ~ 45 minutes at 10 ~ 30 ℃, speed of agitator is 500 ~ 1000 rev/mins, filters, and obtains the selvedge setting agent.
2. the preparation method of a kind of selvedge setting agent according to claim 1 is characterized in that: every 1kg butanone adds dispersant vinyl chloride-vinyl acetate resin 60 ~ 120g, curing agent cumyl peroxide 4 ~ 6g, polystyrene foamed plastics 300 ~ 330g.
3. the preparation method of a kind of selvedge setting agent according to claim 1 is characterized in that: said filtration adopts 200 mesh filter screens to filter.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210195533.0A CN102720062B (en) | 2012-06-14 | 2012-06-14 | Preparation method of selvedge sizing agent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210195533.0A CN102720062B (en) | 2012-06-14 | 2012-06-14 | Preparation method of selvedge sizing agent |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102720062A true CN102720062A (en) | 2012-10-10 |
| CN102720062B CN102720062B (en) | 2014-01-15 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210195533.0A Active CN102720062B (en) | 2012-06-14 | 2012-06-14 | Preparation method of selvedge sizing agent |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106702736A (en) * | 2016-12-28 | 2017-05-24 | 湖州品创孵化器有限公司 | Setting agent used after wool stretch and refinement |
| CN106758189A (en) * | 2016-12-28 | 2017-05-31 | 湖州多恒服饰有限公司 | A kind of selvedge sizing agent |
| CN106758190A (en) * | 2016-12-28 | 2017-05-31 | 湖州品创孵化器有限公司 | A kind of setting agent after the stretching for wool fiber |
| CN107399958A (en) * | 2017-08-08 | 2017-11-28 | 湖南省醴陵市玉果电瓷有限公司 | A kind of porcelain bushing shell and preparation method thereof |
| CN107512901A (en) * | 2017-08-16 | 2017-12-26 | 顾玉城 | A kind of porcelain bushing and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1059383A (en) * | 1991-08-09 | 1992-03-11 | 王祥森 | Knit cap formula of hardening agent and manufacture methods thereof such as crudefiber crop, careless class, paper-straws |
| CN1082587A (en) * | 1992-07-17 | 1994-02-23 | 福建师范大学 | A kind of polystyrene adhesive and production method thereof |
| CN1239131A (en) * | 1999-07-06 | 1999-12-22 | 董金狮 | Dissolving-fusing modification of EPS and process for preparing adhesive |
| CN1659244A (en) * | 2002-06-05 | 2005-08-24 | 巴斯福股份公司 | Printing and coating compositions containing expandable polystyrene |
-
2012
- 2012-06-14 CN CN201210195533.0A patent/CN102720062B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1059383A (en) * | 1991-08-09 | 1992-03-11 | 王祥森 | Knit cap formula of hardening agent and manufacture methods thereof such as crudefiber crop, careless class, paper-straws |
| CN1082587A (en) * | 1992-07-17 | 1994-02-23 | 福建师范大学 | A kind of polystyrene adhesive and production method thereof |
| CN1239131A (en) * | 1999-07-06 | 1999-12-22 | 董金狮 | Dissolving-fusing modification of EPS and process for preparing adhesive |
| CN1659244A (en) * | 2002-06-05 | 2005-08-24 | 巴斯福股份公司 | Printing and coating compositions containing expandable polystyrene |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106702736A (en) * | 2016-12-28 | 2017-05-24 | 湖州品创孵化器有限公司 | Setting agent used after wool stretch and refinement |
| CN106758189A (en) * | 2016-12-28 | 2017-05-31 | 湖州多恒服饰有限公司 | A kind of selvedge sizing agent |
| CN106758190A (en) * | 2016-12-28 | 2017-05-31 | 湖州品创孵化器有限公司 | A kind of setting agent after the stretching for wool fiber |
| CN107399958A (en) * | 2017-08-08 | 2017-11-28 | 湖南省醴陵市玉果电瓷有限公司 | A kind of porcelain bushing shell and preparation method thereof |
| CN107512901A (en) * | 2017-08-16 | 2017-12-26 | 顾玉城 | A kind of porcelain bushing and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102720062B (en) | 2014-01-15 |
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| C06 | Publication | ||
| PB01 | Publication | ||
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| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A preparation method of selvage setting agent Effective date of registration: 20200812 Granted publication date: 20140115 Pledgee: Jiangsu Credit Financing Guarantee Co.,Ltd. Pledgor: NANTONG YIHUA PLASTIC Co.,Ltd. Registration number: Y2020980004916 |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| CP03 | Change of name, title or address |
Address after: 226371 group 3, East, Sun Li Qiao Cun, Xingdong Town, Tongzhou District, Nantong City, Jiangsu Province Patentee after: Yihua high tech materials (Nantong) Co.,Ltd. Address before: 226300 No.18, sunliqiao Industrial Park, Xingdong Town, Tongzhou District, Nantong City, Jiangsu Province Patentee before: NANTONG YIHUA PLASTIC Co.,Ltd. |
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Date of cancellation: 20210930 Granted publication date: 20140115 Pledgee: Jiangsu Credit Financing Guarantee Co.,Ltd. Pledgor: NANTONG YIHUA PLASTIC Co.,Ltd. Registration number: Y2020980004916 |
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| PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A preparation method of edge setting agent Effective date of registration: 20211027 Granted publication date: 20140115 Pledgee: Jiangsu Zaibao South communication Financing Guarantee Co.,Ltd. Pledgor: Yihua high tech materials (Nantong) Co.,Ltd. Registration number: Y2021980011384 |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20221018 Granted publication date: 20140115 Pledgee: Jiangsu Zaibao South communication Financing Guarantee Co.,Ltd. Pledgor: Yihua high tech materials (Nantong) Co.,Ltd. Registration number: Y2021980011384 |
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| PC01 | Cancellation of the registration of the contract for pledge of patent right |