CN102703214B - Spice for cigarettes and extracting method and application thereof - Google Patents
Spice for cigarettes and extracting method and application thereof Download PDFInfo
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- CN102703214B CN102703214B CN201210157973.7A CN201210157973A CN102703214B CN 102703214 B CN102703214 B CN 102703214B CN 201210157973 A CN201210157973 A CN 201210157973A CN 102703214 B CN102703214 B CN 102703214B
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- silkworm excrement
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Abstract
The invention relates to spice for cigarettes and an extracting method and application of the spice, belonging to the technical field of tobacco processing, wherein the spice for the cigarettes is a solvent extract of silkworm excrement waste liquid obtained by extracting chlorophyll from the silkworm excrement; solvent is water, ethanol, acetone or methylene dichloride; the extracting method comprises the following steps: carrying out distillation and extraction to the silkworm excrement waste liquid obtained by extracting chlorophyll from the silkworm excrement for 2-5 hours by water, ethanol, acetone or methylene dichloride, and obtaining the spice after removing the solvent. According to the application of the spice for the cigarettes, the spice is used for flavoring the tobacco; dosage of the spice is 0.025-0.1% of tobacco shred weight; by dint of assay determination, the spice provided by the invention mainly contains twenty-odd aromatic matters such as irisone, furanone, isophorone, jasmine, phytol, phosphate, cyclohexanol and the like; these matters are added to cigarette tobacco shred, so that smoke sweet degree of the cigarettes can be improved obviously; sweet-back engender liquid of cigarette smoke is improved; smoke is softened; and aftertaste is improved. Simultaneously, the silkworm excrement waste liquid obtained by extracting chlorophyll from the silkworm excrement is changed from waste material into things of value; and resource is utilized fully.
Description
Technical field
The invention belongs to tobacco flavoring technical field, relate to a kind of from industrial waste---extract the tobacco aromatics using that silkworm excrement chlorophyll extracts in useless, also relate to extracting method and the application of this tobacco aromatics using simultaneously.
Background technology
Silkworm excrement is China's traditional Chinese medicine among the people, and its taste is sweet, pungent, warm in nature, nontoxic, have dispel rheumatism, the function of removing heat to brighten vision, the analgesic therapy of invigorating blood circulation.Along with the development of technology, silkworm excrement has become the chlorophyllous important source material of industrial extraction.Yet, extract after chlorophyll, in silkworm excrement waste liquid, also contain a large amount of pectin, protein and other abundant beneficiating ingredients.At present, enterprise is conventionally just extracted and is applied in the fields such as medicine, beverage or livestock-raising pectin and protein wherein, and surplus materials directly abandons, and has caused great stock number expense.
Summary of the invention
The object of the invention is, for a kind of tobacco aromatics using is provided, also provides extracting method and the application approach of this tobacco aromatics using simultaneously.
Based on above-mentioned purpose, the invention provides following technical scheme:
A tobacco aromatics using, is the solvent extractable matter that extracts the silkworm excrement waste liquid after chlorophyll, and described solvent is water, ethanol, acetone or methylene dichloride.
The extracting method of described tobacco aromatics using, step is: water, ethanol, acetone or methylene dichloride, to extracting the silkworm excrement waste liquid while distillation extraction 2 ~ 5h after chlorophyll, obtain described spices except after desolventizing.
The application of described tobacco aromatics using, be by described spices for tobacco flavoring, its consumption is the 0.025-0.1% of pipe tobacco weight.
By described spices directly or with being sprayed onto in pipe tobacco after alcohol dilution.
Measure by analysis, in tobacco aromatics using provided by the present invention, mainly contain jononeionone, furanone, isophorone, jasmone, phytol, phosphoric acid ester, hexalin etc. more than 20 and plant fragrance matter, added in cigarette shreds, can obviously improve the sweet degree of cigarette smoke, increase the fragrant Hui Tian of the cigarette sense of promoting the production of body fluid, soft flue gas also improves pleasant impression.
Extracting method provided by the present invention is mainly from the angle of environment, resource, the silkworm excrement waste liquid extracting after chlorophyll is turned waste into wealth, resource is fully utilized, simultaneously, this method also has the advantages such as simple to operate, extraction yield is high, has very strong operability and market potential.The application providing is also very convenient, can not produce burden to existing Cigarette processing technique, can under the prerequisite that keeps the existing performance of cigarette, promote cigarette look sucking quality.
Embodiment
Below in conjunction with specific embodiment, the invention will be further described.
embodiment 1:to while distilling and extracting device one end, add 500ml to extract silkworm excrement waste liquid and a little zeolite after chlorophyll, use electric mantle heated and boiled; The device the other end (receiving end) fills 15mL methylene dichloride, with 60 ℃ of heating in water bath, and while distillation extraction 3h; With rotatory evaporator, steam except the methylene dichloride in extraction liquid, gained spices is placed in and in brown bottle, seals stored refrigerated.
Gained spices is diluted to 5% with dehydrated alcohol, and the ratio (spices consumption be pipe tobacco weight 0.025%) that adds 5g diluent according to every 1000g pipe tobacco evenly sprays in pipe tobacco, after placing 2h under room temperature and absorbing according to normal process cigarette.
embodiment 2:to while distilling and extracting device one end, add 500ml to extract silkworm excrement waste liquid and a little zeolite after chlorophyll, use electric mantle heated and boiled; Device receiving end fills 15mL ethanol, with 85 ℃ of heating in water bath, and while distillation extraction 2h; With rotatory evaporator, steam except the ethanol in extraction liquid, gained spices is placed in and in brown bottle, seals stored refrigerated.
Gained spices is diluted to 10% with dehydrated alcohol, and the ratio (spices consumption be pipe tobacco weight 0.05%) that adds 5g diluent according to every 1000g pipe tobacco evenly sprays in pipe tobacco, after placing 2h under room temperature and absorbing according to normal process cigarette.
embodiment 3:to while distilling and extracting device one end, add 500ml to extract silkworm excrement waste liquid and a little zeolite after chlorophyll, use electric mantle heated and boiled; Device receiving end fills 20mL acetone, with 65 ℃ of heating in water bath, and while distillation extraction 5h; With rotatory evaporator, steam except the acetone in extraction liquid, gained spices is placed in and in brown bottle, seals stored refrigerated.
The ratio that adds 1g spices according to 1000g pipe tobacco, evenly sprays into gained spices in pipe tobacco, after placing 2h under room temperature and absorbing according to normal process cigarette.
the experiment of smokeing panel test:
Embodiment 3 gained spices are added in pipe tobacco according to the applied amount of 0.025wt%, 0.05wt%, 0.1wt% respectively, make three groups of samples, take that what do not add this spices is control sample, carry out respectively sense organ evaluation and test, evaluation result is in Table 1.The test-results of table 1 confirms, tobacco aromatics using of the present invention has increases fragrance matter, improve the sweet degree of flue gas, increase Hui Tian promote the production of body fluid sense, soft flue gas and improve the effect of pleasant impression.
Claims (4)
1. a tobacco aromatics using, is characterized in that, this spices is the solvent extractable matter that extracts the silkworm excrement waste liquid after chlorophyll, and described solvent is water, ethanol, acetone or methylene dichloride.
2. the extracting method of tobacco aromatics using described in claim 1, is characterized in that, step is: water, ethanol, acetone or methylene dichloride, to extracting the silkworm excrement waste liquid while distillation extraction 2 ~ 5h after chlorophyll, obtain described spices except after desolventizing.
3. the application of tobacco aromatics using described in claim 1, is characterized in that, by described spices, for tobacco flavoring, its consumption is the 0.025-0.1% of pipe tobacco weight.
4. application as claimed in claim 3, is characterized in that, by described spices directly or with being sprayed onto in pipe tobacco after alcohol dilution.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210157973.7A CN102703214B (en) | 2012-05-21 | 2012-05-21 | Spice for cigarettes and extracting method and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210157973.7A CN102703214B (en) | 2012-05-21 | 2012-05-21 | Spice for cigarettes and extracting method and application thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102703214A CN102703214A (en) | 2012-10-03 |
| CN102703214B true CN102703214B (en) | 2014-03-19 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210157973.7A Active CN102703214B (en) | 2012-05-21 | 2012-05-21 | Spice for cigarettes and extracting method and application thereof |
Country Status (1)
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| CN (1) | CN102703214B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103131538B (en) * | 2013-03-04 | 2014-05-21 | 湖北中烟工业有限责任公司 | Beer distillation substrate preparation method used for cigarette and application of the preparation method in cigarette |
| RU2593967C1 (en) * | 2015-04-20 | 2016-08-10 | Олег Иванович Квасенков | Method for production of hookah smoking composition |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1696130A (en) * | 2005-06-03 | 2005-11-16 | 四川通世达实业集团生物科技制品有限公司 | Method for continuous extracting chlorophyll from silkworm dropping |
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2012
- 2012-05-21 CN CN201210157973.7A patent/CN102703214B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1696130A (en) * | 2005-06-03 | 2005-11-16 | 四川通世达实业集团生物科技制品有限公司 | Method for continuous extracting chlorophyll from silkworm dropping |
Non-Patent Citations (2)
| Title |
|---|
| 程向红等.蚕沙提取物挥发性成分分析及在卷烟中的应用.《江苏农业科学》.2011,(第04期), |
| 蚕沙提取物挥发性成分分析及在卷烟中的应用;程向红等;《江苏农业科学》;20111231(第04期);第395-397页 * |
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| CN102703214A (en) | 2012-10-03 |
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Address after: 450000 Yulin South Road, Henan, Zheng Dong, No. 16 South Road, Zhengzhou Patentee after: China Tobacco Henan Industrial Co., Ltd. Address before: 450000 Zhengzhou agricultural road, Henan, No. 29 Patentee before: China Tobacco Henan Industrial Co., Ltd. |