CN102634972A - Method for preparing seriously contaminated antique silk substitution sample - Google Patents
Method for preparing seriously contaminated antique silk substitution sample Download PDFInfo
- Publication number
- CN102634972A CN102634972A CN2012101193873A CN201210119387A CN102634972A CN 102634972 A CN102634972 A CN 102634972A CN 2012101193873 A CN2012101193873 A CN 2012101193873A CN 201210119387 A CN201210119387 A CN 201210119387A CN 102634972 A CN102634972 A CN 102634972A
- Authority
- CN
- China
- Prior art keywords
- habotai
- commercially available
- ozone
- pig
- days
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 title claims abstract description 11
- 238000006467 substitution reaction Methods 0.000 title abstract 2
- 235000015277 pork Nutrition 0.000 claims abstract description 13
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 claims abstract description 12
- 210000004185 liver Anatomy 0.000 claims abstract description 8
- 230000032683 aging Effects 0.000 claims abstract description 7
- 239000000203 mixture Substances 0.000 claims abstract description 7
- 239000008280 blood Substances 0.000 claims abstract description 6
- 210000004369 blood Anatomy 0.000 claims abstract description 6
- 235000013372 meat Nutrition 0.000 claims abstract description 4
- 230000005855 radiation Effects 0.000 claims abstract description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000004744 fabric Substances 0.000 claims description 20
- 238000002360 preparation method Methods 0.000 claims description 7
- 230000007306 turnover Effects 0.000 claims description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract description 8
- 229910052742 iron Inorganic materials 0.000 abstract description 4
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 abstract description 3
- 230000001678 irradiating effect Effects 0.000 abstract 1
- 238000007790 scraping Methods 0.000 abstract 1
- 238000002791 soaking Methods 0.000 abstract 1
- 238000004140 cleaning Methods 0.000 description 4
- 150000001413 amino acids Chemical class 0.000 description 1
- 210000001124 body fluid Anatomy 0.000 description 1
- 239000010839 body fluid Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000010186 staining Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Landscapes
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The invention discloses a method for preparing a seriously contaminated antique silk substitution sample. The method comprises the following steps of: A) putting commercially available habotai and a rusty iron product together in a humid environment for 10-15 days so that the commercially available habotai is stained with rust; B) soaking the commercially available habotai stained with rust in fresh pig blood for 12 h and then putting in a mixture of pig meat and pig liver according to a weight ratio of 1: (20-50), and standing for 5-7 days at a cool airtight place, wherein the mixture contains pig fat, pork lean, pig liver and water in a ratio of 2: 1: 1: 4; C) taking out of the commercially available habotai, scraping carrion attached to the surface of the habotai, performing aging treatment on the contaminated sample in a double aging way of ultraviolet rays and ozone, irradiating by means of an ultraviolet treatment box at a radiation intensity of 4000-4600 mu w/cm<2>, and simultaneously supplying ozone into the treatment box for 30 min every hour, wherein the ozone output quantity is 400 mg/h; and turning over the treated commercially available habotai every hour and treating the habotai for 50-80 hours. Compared with the prior art, the method is capable of simulating a cultural relic authentically, simple in operation and low in cost.
Description
Technical field
The invention belongs to the Techniques of Relics Protection field, be specifically related to the preparation method that a kind of serious pollution silk fabric cultural relics substitutes appearance.
Background technology
Silk is the important element of Chinese civilization, and silk fabric cultural relics has great historical value, artistic value, scientific value as the indispensable important carrier of research ancient civilization.
Because of burying the influence that receives various factors in underground or of the remote past for a long time; It is serious that the pollution of many unearthed silk fabric cultural relics destroys situation, the rust staining pollution that for example organic substances such as blood fat protein that decompose of corpse pollute, ironware etc. produces in the buring environment etc.The historical relic's protection worker often because of reasons such as pollutant component are complicated, seriously polluted, the poor rotten intensity of historical relic is low, occurs cleaning difficult even increases the weight of the situation of historical relic destructiveness in cleaning process when cleaning silk fabric cultural relics.Therefore, bury the issuable pollution of process according to silk fabric cultural relics and prepare the serious pollution historical relic and substitute appearance, try to clean and effect assessment after to clean silk fabric cultural relics again be very necessary.
At present, the researcher's silk fabrics that will pass through burin-in process replaces silk fabric cultural relics to study relatively having obtained good effect.But substitute appearance for polluting silk fabric cultural relics, also nobody relates to particularly to substitute the preparation of appearance to the difficult silk fabric cultural relics of washing serious pollution, and it is extremely important that the serious pollution silk fabric cultural relics that therefore the present invention relates to substitutes the preparation method of appearance.
Summary of the invention
The present invention is intended to replenish the deficiency that the existing resist technology field of silk fabric cultural relics exists, and proposes the preparation method that a kind of serious pollution silk fabric cultural relics substitutes appearance.
For this reason, the technical scheme of the present invention's employing is such:
A kind of serious pollution silk fabric cultural relics substitutes the preparation method of appearance, may further comprise the steps:
A) commercially available habotai and the ironwork that gets rusty are mixed together were placed on wet environment 10～15 days, make commercially available habotai be infected with rusty stain;
B) the commercially available habotai that will be infected with rusty stain is immersed in 12h in the fresh pig blood, puts into pork pork liver mixture with weight ratio 1: 20～50 then, and left standstill 5～7 days at airtight place in the cool place; This mixture is a pig fat meat: lean pork: pork liver: water=2: 1: 1: 4;
C) take out this commercially available habotai; Scrape off the slough of surface attachment; Adopt ultraviolet ray to add the aging mode of ozone double with the sample burin-in process of being polluted, utilize the irradiation of UV treatment case, radiation intensity is 4000-4600 μ w/cm2; While is delivery of ozone 30min in treatment box per hour, and the ozone output quantity is 400mg/h; Each hour to the commercially available habotai turn-over of being handled once handled 50 to 80 hours.
The present invention mixes habotai to be placed on the iron block that gets rusty earlier makes it to catch rusty stain in the wet environment; Rot to pollute with body fluid tissues such as mammiferous blood, albumen then, adopt ultraviolet to add the aging mode of ozone double at last the aging serious pollution historical relic that obtains of the sample that is polluted is substituted appearance.Compared with prior art, have and more truly simulate historical relic, simple to operate, characteristics that cost is low.
Through amino acid, testing result such as infrared shows that it is all comparatively similar on institutional framework and composition with silk fabric cultural relics that the historical relic that the present invention handles substitutes appearance, is a kind of good ageing method.Owing in advance silk fabrics has been carried out the serious pollution processing, resulting sample is truer, can be advantageously applied in the middle of the research of silk fabric cultural relics cleaning.
The specific embodiment
A) buy power and spin 1kg, it is some to get the iron nail, the iron wire that have got rusty, through modes such as coating, pile up both is mixed placement, places two weeks of wet environment;
B) take out this habotai, be immersed in 12h in the fresh pig blood;
C) buy pork, pork liver etc., with pig fat meat: lean pork: pork liver: water=2: 1: 1: 4 mixed must about 30kg, and aforesaid habotai is put into wherein, and a week is left standstill at airtight place in the cool place;
D) take out this habotai, scrape off the slough of surface attachment, put into the irradiation of UV treatment case, radiation intensity is 4000-4600 μ w/cm2, and the while is delivery of ozone 30min in treatment box per hour, and the ozone output quantity is 400mg/h; Each hour to the habotai turn-over of being handled once handled 50 hours;
E) obtain required silk fabric cultural relics and substitute appearance.
Claims (1)
1. a serious pollution silk fabric cultural relics substitutes the preparation method of appearance, may further comprise the steps:
A) commercially available habotai and the ironwork that gets rusty are mixed together were placed on wet environment 10～15 days, make commercially available habotai be infected with rusty stain;
B) the commercially available habotai that will be infected with rusty stain is immersed in 12h in the fresh pig blood, puts into pork pork liver mixture with weight ratio 1: 20～50 then, and left standstill 5～7 days at airtight place in the cool place; This mixture is a pig fat meat: lean pork: pork liver: water=2: 1: 1: 4;
C) take out this commercially available habotai; Scrape off the slough of surface attachment; Adopt ultraviolet ray to add the aging mode of ozone double with the sample burin-in process of being polluted, utilize the irradiation of UV treatment case, radiation intensity is 4000-4600 μ w/cm2; While is delivery of ozone 30min in treatment box per hour, and the ozone output quantity is 400mg/h; Each hour to the commercially available habotai turn-over of being handled once handled 50 to 80 hours.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201210119387 CN102634972B (en) | 2012-04-20 | 2012-04-20 | Method for preparing seriously contaminated antique silk substitution sample |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201210119387 CN102634972B (en) | 2012-04-20 | 2012-04-20 | Method for preparing seriously contaminated antique silk substitution sample |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102634972A true CN102634972A (en) | 2012-08-15 |
| CN102634972B CN102634972B (en) | 2013-09-11 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201210119387 Expired - Fee Related CN102634972B (en) | 2012-04-20 | 2012-04-20 | Method for preparing seriously contaminated antique silk substitution sample |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102634972B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104342918A (en) * | 2014-10-30 | 2015-02-11 | 浙江理工大学 | Artificial-accelerated simulated preparation method of multifactor aged wool samples |
| CN107328843A (en) * | 2017-07-21 | 2017-11-07 | 浙江理工大学 | It is a kind of to simulate the method for removing ancient times wool fabric exogenous strontium |
| CN107386000A (en) * | 2017-08-14 | 2017-11-24 | 上海大学 | A kind of fragile organic matter historical relic extraction, reinforce and protect and use analog sample preparation method |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101613937A (en) * | 2009-08-10 | 2009-12-30 | 浙江理工大学 | The bionical method for strengthening of silk-fibroin compound system of silk historical relic |
| CN102102291A (en) * | 2010-12-13 | 2011-06-22 | 首都博物馆 | Method for cooperatively cleaning blood stains on silk cultural relic by using protease and surfactant |
| CN102409541A (en) * | 2011-08-18 | 2012-04-11 | 浙江理工大学 | Preparation method of uncovering agent for silk fabrics solidified with iron rust, copper rust and soil rust |
-
2012
- 2012-04-20 CN CN 201210119387 patent/CN102634972B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101613937A (en) * | 2009-08-10 | 2009-12-30 | 浙江理工大学 | The bionical method for strengthening of silk-fibroin compound system of silk historical relic |
| CN102102291A (en) * | 2010-12-13 | 2011-06-22 | 首都博物馆 | Method for cooperatively cleaning blood stains on silk cultural relic by using protease and surfactant |
| CN102409541A (en) * | 2011-08-18 | 2012-04-11 | 浙江理工大学 | Preparation method of uncovering agent for silk fabrics solidified with iron rust, copper rust and soil rust |
Non-Patent Citations (5)
| Title |
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| "FE、CU对丝绸保存状况的影响": "张晓梅等", 《文物保护与考古科学》 * |
| 《中国优秀博硕士学位论文全文数据库 哲学与人文科学辑》 20041020 孔旭 "古代纺织品的保护_丝织品文物清洁及贮藏的研究" 第38-39页 1 , 第03期 * |
| 《长江大学学报（自然科学版）》 20110930 郭敏等 "丝织品的氙灯光老化及污布制作观察" 第248-251页 1 第８卷, 第９期 * |
| 孔旭: ""古代纺织品的保护_丝织品文物清洁及贮藏的研究"", 《中国优秀博硕士学位论文全文数据库 哲学与人文科学辑》 * |
| 郭敏等: ""丝织品的氙灯光老化及污布制作观察"", 《长江大学学报（自然科学版）》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104342918A (en) * | 2014-10-30 | 2015-02-11 | 浙江理工大学 | Artificial-accelerated simulated preparation method of multifactor aged wool samples |
| CN107328843A (en) * | 2017-07-21 | 2017-11-07 | 浙江理工大学 | It is a kind of to simulate the method for removing ancient times wool fabric exogenous strontium |
| CN107386000A (en) * | 2017-08-14 | 2017-11-24 | 上海大学 | A kind of fragile organic matter historical relic extraction, reinforce and protect and use analog sample preparation method |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102634972B (en) | 2013-09-11 |
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Granted publication date: 20130911 Termination date: 20140420 |