CN102677785A - Styrene-ethylene-butylene-styrene (SEBS) self-adhesion waterproof plate and production method thereof - Google Patents
Styrene-ethylene-butylene-styrene (SEBS) self-adhesion waterproof plate and production method thereof Download PDFInfo
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- CN102677785A CN102677785A CN2012101315565A CN201210131556A CN102677785A CN 102677785 A CN102677785 A CN 102677785A CN 2012101315565 A CN2012101315565 A CN 2012101315565A CN 201210131556 A CN201210131556 A CN 201210131556A CN 102677785 A CN102677785 A CN 102677785A
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Abstract
The invention relates to a styrene-ethylene-butylene-styrene (SEBS) self-adhesion waterproof plate and a production method thereof and belongs to the field of building waterproof materials. A coiled material is composed of layers of a separation layer, an SEBS self-adhesion glue layer and a substrate, the production method includes firstly adding an SEBS elastomer and a rubber, adding a tackifier, a resin and a softening agent, stirring the mixture for 2.5-4 hours at the temperature of 140 DEG C-180 DEG C, performing swelling and blending, using a guide cylinder of a power shearing device for dispersing, and adding and stirring rest rubbers, the tackifier and functional auxiliaries to obtain an even and stable thick rubber and plastic mixing modified viscoelasticity composition-SEBS self-adhesion glue liquid; reducing the temperature to 140 DEG C to 160 DEG C for standby application; coating the cooled SEBS self-adhesion glue liquid on the substrate to form the SEBS self-adhesion glue layer; and covering the separation layer which is used for separating materials from being adhered. According to the SEBS self-adhesion waterproof plate and the production method thereof, the problems of insecure adhesion, bugling foaming, water escaping, leakage and the like are solved.
Description
Technical field
The present invention relates to a kind of non-asphaltic base self-adhesion splash guard and production method thereof, belong to the architectural waterproof material field.
Background technology
At present, waterproofing materials is divided into waterproof roll, water-repellent paint, leak stopping water material, rigid waterproofing and encapsulant five big classes usually.For large-area waterproof construction, waterproof roll is the preferred material of passing through.Traditional asphaltic base waterproof roll; All be with high-polymer modified pitch or be referred to as the waterproof roll that the polymer modified asphalt manufacturing forms; Like SBS modified asphalt waterproof coiled material, APP modified asphalt waterproof coiled material, self-adhering polymer modification bitumen waterproof roll, bridge surface waterproof layer with polymer modified bituminous waterproof sheet material etc.; They adopt hot melt or self-adhesion to construct, and they have played enormous function on the performance water-proof function, but the material of these traditional asphalt modification classes is under normal the use; Be generally its service life 25 years to 30 years, and be difficult to reach and building synchronous situation in application life; In addition, the blackbase of coiled material and concrete structure caking property are influenced greatly by constructor's skill operation, base treatment agent quality and construction environment during construction, and the difficult quality unanimity reaches the job specfication requirement efficiently.So often occur that bonding is not firm, hollowing, bubble, scurry problem such as seepage.
Summary of the invention
The technical problem that the present invention will solve provides the SEBS self-adhesion splash guard of a kind of pre-spread/wet shop of a kind of long service life good water-proof effect and easy construction, also discloses the production method of this SEBS self-adhesion splash guard simultaneously.
The present invention realizes through following technical scheme:
A kind of SEBS self-adhesion splash guard, this coiled material contains following each layer: separation layer, SEBS self-adhesion glue-line, base material at least simultaneously are covered with SEBS self-adhesion glue-line and separation layer successively on the base material.
Said base material is a macromolecular sheet material, its core thickness ≮ 0.5mm.
Said macromolecular sheet material can be materials such as TPO, EVA, ECB, CPE, PVC, is divided into homogeneous sheet and composite sheet.
Said macromolecular sheet material is a composite sheet, and it simultaneously is SEBS self-adhesion glue-line and separation layer, on the nonwoven that another side covers suspender belt can be arranged.
Said base material is a geomembrane, its core thickness ≯ 0.5mm.
Said geomembrane is a cloth one film.
Said geomembrane is two cloth, one films.
On the nonwoven of said two cloth, one film is SEBS self-adhesion glue-line and separation layer, on the nonwoven of another side suspender belt can be arranged.
Said separation layer is PE barrier film or silicone oil paper or the special-purpose antiseized barrier coat that is coated with the PET barrier film of silicone oil or is coated with silicone oil;
The invention still further relates to the production method of SEBS self-adhesion splash guard:
Earlier with SEBS elastic body, 1/2 amount rubber; 1/2 amount tackifier, resin and softening agent add agitated reactor; Under 140～180 ℃ of conditions, stirred 2.5～4 hours, the swelling mixing is led jar dispersion one time through powerful shearing equipment then; Add residue rubber, tackifier and auxiliary agent again and stir, obtain the viscoelastic composition-SEBS self-adhesive liquid of uniform and stable thick rubber plastic blend modification at last; Be cooled to 140～160 ℃ for use;
SEBS self-adhesive liquid after the cooling is coated on the base material, forms SEBS self-adhesion glue-line;
Outside SEBS self-adhesion glue-line, cover the separation layer of isolated material with anti-stick.
The styrene weight content 30～40% of described SEBS;
Described softening agent is a rubber processing oil;
Described rubber is butyl rubber, butadiene-styrene rubber, natural rubber;
Described resin is vistanex, modified polyolefin resin;
Described auxiliary agent comprises age resistor, filler, tackifier, functional aid;
Described functional aid is the copolymer that acid anhydrides or ester group functional group are arranged;
Described filler comprises dicalcium powder, French chalk or flake asbestos, mineral powder, fine particle calcium carbonate, kieselguhr, swell soil etc.;
Said macromolecular sheet material can be materials such as TPO, EVA, ECB, CPE, PVC, is divided into homogeneous sheet and composite sheet.
Said macromolecular sheet material is a composite sheet, and it simultaneously is SEBS self-adhesion glue-line and separation layer, on the nonwoven that another side covers suspender belt can be arranged.
Said base material is a geomembrane, its core thickness ≯ 0.5mm.
Said geomembrane is a cloth one film.
Said geomembrane is two cloth, one films.
On the nonwoven of said two cloth, one film is SEBS self-adhesion glue-line and separation layer, on the nonwoven of another side suspender belt can be arranged.
Said separation layer is PE barrier film or silicone oil paper or the special-purpose antiseized barrier coat that is coated with the PET barrier film of silicone oil or is coated with silicone oil;
The invention still further relates to the production method of SEBS self-adhesion splash guard:
Earlier with SEBS elastic body, 1/2 amount rubber; 1/2 amount tackifier, resin and softening agent add agitated reactor; Under 140～180 ℃ of conditions, stirred 2.5～4 hours, the swelling mixing is led jar dispersion one time through powerful shearing equipment then; Add residue rubber, tackifier and auxiliary agent again and stir, obtain the viscoelastic composition-SEBS self-adhesive liquid of uniform and stable thick rubber plastic blend modification at last; Be cooled to 140～160 ℃ for use;
SEBS self-adhesive liquid after the cooling is coated on the base material, forms SEBS self-adhesion glue-line;
Outside SEBS self-adhesion glue-line, cover the separation layer of isolated material with anti-stick.
The styrene weight content 30～40% of described SEBS;
Described softening agent is a rubber processing oil;
Described rubber is butyl rubber, butadiene-styrene rubber, natural rubber;
Described resin is vistanex, modified polyolefin resin;
Described auxiliary agent comprises age resistor, filler, tackifier, functional aid;
Described functional aid is the copolymer that acid anhydrides or ester group functional group are arranged;
Described filler comprises dicalcium powder, French chalk or flake asbestos, mineral powder, fine particle calcium carbonate, kieselguhr, swell soil etc.;
The SEBS weight content is 2～8% in the described SEBS self-adhesive liquid; The weight content of rubber is 15～24%; The weight content of resin is 3～6%; The weight content of auxiliary agent is 45～47%; All the other are softening agent content.
The weight ratio of SEBS and softening agent is 1: 3～13.
The SEBS self-adhesion splash guard of this structure and the SEBS self-adhesion splash guard long service life that adopts this production method to obtain, good water-proof effect and easy construction, bonding firmly, not hollowing, non-foaming, do not have problems such as scurrying seepage.
Description of drawings
Fig. 1 is the structural representation of the macromolecular sheet material single face SEBS self-adhesion splash guard of homogeneous sheet for base material.
Fig. 2 is the structural representation of single face SEBS self-adhesion splash guard of the macromolecular sheet material of composite sheet for base material
Fig. 3 is the structural representation of two-sided SEBS self-adhesion splash guard of the macromolecular sheet material of homogeneous sheet for base material.
Fig. 4 is geomembrane for base material and is the structural representation of the single face SEBS self-adhesion splash guard of a cloth one film.
Fig. 5 is geomembrane for base material and is the structural representation of the two-sided SEBS self-adhesion splash guard of two cloth, one film.
The specific embodiment
With reference to Fig. 1, base material is to be followed successively by SEBS self-adhesion glue-line 3 and separation layer 4 on the macromolecular sheet material 1 of homogeneous sheet.
With reference to Fig. 2, base material is the single face SEBS self-adhesion splash guard of the macromolecular sheet material of composite sheet, and suspender belt 25 is arranged on the nonwoven 22, and the another side of macromolecular sheet material 21 is followed successively by SEBS self-adhesion glue-line 23 and separation layer 24.
With reference to Fig. 3, base material is the two-sided SEBS self-adhesion splash guard of the macromolecular sheet material 31 of homogeneous sheet, and the two sides symmetry has SEBS self-adhesion glue-line 33 and separation layer 34 on the macromolecular sheet material 31.
With reference to Fig. 4, base material is geomembrane and is the single face SEBS self-adhesion splash guard of a cloth one film 41 that the one side of geomembrane can have suspender belt 45 for there not being anti-cloth 42 on the nonwoven 42, and another side is followed successively by SEBS self-adhesion glue-line 43 and separation layer 44.
With reference to Fig. 5, base material is geomembrane and is the two-sided SEBS self-adhesion splash guard of two cloth, one film that 51 two symmetries of geomembrane have or not anti-cloth 52, SEBS self-adhesion glue-line 53 and separation layer 54.
The production method of SEBS self-adhesion splash guard:
Embodiment 1: get SEBS elastic body weight content earlier and be 2%, rubber adds 11.5%, tackifier add 20%, resin 5% stirred 2.5 hours under 140～180 ℃ of conditions with softening agent 26%; The swelling mixing; Lead jar dispersion one time through powerful shearing equipment then; Add residue rubber 11.5%, tackifier 20%, age resistor 1.5% and functional aid 2.5% again and stir, obtain the viscoelastic composition-SEBS self-adhesive liquid of uniform and stable thick rubber plastic blend modification at last; Be cooled to 145 ℃ for use;
SEBS self-adhesive liquid after the cooling is coated on the base material, forms SEBS self-adhesion glue-line;
Outside SEBS self-adhesion glue-line, cover the separation layer of isolated material with anti-stick.
Embodiment 2: get SEBS elastic body weight content earlier and be 5%, rubber adds 9.5%; Tackifier adding 19%, resin 4% stirred 2.5 hours under 140～180 ℃ of conditions with softening agent 26%; The swelling mixing; Lead jar dispersion one time through powerful shearing equipment then; Add residue rubber 9.5%, tackifier 19%, age resistor 1% again, filler 4%, functional aid 3% stir, and obtain the viscoelastic composition-SEBS self-adhesive liquid of uniform and stable thick rubber plastic blend modification at last; Be cooled to 150 ℃ for use;
SEBS self-adhesive liquid after the cooling is coated on the base material, forms SEBS self-adhesion glue-line;
Outside SEBS self-adhesion glue-line, cover the separation layer of isolated material with anti-stick.
Embodiment 3: get SEBS elastic body weight content earlier and be 8%, rubber adds 7.5%; Tackifier adding 15.5%, resin 4% stirred 2.5 hours under 140～180 ℃ of conditions with softening agent 27%; The swelling mixing; Lead jar dispersion one time through powerful shearing equipment then; Add residue rubber 7.5%, tackifier 15.5%, age resistor 1% again, filler 10%, functional aid 4% stir, and obtain the viscoelastic composition-SEBS self-adhesive liquid of uniform and stable thick rubber plastic blend modification at last; Be cooled to 160 ℃ for use;
SEBS self-adhesive liquid after the cooling is coated on the base material, forms SEBS self-adhesion glue-line;
Outside SEBS self-adhesion glue-line, cover the separation layer of isolated material with anti-stick.
Claims (15)
1. SEBS self-adhesion splash guard is characterized in that this coiled material contains following each layer: separation layer, SEBS self-adhesion glue-line, base material, on the said base material at least one side be covered with SEBS self-adhesion glue-line and separation layer successively.
2. SEBS self-adhesion splash guard according to claim 1 is characterized in that: base material is a macromolecular sheet material, its core thickness ≮ 0.5mm.
3. SEBS self-adhesion splash guard according to claim 2, it is characterized in that: said macromolecular sheet material can be materials such as TPO, EVA, ECB, CPE, PVC, is divided into homogeneous sheet and composite sheet.
4. according to claim 1,3 described SEBS self-adhesion splash guards, it is characterized in that: macromolecular sheet material is a composite sheet, and it simultaneously is SEBS self-adhesion glue-line and separation layer, on the nonwoven that another side covers suspender belt can be arranged.
5. SEBS self-adhesion splash guard according to claim 1 is characterized in that: base material is a geomembrane, its core thickness ≯ 0.5mm.
6. SEBS self-adhesion splash guard according to claim 5 is characterized in that: said geomembrane is a cloth one film.
7. SEBS self-adhesion splash guard according to claim 5 is characterized in that: said geomembrane is two cloth, one films.
8. according to claim 1,7 described SEBS self-adhesion splash guards, it is characterized in that: being on the nonwoven of two cloth, one film SEBS self-adhesion glue-line and separation layer can have suspender belt on the nonwoven of another side.
9. according to claim 1,2,3,5,6 or 7 described SEBS self-adhesion splash guards, it is characterized in that: said separation layer is PE barrier film or silicone oil paper or the special-purpose antiseized barrier coat that is coated with the PET barrier film of silicone oil or is coated with silicone oil.
10. the production method of a SEBS self-adhesion splash guard; It is characterized in that: earlier SEBS elastic body, rubber, resin and softening agent were stirred 1.5～3 hours under 140～180 ℃ of conditions; The swelling mixing; Lead jar dispersion 1～2 hour through powerful shearing equipment then, add the residue auxiliary agent again and stir, obtain the viscoelastic composition-SEBS self-adhesive liquid of uniform and stable thick rubber plastic blend modification at last;
Be cooled to 140～160 ℃ for use;
SEBS self-adhesive liquid after the cooling is coated on the base material, forms SEBS self-adhesion glue-line;
Outside SEBS self-adhesion glue-line, cover the separation layer of isolated material with anti-stick.
11. the production method of a kind of SEBS self-adhesion splash guard according to claim 10 is characterized in that: the styrene weight content 30～40% of described SEBS;
Described softening agent is a rubber processing oil;
Described rubber is butyl rubber, butadiene-styrene rubber, natural rubber;
Described resin is vistanex, modified polyolefin resin;
Described auxiliary agent comprises age resistor, filler, tackifier, functional aid.
12. the production method of a kind of SEBS self-adhesion splash guard according to claim 11 is characterized in that: described functional aid is the copolymer that acid anhydrides or ester group functional group are arranged.
13. the production method of a kind of SEBS self-adhesion splash guard according to claim 11 is characterized in that: described filler comprises dicalcium powder, French chalk or flake asbestos, mineral powder, fine particle calcium carbonate, kieselguhr, swell soil.
14. the production method according to claim 10 or 11 described a kind of SEBS self-adhesion splash guards is characterized in that: the SEBS weight content is 2～8% in the described SEBS self-adhesive liquid; The weight content of rubber is 15～24%; The weight content of resin is 3～6%; The weight content of auxiliary agent is 45～47%; All the other are softening agent content.
15. the production method of a kind of SEBS self-adhesion splash guard according to claim 14 is characterized in that: the weight ratio of SEBS and softening agent is 1: 3～13.
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| CN201210131556.5A CN102677785B (en) | 2012-04-21 | 2012-04-21 | Styrene-ethylene-butylene-styrene (SEBS) self-adhesion waterproof plate and production method thereof |
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| CN201210131556.5A CN102677785B (en) | 2012-04-21 | 2012-04-21 | Styrene-ethylene-butylene-styrene (SEBS) self-adhesion waterproof plate and production method thereof |
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| CN102677785B CN102677785B (en) | 2015-06-17 |
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| WO2014110960A1 (en) * | 2013-01-15 | 2014-07-24 | 江苏凯伦建材股份有限公司 | Macromolecule wet-paving waterproof coiled material |
| CN104086908A (en) * | 2014-06-19 | 2014-10-08 | 蚌埠市光华金属制品有限公司 | Preparation method for unvulcanized butyl rubber waterproof coil |
| CN104441816A (en) * | 2014-11-17 | 2015-03-25 | 潍坊市宏源防水材料有限公司 | Macromolecular self-adhesive glue film coiled material adopting SEBS self-adhesive glue as self-adhesive layer and production method of macromolecular self-adhesive glue film coiled material |
| CN104476878A (en) * | 2014-11-19 | 2015-04-01 | 上海东方雨虹防水技术有限责任公司 | Flexible self-adhesive thermoplastic polyolefin waterproof coil material and preparation method thereof |
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| CN104742431A (en) * | 2014-08-19 | 2015-07-01 | 吴华林 | Macromolecular elastic self-sticking waterproof coiled material |
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| CN105017983A (en) * | 2015-07-16 | 2015-11-04 | 广东禹能建材科技股份有限公司 | Non-asphalt multifunctional waterproof coiled material laminated adhesive and application thereof, and non-asphalt multifunctional waterproof coiled material |
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| CN109971386A (en) * | 2017-12-28 | 2019-07-05 | 科建高分子材料（上海）股份有限公司 | A kind of fiberglass aluminum foil grid cloth waterproof roll with butyl self-adhesive layer |
| CN108340637A (en) * | 2018-02-25 | 2018-07-31 | 厦门力嘉诚防水工程有限公司 | A kind of graphene self-adhesion glued membrane root-resistance waterproof coiled material |
| CN112026309A (en) * | 2019-08-09 | 2020-12-04 | 乐清市川嘉电气科技有限公司 | Processing technology of impervious bentonite waterproof blanket |
| CN110984360A (en) * | 2019-11-21 | 2020-04-10 | 清远肆柒柒新材料科技有限公司 | Anti-leakage building prefabricated member |
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