CN102675709A - Color masterbatch and preparation method thereof - Google Patents
Color masterbatch and preparation method thereof Download PDFInfo
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- CN102675709A CN102675709A CN2011100533163A CN201110053316A CN102675709A CN 102675709 A CN102675709 A CN 102675709A CN 2011100533163 A CN2011100533163 A CN 2011100533163A CN 201110053316 A CN201110053316 A CN 201110053316A CN 102675709 A CN102675709 A CN 102675709A
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Abstract
An object of the invention is to disclose a color masterbatch and a preparation method thereof. The color masterbatch comprises the following components of, by weight, 60%-70% of a thermoplastic resin, 5%-10% of an additive and 25%-30% of a pigment. The color masterbatch prepared by the above components has the characteristics of good temperature resistance, excellent dispersion property and high dimension stability of products, is widely applied for coloring plastic caps and other injection products, and realizes the object of the invention.
Description
Technical field
The present invention relates to a kind of Masterbatch and preparation method thereof, particularly a kind of painted Masterbatch of plastic bottle closure and preparation method thereof that is applied to.
Background technology
Masterbatch is by a high proportion of pigment or additive and thermoplastic resin, and through the plastic colorant that good distribution forms, its resin of selecting for use has good wet and dissemination to tinting material, and with had good consistency by coloured material.That is: pigment+carrier+additive=Masterbatch.
What existing Masterbatch technical matters generally adopted is wet processing.The Masterbatch material forms through water grinding, phase inversion, washing, drying, granulation, and only in this way quality product just can be guaranteed.Pigment also should carry out a series of Masterbatch technology for detection in milled processed in addition, like projects such as fineness, the diffusion of measuring the sand milling slurries of measuring the sand milling slurries, the solids content of measuring the sand milling slurries and mensuration mill base fineness.
The shortcoming that existing Masterbatch exists is: resistance to elevated temperatures is poor, dispersion is inhomogeneous, the toner point is arranged;
In sum, to the defective of prior art, need a kind of Masterbatch and preparation method thereof especially, with the problem of mentioning more than solving.
Summary of the invention
The present invention aims to provide a kind of Masterbatch and preparation method thereof, to the defective of above-mentioned prior art, solves the deficiency that PE plastics and bottle cap thermal contraction exist.
For realizing above-mentioned purpose, the technical problem that the present invention solved can adopt following technical scheme to realize:
One aspect of the present invention provides a kind of Masterbatch, it is characterized in that, its prescription contains the component of following weight ratio: thermoplastic resin 60%-70%, additive 5%-10% and pigment 25%-30%.
In one embodiment of the invention, said thermoplastic resin is new LDPE (film grade), high density polyethylene(HDPE), linear low density polyethylene, HOPP, COPP.
In one embodiment of the invention, said additive comprises Rutile type Titanium Dioxide, anatase thpe white powder.
In one embodiment of the invention, said pigment comprises Pigment Yellow 73 001, Pigment Yellow 73 042, Pigment Yellow 73 109, Pigment Yellow 73 110, Pigment Yellow 73 119, pigment Yellow 12 8, pigment yellow 13, pigment yellow 13 8, pigment Yellow 14, pigment yellow 147, Pigment Yellow 73 151, pigment yellow 154, Pigment Yellow 73 168, Pigment Yellow 73 180, Pigment Yellow 73 181, Pigment Yellow 73 183, Pigment Yellow 73 191:1, Pigment Yellow 73 215, Pigment Yellow 73 42, Pigment Yellow 73 53, Pigment Yellow 73 62, Pigment Yellow 73 65, Pigment Yellow 73 74, pigment yellow 83, Pigment Yellow 73 93, Pigment Yellow 73 95, pigment Blue 15, pigment Blue 15: 1, pigment blue 16, Pigment blue 2, Pigment blue 28, Pigment blue 29, Pigment blue 36, pigment blue 60, Pigment blue 72, Pigment green 17, pigment green 36, Pigment green 50, pigment Green 7 add Phthalocyanine Green G, pigment violet 19, pigment violet 2, pigment Violet 23 and add permanent violet RL, pigment violet 29, pigment violet 37, pigment brown 23, pigment brown 24, pigment brown 6, pigment Orange 13, pigment orange 16, pigment orange 43, pigment orange 61, pigment orange 64, pigment orange 71, Pigment black 011, Pigment black 23, Pigment black 28, Pigment black 7, Pigment red 101 and add red stone, Pigment Red 112, pigment red 122, Pigment red 144, pigment red 146, pigment red 149, Pigment red 166, Pigment red 170, Pigment red 177, Pigment red 178, Pigment red 179, Pigment red 181, Pigment red 187, Pigment red 202, Pigment Red 207, Pigment red 208, Pigment red 209, pigment red 21 4, Pigment red 220, Pigment red 221, Pigment red 247, Pigment red 254, Pigment red 264, Pigment red 272, pigment red 4 8:2, pigment red 4 9:2, Pigment red 5, Pigment red 52:2, Pigment red 57:1, Pigment red 68.
In one embodiment of the invention, the moisture content of said Masterbatch is 0.1%-0.5% (wt), and aberration is the 4-5 level, and fusing point is 100 ℃-170 ℃, and thermotolerance is 200 ℃-300 ℃, and filterableness (DF value) is 0.3barcm
2/ g-1barcm
2/ g.
Another aspect of the present invention provides a kind of preparation method of Masterbatch, it is characterized in that, it comprises following technical process:
Batch mixing-blanking-fusion batch mixing-cooling-pelletizing-air-dry-packing.
In one embodiment of the invention, said fusion batch mixing is to melt extrude through the twin-screw mixer forcing machine, and said screw speed is 300RPM-320RPM, and mixing time is 500 seconds-800 seconds, and mixture temperature is 15 ℃-50 ℃.
In one embodiment of the invention, said refrigerative mode is water cooling, and cooling temperature is 30 ℃-80 ℃.
Masterbatch of the present invention and preparation method thereof, the Masterbatch temperature tolerance that produces is good, strainability is excellent, the spinning cycle is long, with its excellent performance, is widely used in before the spinning of polyester filament and short fiber paintedly, realizes the object of the invention.
Embodiment
Below further specify the present invention through embodiment, but should be understood that these embodiment are exemplary, the present invention does not limit to this.
Masterbatch of the present invention, its prescription contains the component of following weight ratio: thermoplastic resin 60%-70%, additive 5%-10% and pigment 25%-30%.
Said thermoplastic resin is new LDPE (film grade), high density polyethylene(HDPE), linear low density polyethylene, HOPP, COPP.
Said additive comprises Rutile type Titanium Dioxide, anatase thpe white powder.
Said pigment comprises Pigment Yellow 73 001; Pigment Yellow 73 042; Pigment Yellow 73 109; Pigment Yellow 73 110; Pigment Yellow 73 119; Pigment Yellow 12 8; Pigment yellow 13; Pigment yellow 13 8; Pigment Yellow 14; Pigment yellow 147; Pigment Yellow 73 151; Pigment yellow 154; Pigment Yellow 73 168; Pigment Yellow 73 180; Pigment Yellow 73 181; Pigment Yellow 73 183; Pigment Yellow 73 191:1; Pigment Yellow 73 215; Pigment Yellow 73 42; Pigment Yellow 73 53; Pigment Yellow 73 62; Pigment Yellow 73 65; Pigment Yellow 73 74; Pigment yellow 83; Pigment Yellow 73 93; Pigment Yellow 73 95; Pigment Blue 15; Pigment Blue 15: 1; Pigment blue 16; Pigment blue 2; Pigment blue 28; Pigment blue 29; Pigment blue 36; Pigment blue 60; Pigment blue 72; Pigment green 17; Pigment green 36; Pigment green 50; Pigment Green 7 adds Phthalocyanine Green G; Pigment violet 19; Pigment violet 2; Pigment Violet 23 adds permanent violet RL; Pigment violet 29; Pigment violet 37; Pigment brown 23; Pigment brown 24; Pigment brown 6; Pigment Orange 13; Pigment orange 16; Pigment orange 43; Pigment orange 61; Pigment orange 64; Pigment orange 71; Pigment black 011; Pigment black 23; Pigment black 28; Pigment black 7; Pigment red 101 adds red stone; Pigment Red 112; Pigment red 122; Pigment red 144; Pigment red 146; Pigment red 149; Pigment red 166; Pigment red 170; Pigment red 177; Pigment red 178; Pigment red 179; Pigment red 181; Pigment red 187; Pigment red 202; Pigment Red 207; Pigment red 208; Pigment red 209; Pigment red 21 4; Pigment red 220; Pigment red 221; Pigment red 247; Pigment red 254; Pigment red 264; Pigment red 272; Pigment red 4 8:2; Pigment red 4 9:2; Pigment red 5; Pigment red 52:2; Pigment red 57:1; Pigment red 68.
The preparation method of Masterbatch of the present invention, it comprises following technical process:
Batch mixing-blanking-fusion batch mixing-cooling-pelletizing-air-dry-packing.
Said fusion batch mixing is to melt extrude through the twin-screw mixer forcing machine, and said screw speed is 300RPM-320RPM, and mixing time is 500 seconds-800 seconds, and mixture temperature is 15 ℃-50 ℃.
Said refrigerative mode is water cooling, and cooling temperature is 30 ℃-80 ℃.
The moisture content of said Masterbatch is 0.1%-0.5% (wt), and aberration is the 4-5 level, and fusing point is 100 ℃-170 ℃, and thermotolerance is 200 ℃-300 ℃, and filterableness (DF value) is 0.3barcm
2/ g-1barcm
2/ g.
Embodiment 1:
In the present embodiment, thermoplastic resin 60%, additive 10% and pigment 30%; Said thermoplastic resin is a new LDPE (film grade), and said additive comprises Rutile type Titanium Dioxide, and said pigment comprises (pigment yellow 83, pigment red 4 8:2, pigment red 21 4).
During preparation, adopt following technical process: batch mixing-blanking-fusion batch mixing-cooling-pelletizing-air-dry-packing.
Said fusion batch mixing is to melt extrude through the twin-screw mixer forcing machine, and said screw speed is 300RPM, and mixing time is 500 seconds, and mixture temperature is 30 ℃.
Said refrigerative mode is water cooling, and cooling temperature is 35 ℃.
The moisture content of said Masterbatch is 0.2% (wt), and aberration is the 4-5 level, and fusing point is 110 ℃, and thermotolerance is 200 ℃, and filterableness (DF value) is 0.3barcm
2/ g.
Embodiment 2:
In the present embodiment, thermoplastic resin 70%, additive 5% and pigment 25%; Said thermoplastic resin is a high density polyethylene(HDPE), and said additive comprises Rutile type Titanium Dioxide, and said pigment comprises (pigment Green 7, Pigment Yellow 73 183).
During preparation, adopt following technical process: batch mixing-blanking-fusion batch mixing-cooling-pelletizing-air-dry-packing.
Said fusion batch mixing is to melt extrude through the twin-screw mixer forcing machine, and said screw speed is 300RPM, and mixing time is 500 seconds, and mixture temperature is 30 ℃.
Said refrigerative mode is water cooling, and cooling temperature is 35 ℃.
The moisture content of said Masterbatch is 0.15% (wt), and aberration is the 4-5 level, and fusing point is 120 ℃, and thermotolerance is 280 ℃, and filterableness (DF value) is 0.5barcm
2/ g.
Embodiment 3:
In the present embodiment, thermoplastic resin 67.92%, additive 5.76 and pigment 26.32%; Said thermoplastic resin is a COPP, and said additive comprises anatase thpe white powder, and said pigment comprises (pigment Blue 15: 1, Pigment black 7, Pigment Yellow 73 180).
During preparation, adopt following technical process: batch mixing-blanking-fusion batch mixing-cooling-pelletizing-air-dry-packing.
Said fusion batch mixing is to melt extrude through the twin-screw mixer forcing machine, and said screw speed is 320RPM, and mixing time is 500 seconds, and mixture temperature is 30 ℃.
Said refrigerative mode is water cooling, and cooling temperature is 35 ℃.
The moisture content of said Masterbatch is 0.2% (wt), and aberration is the 4-5 level, and fusing point is 170 ℃, and thermotolerance is 260 ℃, and filterableness (DF value) is 0.6barcm
2/ g.
More than show and described ultimate principle of the present invention and principal character and advantage of the present invention.The technician of the industry should understand; The present invention is not restricted to the described embodiments; That describes in the foregoing description and the specification sheets just explains principle of the present invention, and under the prerequisite that does not break away from spirit and scope of the invention, the present invention also has various changes and modifications; These variations and improvement all fall in the scope of the invention that requires protection, and the present invention requires protection domain to be defined by appending claims and equivalent thereof.
Claims (8)
1. a Masterbatch is characterized in that, its prescription contains the component of following weight ratio: thermoplastic resin 60%-70%, additive 5%-10% and pigment 25%-30%.
2. Masterbatch according to claim 1 is characterized in that, said thermoplastic resin is new LDPE (film grade), high density polyethylene(HDPE), linear low density polyethylene, HOPP, COPP.
3. Masterbatch according to claim 1 is characterized in that said additive comprises Rutile type Titanium Dioxide, anatase titanium dioxide.
4. Masterbatch according to claim 1; It is characterized in that said pigment comprises Pigment Yellow 73 001, Pigment Yellow 73 042, Pigment Yellow 73 109, Pigment Yellow 73 110, Pigment Yellow 73 119, pigment Yellow 12 8, pigment yellow 13, pigment yellow 13 8, pigment Yellow 14, pigment yellow 147, Pigment Yellow 73 151, pigment yellow 154, Pigment Yellow 73 168, Pigment Yellow 73 180, Pigment Yellow 73 181, Pigment Yellow 73 183, Pigment Yellow 73 191:1, Pigment Yellow 73 215, Pigment Yellow 73 42, Pigment Yellow 73 53, Pigment Yellow 73 62, Pigment Yellow 73 65, Pigment Yellow 73 74, pigment yellow 83, Pigment Yellow 73 93, Pigment Yellow 73 95, pigment Blue 15, pigment Blue 15: 1, pigment blue 16, Pigment blue 2, Pigment blue 28, Pigment blue 29, Pigment blue 36, pigment blue 60, Pigment blue 72, Pigment green 17, pigment green 36, Pigment green 50, pigment Green 7 add Phthalocyanine Green G, pigment violet 19, pigment violet 2, pigment Violet 23 and add permanent violet RL, pigment violet 29, pigment violet 37, pigment brown 23, pigment brown 24, pigment brown 6, pigment Orange 13, pigment orange 16, pigment orange 43, pigment orange 61, pigment orange 64, pigment orange 71, Pigment black 011, Pigment black 23, Pigment black 28, Pigment black 7, Pigment red 101 and add red stone, Pigment Red 112, pigment red 122, Pigment red 144, pigment red 146, pigment red 149, Pigment red 166, Pigment red 170, Pigment red 177, Pigment red 178, Pigment red 179, Pigment red 181, Pigment red 187, Pigment red 202, Pigment Red 207, Pigment red 208, Pigment red 209, pigment red 21 4, Pigment red 220, Pigment red 221, Pigment red 247, Pigment red 254, Pigment red 264, Pigment red 272, pigment red 4 8:2, pigment red 4 9:2, Pigment red 5, Pigment red 52:2, Pigment red 57:1, Pigment red 68.
5. Masterbatch according to claim 1 is characterized in that, the moisture content of said Masterbatch is 0.1%-0.5% (wt), and aberration is the 4-5 level, and fusing point is 100 ℃-170 ℃, and thermotolerance is 200 ℃-300 ℃, and filterableness (DF value) is 0.3barcm
2/ g-1barcm
2/ g.
6. the preparation method of a Masterbatch is characterized in that, it comprises following technical process:
Batch mixing-blanking-fusion batch mixing-cooling-pelletizing-air-dry-packing.
7. the preparation method of Masterbatch according to claim 6; It is characterized in that said fusion batch mixing is to melt extrude through the twin-screw mixer forcing machine, said screw speed is 300RPM-320RPM; Mixing time is 500 seconds-800 seconds, and mixture temperature is 15 ℃-50 ℃.
8. the preparation method of Masterbatch according to claim 6 is characterized in that, said refrigerative mode is water cooling, and cooling temperature is 30 ℃-80 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011100533163A CN102675709A (en) | 2011-03-07 | 2011-03-07 | Color masterbatch and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011100533163A CN102675709A (en) | 2011-03-07 | 2011-03-07 | Color masterbatch and preparation method thereof |
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|---|---|
| CN102675709A true CN102675709A (en) | 2012-09-19 |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102649849A (en) * | 2011-11-21 | 2012-08-29 | 上海彩艳实业有限公司 | Color master batch for colorizing medical composite non-woven fabric melt-blown layer and preparation method thereof |
| CN103289333A (en) * | 2013-05-31 | 2013-09-11 | 上海彩艳实业有限公司 | High-weather-proof automobile interior trimming cloth color master batch and preparation method thereof |
| CN103865294A (en) * | 2012-12-12 | 2014-06-18 | 天彩企业有限公司 | Infrared ray low heating pigment composition and infrared ray low heating material |
| CN104231399A (en) * | 2014-09-24 | 2014-12-24 | 苏州冰心文化用品有限公司 | Color master batch material and preparation method thereof |
| CN104558799A (en) * | 2014-12-22 | 2015-04-29 | 山东农业大学 | Special anti-ageing dimming green master batch for ginger greenhouse film and preparation method of special anti-ageing dimming green master batch |
| CN104558765A (en) * | 2014-12-22 | 2015-04-29 | 山东农业大学 | Special light-dimming green master batch for ginger mulching film and preparation method of master batch |
| CN106087102A (en) * | 2016-06-17 | 2016-11-09 | 上海洋帆实业有限公司 | A kind of original liquid coloring tent fabric and preparation method thereof |
| CN106566083A (en) * | 2016-11-03 | 2017-04-19 | 苏州圣鑫莱新材料有限公司 | Nano PP color masterbatch |
| WO2018154409A1 (en) * | 2017-02-21 | 2018-08-30 | 李耀辉 | Color masterbatch composition for dark textiles or engineering plastics and article produced therefrom |
| CN109023569A (en) * | 2018-08-16 | 2018-12-18 | 江苏华昌织物有限公司 | A kind of colored shade net and preparation method thereof for Chinese little greens |
| CN111363251A (en) * | 2020-02-11 | 2020-07-03 | 广东波斯科技股份有限公司 | Special coloring master batch for PPR pipe and preparation method and application thereof |
| CN112812486A (en) * | 2020-12-31 | 2021-05-18 | 杭州诺莘科技有限责任公司 | Infrared light reflection heat insulation COC plastic and preparation method and application thereof |
| CN114685818A (en) * | 2020-12-31 | 2022-07-01 | 中国纺织科学研究院有限公司 | Preparation method of polyamide color master batch carrier resin and polyamide color master batch |
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| CN101831099A (en) * | 2010-04-19 | 2010-09-15 | 成都菲斯特化工有限公司 | Method for preparing full-dispersion polyethylene color masterbatch |
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| US20050038189A1 (en) * | 2001-10-16 | 2005-02-17 | Idemitsu Petrochemical Co., Ltd | Coloring pigment masterbatch composition and method of molding |
| CN101440189A (en) * | 2008-12-19 | 2009-05-27 | 常州市改性塑料厂有限公司 | Special color master batch for refrigerator plate and preparation thereof |
| CN101831099A (en) * | 2010-04-19 | 2010-09-15 | 成都菲斯特化工有限公司 | Method for preparing full-dispersion polyethylene color masterbatch |
Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102649849A (en) * | 2011-11-21 | 2012-08-29 | 上海彩艳实业有限公司 | Color master batch for colorizing medical composite non-woven fabric melt-blown layer and preparation method thereof |
| CN103865294B (en) * | 2012-12-12 | 2016-12-21 | 天彩企业有限公司 | Infrared ray low intensification pigment constituent and low liter of adiabator of infrared ray |
| CN103865294A (en) * | 2012-12-12 | 2014-06-18 | 天彩企业有限公司 | Infrared ray low heating pigment composition and infrared ray low heating material |
| CN103289333A (en) * | 2013-05-31 | 2013-09-11 | 上海彩艳实业有限公司 | High-weather-proof automobile interior trimming cloth color master batch and preparation method thereof |
| CN104231399A (en) * | 2014-09-24 | 2014-12-24 | 苏州冰心文化用品有限公司 | Color master batch material and preparation method thereof |
| CN104558799A (en) * | 2014-12-22 | 2015-04-29 | 山东农业大学 | Special anti-ageing dimming green master batch for ginger greenhouse film and preparation method of special anti-ageing dimming green master batch |
| CN104558765B (en) * | 2014-12-22 | 2016-10-05 | 山东农业大学 | Green master batch of the special light modulation of a kind of Rhizoma Zingiberis Recens mulch film and preparation method thereof |
| CN104558765A (en) * | 2014-12-22 | 2015-04-29 | 山东农业大学 | Special light-dimming green master batch for ginger mulching film and preparation method of master batch |
| CN104558799B (en) * | 2014-12-22 | 2017-06-30 | 山东农业大学 | A kind of special green master batch of anti-aging light modulation of ginger canopy film and preparation method thereof |
| CN106087102A (en) * | 2016-06-17 | 2016-11-09 | 上海洋帆实业有限公司 | A kind of original liquid coloring tent fabric and preparation method thereof |
| CN106566083A (en) * | 2016-11-03 | 2017-04-19 | 苏州圣鑫莱新材料有限公司 | Nano PP color masterbatch |
| WO2018154409A1 (en) * | 2017-02-21 | 2018-08-30 | 李耀辉 | Color masterbatch composition for dark textiles or engineering plastics and article produced therefrom |
| CN109023569A (en) * | 2018-08-16 | 2018-12-18 | 江苏华昌织物有限公司 | A kind of colored shade net and preparation method thereof for Chinese little greens |
| CN109023569B (en) * | 2018-08-16 | 2021-04-09 | 江苏华昌织物有限公司 | Colorful sunshade net for Chinese little greens and preparation method thereof |
| CN111363251A (en) * | 2020-02-11 | 2020-07-03 | 广东波斯科技股份有限公司 | Special coloring master batch for PPR pipe and preparation method and application thereof |
| CN112812486A (en) * | 2020-12-31 | 2021-05-18 | 杭州诺莘科技有限责任公司 | Infrared light reflection heat insulation COC plastic and preparation method and application thereof |
| CN114685818A (en) * | 2020-12-31 | 2022-07-01 | 中国纺织科学研究院有限公司 | Preparation method of polyamide color master batch carrier resin and polyamide color master batch |
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Application publication date: 20120919 |