CN102652716B - Preparation method of rose traditional Chinese medicine foot-bath powder - Google Patents
Preparation method of rose traditional Chinese medicine foot-bath powder Download PDFInfo
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- CN102652716B CN102652716B CN 201110047888 CN201110047888A CN102652716B CN 102652716 B CN102652716 B CN 102652716B CN 201110047888 CN201110047888 CN 201110047888 CN 201110047888 A CN201110047888 A CN 201110047888A CN 102652716 B CN102652716 B CN 102652716B
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- 239000000843 powder Substances 0.000 title claims abstract description 34
- 238000002360 preparation method Methods 0.000 title claims abstract description 6
- 239000003814 drug Substances 0.000 title abstract description 14
- 241000220317 Rosa Species 0.000 title abstract 3
- 239000000706 filtrate Substances 0.000 claims abstract description 34
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 28
- 238000001914 filtration Methods 0.000 claims abstract description 21
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 15
- 238000000605 extraction Methods 0.000 claims abstract description 15
- 239000011780 sodium chloride Substances 0.000 claims abstract description 15
- 235000002639 sodium chloride Nutrition 0.000 claims abstract description 15
- 238000001035 drying Methods 0.000 claims abstract description 10
- 238000003756 stirring Methods 0.000 claims abstract description 9
- 241000756943 Codonopsis Species 0.000 claims abstract description 8
- 239000007787 solid Substances 0.000 claims abstract description 8
- 241000628997 Flos Species 0.000 claims description 15
- 239000012141 concentrate Substances 0.000 claims description 7
- 239000000463 material Substances 0.000 claims description 3
- 238000000034 method Methods 0.000 abstract description 6
- 239000000047 product Substances 0.000 abstract description 4
- 230000000694 effects Effects 0.000 abstract description 3
- 244000061520 Angelica archangelica Species 0.000 abstract 1
- 244000124209 Crocus sativus Species 0.000 abstract 1
- 235000015655 Crocus sativus Nutrition 0.000 abstract 1
- 240000004670 Glycyrrhiza echinata Species 0.000 abstract 1
- 235000001453 Glycyrrhiza echinata Nutrition 0.000 abstract 1
- 235000006200 Glycyrrhiza glabra Nutrition 0.000 abstract 1
- 235000017382 Glycyrrhiza lepidota Nutrition 0.000 abstract 1
- 235000001287 Guettarda speciosa Nutrition 0.000 abstract 1
- 241000244365 Ligusticum sinense Species 0.000 abstract 1
- 238000000227 grinding Methods 0.000 abstract 1
- 229940010454 licorice Drugs 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- 239000013543 active substance Substances 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- 239000000284 extract Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 235000008216 herbs Nutrition 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 239000006210 lotion Substances 0.000 description 2
- 235000010755 mineral Nutrition 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- 235000003143 Panax notoginseng Nutrition 0.000 description 1
- 241000180649 Panax notoginseng Species 0.000 description 1
- 241001604597 Pyrestini Species 0.000 description 1
- 241000545442 Radix Species 0.000 description 1
- 241000657665 Rhopilema esculentum Species 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 238000003287 bathing Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 229940126678 chinese medicines Drugs 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 229920001495 poly(sodium acrylate) polymer Polymers 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- NNMHYFLPFNGQFZ-UHFFFAOYSA-M sodium polyacrylate Chemical compound [Na+].[O-]C(=O)C=C NNMHYFLPFNGQFZ-UHFFFAOYSA-M 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
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- Medicines Containing Plant Substances (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to a traditional Chinese medicine health-care medicine, and particularly relates to a preparation method of rose traditional Chinese medicine foot-bath powder. The method comprises the following steps: adding 100 g of saffron crocus, 80 g of angelica, 100 g of ligusticum chuanxiong hort, 60 g of radix codonopsis, 100 g of licorice into 5 kg of water, performing countercurrent extraction for 2 hours, filtering, adding 3 kg of water into a filter residue, performing countercurrent extraction for 1.5 hours, filtering, combining two filtrates, standing for 20 hours at the temperature of 1-4 DEG C, filtering to obtain a filtrate, concentrating the filtrate under a reduced pressure to a third volume of the original volume, mixing the concentrated filtrate with sea salt according to a mass ratio of 10:1, fully and uniformly stirring and drying in a drying oven at the temperature of 50-100 DEG C, grinding the dried solid into powder, and adding 10-50 g of rose in the powder. The product of the invention has the advantages of good curative effect and long shelf life.
Description
Technical field
The present invention relates to a kind of Chinese medicine health-care medicine, specifically a kind of preparation method of Flos Rosae Rugosae Chinese herb bath foot-powder.
Background technology
Along with improving constantly and the healthy enhancing looked like of people's living standard, people are also more and more higher to the health care consciousness of foot.Therefore the products such as foot bath powder, foot bath mud, foot bathing lotion, health-care lotion for foot bath constantly present on market.But this series products generally can not be fully very short with the shelf-life of foot skin contact or product by the Chinese medicine elite, to consumer's use, brings a lot of inconvenience.The patent Introduction of publication number CN101181207 a kind of foot bath mud, by the macromolecular material sodium polyacrylate, with the medicated powder of the porphyrizes such as Cortex Acanthopancis, Cortex erythrinae, Flos Carthami, Radix Saposhnikoviae, Radix Scutellariae, Ramulus Cinnamomi, Radix Notoginseng, Radix Angelicae Sinensis, mixed mutually, stirring forms.The patent Introduction of publication number CN1255330 a kind of medical herbs foot bath health-care agent, by Chinese medicine direct matchings such as Radix Angelicae Dahuricae (Radix Heraclei Scabridi), Cortex cinnamomi japonici (Ramulus Cinnamomi), Cacumen Platycladi (Cacumen Biotae), Radix Aristolochiae, Herba speranskiae tuberculataes, formed.The patent Introduction of publication number CN1528267 a kind ofly by herbal powders such as Flos Caryophylli, Flos Carthami, Flos Chrysanthemi Indici, Rhizoma Zingiberis, Herba Pogostemonis, Radix Angelicae Sinensis, the Radixs Stemonae, mixed by a certain percentage.Above patent has two shortcomings.One, the water temperature due to foot bath can be very not high, and the time of medicated powder in warm water can be very not long yet, thus the active component in medicated powder to be dissolved into the ratio of water limited, so its effect is also limited.Two, medicated powder adds in warm water, and some powder swim on the water surface, and what have sinks to the bottom, affects the sensation of foot, also has a lot of impurity and sneaks in medicated powder, affects the enjoyment process of foot bath process simultaneously.Patent CN1583033 has introduced and a kind ofly with Chinese medicines such as Flos Carthami, Rhizoma Gastrodiae, shell, Rhopilema esculenta, Radix Angelicae Sinensis, has been mixed in proportion after adding water boil and filters, and filtrate adds foot bath in foot bath warm water.All need decocting herb before the each foot bath of this patent, then filter, filtrate is added in foot bath water, whole process is very inconvenient, and liquid medicine need to use as early as possible, otherwise is easy to go bad.
Summary of the invention
Purpose of the present invention is exactly the defect for existing foot bath powder, provides the preparation method of the Flos Rosae Rugosae Chinese herb bath foot-powder of a kind of good effect, long shelf-life, to make up the deficiencies in the prior art.
Technical scheme of the present invention is achieved in that it is by Stigma Croci 80-120 gram, Radix Angelicae Sinensis 60-100 gram, Rhizoma Chuanxiong 80-100 gram, Radix Codonopsis 40-80 gram, Radix Glycyrrhizae 80-120 gram joins in the water of 4～10 times of quality, countercurrent extraction 0.5～3 hour, filter, to the water that adds 4～10 times of quality in filtering residue, countercurrent extraction 0.5～3 hour, filter, merge filtrate twice, standing 10-24 hour, filtration obtains filtrate, concentrate filtrate to 1/3～1/10 of original volume, filtrate after concentrated be take to the ratio that mass ratio is 1:1～10:1 mixes with sea salt, fully stir evenly post-drying, then the solid after drying is crushed into powder.
The present invention's technical scheme preferably is: by Stigma Croci 100 grams, Radix Angelicae Sinensis 80 grams, Rhizoma Chuanxiong 100 grams, Radix Codonopsis 60 grams, Radix Glycyrrhizae 100 grams add the water of 5 kilograms, adverse current stream extracts 2 hours, filter, to the water that adds 3 kilograms in filtering residue, countercurrent extraction 1.5 hours, filter, merge filtrate twice, 1～4 ℃ of stand at low temperature 20 hours, filtration obtains filtrate, concentrate filtrate to 1/3 of original volume, filtrate after concentrated be take to the ratio that mass ratio is 10:1 mixes with sea salt, after fully stirring evenly, material is put into to 50 ℃～100 ℃ oven dry of baking oven, then the solid after drying is crushed into powder, add Flos Rosae Rugosae 10-50 gram in powder.
The present invention mixes the concentrated liquid of tradition Chinese medicine with middle with sea salt, sea salt itself has the sterilization anti-inflammatory efficacy, contains various mineral in sea salt simultaneously, can provide various mineral for the foot skin.After the abundant melting of the concentrated liquid of tradition Chinese medicine and sea salt, then the moisture evaporation of mixture is dry, guarantee that active substance is retained in final dried crystals powder fully. then in the process of using, after adding a small amount of foot bath powder in warm water, active substance and sea salt can be dissolved in warm water immediately, thereby allow various active substances discharge fully.The Chinese herb bath foot-powder contains active ingredient of Chinese herbs and sea salt in end, and the characteristic with bacteria growing inhibiting of sea salt itself, therefore, the situations such as mildew goes bad, can not occur in Chinese herb bath foot-powder steady quality.Chinese herbal medicine is pulverized laggard row reflux, extract, 2 times, allows active substance in Chinese medicine fully be dissolved into and extracts in solvent.And often can not allow the active substance of Chinese medicine fully be dissolved into warm water the traditional method that Chinese medicine is put into the warm water foot bath.
The specific embodiment
Below in conjunction with embodiment, the present invention is described further:
EXAMPLE l
Selected Stigma Croci 100 grams, Radix Angelicae Sinensis 80 grams, Rhizoma Chuanxiong 100 grams, Radix Codonopsis 60 grams, Radix Glycyrrhizae 100 grams.The water that adds 5 kilograms, countercurrent extraction 2 hours, filter, and to the water that adds 3 kilograms in filtering residue, countercurrent extraction 80 minutes, filter, merging filtrate, 1～4 ℃ of stand at low temperature is spent the night, and plate-and-frame filtration obtains filtrate.Concentrate filtrate to 1/3 of original volume, plate-and-frame filtration, mix with the ratio of mass ratio 10:1 the filtrate after concentrated with sea salt, put into 90 ℃ of oven dry of baking oven after fully stirring evenly, and then allows the solid after drying be crushed into powder.Add Flos Rosae Rugosae 10 grams in powder.
Embodiment 2
Selected Stigma Croci 80 grams, Radix Angelicae Sinensis 100 grams, Rhizoma Chuanxiong 120 grams, Radix Codonopsis 60 grams, Radix Glycyrrhizae 80 grams.The water that adds 4 kilograms, countercurrent extraction 1 hour, filter, and to the water that adds 3 kilograms in filtering residue, countercurrent extraction 1 hour, filter, merging filtrate, 1～4 ℃ of stand at low temperature is spent the night, and plate-and-frame filtration obtains filtrate.Concentrate filtrate to 1/5 of original volume, plate-and-frame filtration, mix with the ratio of mass ratio 5:1 the filtrate after concentrated with sea salt, put into 90 ℃ of oven dry of baking oven after fully stirring evenly, and then allows the solid after drying be crushed into powder.Add Flos Rosae Rugosae 50 grams in powder.
Embodiment 3
Selected Stigma Croci 60 grams, Radix Angelicae Sinensis 60 grams, Rhizoma Chuanxiong 80 grams, Radix Codonopsis 40 grams, Radix Glycyrrhizae 80 grams.The water that adds 5 kilograms, countercurrent extraction 2 hours, filter, and to the water that adds 3 kilograms in filtering residue, countercurrent extraction 40 minutes, filter, merging filtrate, 1～4 ℃ of stand at low temperature is spent the night, and plate-and-frame filtration obtains filtrate.Concentrate filtrate to 1/10 of original volume, plate-and-frame filtration, mix with the ratio of mass ratio 1:1 the filtrate after concentrated with sea salt, put into 90 ℃ of oven dry of baking oven after fully stirring evenly, and then allows the solid after drying be crushed into powder.Add Flos Rosae Rugosae 20 grams in powder.
Embodiment 4
Selected Stigma Croci 100 grams, Radix Angelicae Sinensis 80 grams, Rhizoma Chuanxiong 100 grams, Radix Codonopsis 60 grams, Radix Glycyrrhizae 100 grams.The water that adds 5 kilograms, countercurrent extraction 2 hours, filter, and to the water that adds 3 kilograms in filtering residue, countercurrent extraction 80 minutes, filter, merging filtrate, 1～4 ℃ of stand at low temperature is spent the night, and plate-and-frame filtration obtains filtrate.Concentrate filtrate to 1/6 of original volume, plate-and-frame filtration, mix with the ratio of mass ratio 10:1 the filtrate after concentrated with sea salt, put into 90 ℃ of oven dry of baking oven after fully stirring evenly, and then allows the solid after drying be crushed into powder.Add Flos Rosae Rugosae 30 grams in powder.
Claims (1)
1. the preparation method of a Flos Rosae Rugosae Chinese herb bath foot-powder, it is characterized in that: it is by Stigma Croci 100 grams, Radix Angelicae Sinensis 80 grams, Rhizoma Chuanxiong 100 grams, Radix Codonopsis 60 grams, Radix Glycyrrhizae 100 grams add the water of 5 kilograms, countercurrent extraction 2 hours, filter, to the water that adds 3 kilograms in filtering residue, countercurrent extraction 1.5 hours, filter, merge filtrate twice, 1～4 ℃ of stand at low temperature 20 hours, filtration obtains filtrate, concentrate filtrate to 1/3 of original volume, filtrate after concentrated be take to the ratio that mass ratio is 10:1 mixes with sea salt, after fully stirring evenly, material is put into to 50 ℃～100 ℃ oven dry of baking oven, then the solid after drying is crushed into powder, add Flos Rosae Rugosae 10-50 gram in powder.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110047888 CN102652716B (en) | 2011-03-01 | 2011-03-01 | Preparation method of rose traditional Chinese medicine foot-bath powder |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110047888 CN102652716B (en) | 2011-03-01 | 2011-03-01 | Preparation method of rose traditional Chinese medicine foot-bath powder |
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| CN102652716A CN102652716A (en) | 2012-09-05 |
| CN102652716B true CN102652716B (en) | 2013-12-18 |
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Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103385914B (en) * | 2013-06-26 | 2015-02-11 | 山东无棣精盐厂 | Hot compress salt and preparation method thereof |
| CN104225563A (en) * | 2014-09-30 | 2014-12-24 | 中盐东兴盐化股份有限公司 | Healthcare foot bath salt |
| CN104306499A (en) * | 2014-09-30 | 2015-01-28 | 中盐东兴盐化股份有限公司 | Foot bath salt with functions of clearing cold and inducing diuresis |
| CN104225561A (en) * | 2014-09-30 | 2014-12-24 | 中盐东兴盐化股份有限公司 | Health-care foot bath salt capable of activating blood circulation |
| CN104398420A (en) * | 2014-11-13 | 2015-03-11 | 哈尔滨灵草舒生物科技有限公司 | Gordon euryale stem bath powder for removing heat to promote salivation and production method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101607029A (en) * | 2008-06-22 | 2009-12-23 | 董宪常 | Method for treating insomnia by soaking feet with traditional Chinese medicines |
| CN101612298A (en) * | 2008-06-24 | 2009-12-30 | 董宪常 | Method for treating middle-aged insomnia by foot bath with traditional Chinese medicines |
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- 2011-03-01 CN CN 201110047888 patent/CN102652716B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101607029A (en) * | 2008-06-22 | 2009-12-23 | 董宪常 | Method for treating insomnia by soaking feet with traditional Chinese medicines |
| CN101612298A (en) * | 2008-06-24 | 2009-12-30 | 董宪常 | Method for treating middle-aged insomnia by foot bath with traditional Chinese medicines |
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| CN102652716A (en) | 2012-09-05 |
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