CN102634999A - Sodium alga acid printing paste and preparation process thereof - Google Patents
Sodium alga acid printing paste and preparation process thereof Download PDFInfo
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- CN102634999A CN102634999A CN2012101110832A CN201210111083A CN102634999A CN 102634999 A CN102634999 A CN 102634999A CN 2012101110832 A CN2012101110832 A CN 2012101110832A CN 201210111083 A CN201210111083 A CN 201210111083A CN 102634999 A CN102634999 A CN 102634999A
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- sodium
- sodium alginate
- alga acid
- printing paste
- anhydrous sodium
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Abstract
The invention relates to sodium alga acid printing paste, comprising the following components in percent by weight: 60-90% of sodium alga acid, 5-15% of sodium hexametaphosphate and 5-25% of anhydrous sodium sulphate. The preparation method of the sodium alga acid printing paste comprises the following steps of: (1) weighing sodium alga acid, sodium hexametaphosphate and anhydrous sodium sulphate in the proportion of a formula; (2) smashing the sodium alga acid to 30-40 meshes; (3) placing smashed sodium alga acid, sodium hexametaphosphate and anhydrous sodium sulphate into a mixing tank to be stirred; and (4) stirring to be completely uniform, thus the sodium alga acid printing paste finished product is obtained. The sodium alga acid printing paste disclosed by the invention has the beneficial effects that (1) sodium carboxymethyl starch having adverse effects on colouring is removed, and anhydrous sodium sulphate which can activate active groups in dye and has high colouring rate is adopted; and (2) sodium hexametaphosphate can cause calcium ions or magnesium ions in water to enter into sodium hexametaphosphate molecules to be changed into stable soluble complex, thus permeability of the printing paste is improved, colour fastness is improved, and the dye can be saved.
Description
Technical field
The invention belongs to the carrier that fabric printing is used, sodium alginate printing gum and preparation technology thereof that particularly a kind of stamp is used.
Background technology
Sodium alginate slurry is a kind of more satisfactory thickener in stamp is used, its maximum characteristics be not with dye, make dyestuff transfer to fiber easily and get on from thickener, the decorative pattern that prints off is clear, tinctorial yield is high, good hand touch.The sodium alginate slurry is not only applicable to the cotton red ink paste used for seals, is applicable to the stamp of wool, silk, synthetic fiber yet.
Present sodium alginate slurry majority is to be processed by pure sodium alginate, and sodium alginate mainly extracts from sea-tangle, but in recent years along with the application of sodium alginate on food industry and medical industry, marine algae resource is more and more nervous, and cost obviously improves; In addition, it is too short that sodium alginate is starched in use stationary phase, and slurry is stored and had only 2 days under the normal temperature, under summer high temperature, needs the existing usefulness at present of beating, and both inconvenience caused waste again easily.
Number of patent application is that the prescription of 03151285.2 " a kind of printing gum and preparation method thereof " is: CMS receives 20～74.5%, sodium alginate 20～70%, and mineral oil 0.5～2%, and can add calgon 5～20% or preservative agent 2～8%.This prescription has reduced production cost, and the product cold water-soluble is good, has good stable property.But since the carboxyl in the sodium carboxymethyl starch be prone to REACTIVE DYES in active group combine, cause fastness poor, give look light, meet water and be prone to the formation imbibition and wash problem such as discolor by rubbing with the hands.
Summary of the invention
The present invention is directed to the present situation of sodium alginate printing gum, a kind of tinctorial yield height, good evenness, sodium alginate printing gum and preparation technology thereof that dyefastness is strong are provided.
Technical scheme of the present invention: a kind of sodium alginate printing gum is characterized in that: the component and the percentage by weight thereof of said printing gum are following: the 60%-90% sodium alginate; The 5%-15% calgon; The 5%-25% anhydrous sodium sulfate.
The present invention also provides the preparation technology of sodium alginate printing gum, may further comprise the steps:
(1) takes by weighing sodium alginate, calgon, anhydrous sodium sulfate by formula rate;
(2) sodium alginate is crushed to the 30-40 order;
(3) sodium alginate after pulverizing is put into mixing tank with calgon, anhydrous sodium sulfate and is fully stirred, mixes;
(4) continue to stir 10-60 minute,, after inspection by sampling is qualified, get sodium alginate printing gum finished product until fully evenly.
Beneficial effect of the present invention is: the sodium carboxymethyl starch that adverse effect is arranged to painted has been removed in (1), has adopted anhydrous sodium sulfate; Anhydrous sodium sulfate can activate the active group in the dyestuff, and tinctorial yield is high.(2) calgon can make calcium ion or magnesium ion in the water get in the hexa metaphosphoric acid sodium molecule, becomes stable soluble complexes, thereby has improved the permeability of printing gum, has improved dyefastness, thereby can practice thrift dyestuff.
The specific embodiment
Embodiment 1
(1) by 60% sodium alginate, 15% calgon, the ratio of 25% anhydrous sodium sulfate takes by weighing 60kg sodium alginate, 15kg calgon, 25kg anhydrous sodium sulfate;
(2) sodium alginate is crushed to 30 orders;
(3) sodium alginate after pulverizing is put into mixing tank with calgon, anhydrous sodium sulfate and is fully stirred, mixes;
(4) continue to stir 20 minutes,, after inspection by sampling is qualified, get sodium alginate printing gum finished product until fully evenly.
(5) metering packing as requested.
Embodiment 2
(1) by 90% sodium alginate, 5% calgon, the ratio of 5% anhydrous sodium sulfate takes by weighing 90kg sodium alginate, 5kg calgon, 5kg anhydrous sodium sulfate;
(2) sodium alginate is crushed to 40 orders;
(3) sodium alginate after pulverizing is put into mixing tank with calgon, anhydrous sodium sulfate and is fully stirred, mixes;
(4) continue to stir 60 minutes,, after inspection by sampling is qualified, get sodium alginate printing gum finished product until fully evenly.
(5) metering packing as requested.
Embodiment 3
(1) by 70% sodium alginate, 8% calgon, the ratio of 22% anhydrous sodium sulfate takes by weighing 70kg sodium alginate, 10kg calgon, 20kg anhydrous sodium sulfate;
(2) sodium alginate is crushed to 35 orders;
(3) sodium alginate after pulverizing is put into mixing tank with calgon, anhydrous sodium sulfate and is fully stirred, mixes;
(4) continue to stir 40 minutes,, after inspection by sampling is qualified, get sodium alginate printing gum finished product until fully evenly.
(5) metering packing as requested.
Embodiment 4
(1) by 80% sodium alginate, 12% calgon, the ratio of 18% anhydrous sodium sulfate takes by weighing 80kg sodium alginate, 12kg calgon, 18kg anhydrous sodium sulfate;
(2) sodium alginate is crushed to 40 orders;
(3) sodium alginate after pulverizing is put into mixing tank with calgon, anhydrous sodium sulfate and is fully stirred, mixes;
(4) continue to stir 10 minutes,, after inspection by sampling is qualified, get sodium alginate printing gum finished product until fully evenly.
(5) metering packing as requested.
Claims (2)
1. sodium alginate printing gum, it is characterized in that: the component and the percentage by weight thereof of said printing gum are following:
Sodium alginate 60%-90%;
Calgon 5%-15%;
Anhydrous sodium sulfate 5%-25%.
2. the preparation technology of a sodium alginate printing gum is characterized in that: comprise the steps:
(1) takes by weighing sodium alginate, calgon, anhydrous sodium sulfate by formula rate;
(2) sodium alginate is pulverized the 30-40 order;
(3) sodium alginate after pulverizing is put into mixing tank with calgon, anhydrous sodium sulfate and is fully stirred, mixes;
(4) continue to stir 10-60 minute,, after inspection by sampling is qualified, get sodium alginate printing gum finished product until fully evenly.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012101110832A CN102634999A (en) | 2012-04-17 | 2012-04-17 | Sodium alga acid printing paste and preparation process thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012101110832A CN102634999A (en) | 2012-04-17 | 2012-04-17 | Sodium alga acid printing paste and preparation process thereof |
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| Publication Number | Publication Date |
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| CN102634999A true CN102634999A (en) | 2012-08-15 |
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| CN2012101110832A Pending CN102634999A (en) | 2012-04-17 | 2012-04-17 | Sodium alga acid printing paste and preparation process thereof |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103469618A (en) * | 2013-09-06 | 2013-12-25 | 浙江华东纺织印染有限公司 | Non-urea reactive dye printing paste, manufacturing method and printing and dyeing method |
| CN104141243A (en) * | 2014-07-28 | 2014-11-12 | 绍兴县彩色橼纺织科技有限公司 | Three-dimensional printing paste |
| CN105386338A (en) * | 2015-12-14 | 2016-03-09 | 青岛明月海藻集团有限公司 | Preparation method of instant sodium alginate printing gum |
| CN106835753A (en) * | 2017-02-28 | 2017-06-13 | 山东洁晶集团股份有限公司 | Printing gum and use its printing method |
| CN108049207A (en) * | 2017-12-20 | 2018-05-18 | 苏州润弘贸易有限公司 | Composite reactive printing gum |
| CN108060591A (en) * | 2017-12-15 | 2018-05-22 | 青岛明月海藻集团有限公司 | A kind of sodium alginate and its preparation method and application |
| CN108691222A (en) * | 2018-06-08 | 2018-10-23 | 山东拓普精化有限公司 | A kind of novel active printing gum |
| CN108708192A (en) * | 2018-06-08 | 2018-10-26 | 山东港源海洋生物工程有限公司 | A kind of reactive printing gum and preparation method thereof |
| CN108951217A (en) * | 2018-06-07 | 2018-12-07 | 山东港源海洋生物工程有限公司 | A kind of sodium alga acid printing paste and its preparation process |
| CN108951227A (en) * | 2018-06-08 | 2018-12-07 | 山东拓普精化有限公司 | A kind of silk printing gum based on substitution guar gum preparation |
| CN110981989A (en) * | 2019-12-19 | 2020-04-10 | 青岛聚大洋藻业集团有限公司 | Production process of sodium alginate with low calcium content |
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103469618A (en) * | 2013-09-06 | 2013-12-25 | 浙江华东纺织印染有限公司 | Non-urea reactive dye printing paste, manufacturing method and printing and dyeing method |
| CN104141243A (en) * | 2014-07-28 | 2014-11-12 | 绍兴县彩色橼纺织科技有限公司 | Three-dimensional printing paste |
| CN105386338A (en) * | 2015-12-14 | 2016-03-09 | 青岛明月海藻集团有限公司 | Preparation method of instant sodium alginate printing gum |
| CN106835753A (en) * | 2017-02-28 | 2017-06-13 | 山东洁晶集团股份有限公司 | Printing gum and use its printing method |
| CN106835753B (en) * | 2017-02-28 | 2019-02-19 | 山东洁晶集团股份有限公司 | Printing gum and the printing method for using it |
| CN108060591A (en) * | 2017-12-15 | 2018-05-22 | 青岛明月海藻集团有限公司 | A kind of sodium alginate and its preparation method and application |
| CN108049207A (en) * | 2017-12-20 | 2018-05-18 | 苏州润弘贸易有限公司 | Composite reactive printing gum |
| CN108951217A (en) * | 2018-06-07 | 2018-12-07 | 山东港源海洋生物工程有限公司 | A kind of sodium alga acid printing paste and its preparation process |
| CN108691222A (en) * | 2018-06-08 | 2018-10-23 | 山东拓普精化有限公司 | A kind of novel active printing gum |
| CN108708192A (en) * | 2018-06-08 | 2018-10-26 | 山东港源海洋生物工程有限公司 | A kind of reactive printing gum and preparation method thereof |
| CN108951227A (en) * | 2018-06-08 | 2018-12-07 | 山东拓普精化有限公司 | A kind of silk printing gum based on substitution guar gum preparation |
| CN110981989A (en) * | 2019-12-19 | 2020-04-10 | 青岛聚大洋藻业集团有限公司 | Production process of sodium alginate with low calcium content |
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Address after: 266400 Shandong Province, Qingdao city Huangdao District Feiyu Road No. 118 Applicant after: QINGDAO JUDAYANG ALGAE INDUSTRY GROUP CO., LTD. Address before: 266000, No. two, 17 West Road, Jiaonan, Shandong, Shanghai, Qingdao Applicant before: Qingdao Gather Great Ocean Seaweed Industry Co., Ltd. |
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Free format text: CORRECT: APPLICANT; FROM: QINGDAO JUDAYANG SEAWEED INDUSTRY CO., LTD. TO: QINGDAO JUDAYANG ALGAE INDUSTRY GROUP CO., LTD. |
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Application publication date: 20120815 |