CN102626092A - 治疗根结线虫的印楝素水溶剂及其制备方法 - Google Patents
治疗根结线虫的印楝素水溶剂及其制备方法 Download PDFInfo
- Publication number
- CN102626092A CN102626092A CN201210067320XA CN201210067320A CN102626092A CN 102626092 A CN102626092 A CN 102626092A CN 201210067320X A CN201210067320X A CN 201210067320XA CN 201210067320 A CN201210067320 A CN 201210067320A CN 102626092 A CN102626092 A CN 102626092A
- Authority
- CN
- China
- Prior art keywords
- nimbin
- root
- knot nematode
- azadirachtin
- soil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 241000243785 Meloidogyne javanica Species 0.000 title claims abstract description 63
- 238000002360 preparation method Methods 0.000 title claims abstract description 20
- 201000010099 disease Diseases 0.000 title abstract description 20
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 title abstract description 20
- FTNJWQUOZFUQQJ-IRYYUVNJSA-N azadirachtin A Natural products C([C@@H]([C@]1(C=CO[C@H]1O1)O)[C@]2(C)O3)[C@H]1[C@]23[C@]1(C)[C@H](O)[C@H](OC[C@@]2([C@@H](C[C@@H]3OC(=O)C(\C)=C/C)OC(C)=O)C(=O)OC)[C@@H]2[C@]32CO[C@@](C(=O)OC)(O)[C@@H]12 FTNJWQUOZFUQQJ-IRYYUVNJSA-N 0.000 title abstract description 12
- FTNJWQUOZFUQQJ-NDAWSKJSSA-N azadirachtin A Chemical compound C([C@@H]([C@]1(C=CO[C@H]1O1)O)[C@]2(C)O3)[C@H]1[C@]23[C@]1(C)[C@H](O)[C@H](OC[C@@]2([C@@H](C[C@@H]3OC(=O)C(\C)=C\C)OC(C)=O)C(=O)OC)[C@@H]2[C@]32CO[C@@](C(=O)OC)(O)[C@@H]12 FTNJWQUOZFUQQJ-NDAWSKJSSA-N 0.000 title abstract description 12
- 239000005878 Azadirachtin Substances 0.000 title abstract description 9
- VEHPJKVTJQSSKL-UHFFFAOYSA-N azadirachtin Natural products O1C2(C)C(C3(C=COC3O3)O)CC3C21C1(C)C(O)C(OCC2(OC(C)=O)C(CC3OC(=O)C(C)=CC)OC(C)=O)C2C32COC(C(=O)OC)(O)C12 VEHPJKVTJQSSKL-UHFFFAOYSA-N 0.000 title abstract description 9
- 239000007864 aqueous solution Substances 0.000 title abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 42
- 238000003756 stirring Methods 0.000 claims abstract description 10
- NHOIBRJOQAYBJT-IMGVWCFESA-N nimbin Chemical compound C=1([C@@H]2C[C@H]3O[C@H]4[C@](C3=C2C)(C)[C@@H]([C@]2(C(=O)C=C[C@](C)([C@@H]2[C@H]4OC(C)=O)C(=O)OC)C)CC(=O)OC)C=COC=1 NHOIBRJOQAYBJT-IMGVWCFESA-N 0.000 claims description 172
- ZQIYJHBQRBBBRZ-UHFFFAOYSA-N nimbin Natural products COC(=O)CC1C2C(C(OC(=O)C)C3OC4CC(C(=C4C13C)C)c5cocc5)C(C)(C=CC2=O)C(=O)OC ZQIYJHBQRBBBRZ-UHFFFAOYSA-N 0.000 claims description 172
- 239000003125 aqueous solvent Substances 0.000 claims description 56
- 238000011282 treatment Methods 0.000 claims description 29
- 239000002994 raw material Substances 0.000 claims description 11
- 239000002689 soil Substances 0.000 abstract description 57
- 230000000694 effects Effects 0.000 abstract description 25
- 239000000575 pesticide Substances 0.000 abstract description 6
- 230000015556 catabolic process Effects 0.000 abstract description 3
- 238000006731 degradation reaction Methods 0.000 abstract description 3
- 230000006872 improvement Effects 0.000 abstract description 3
- KAJFOBKSQVMLSY-UHFFFAOYSA-N azadirachtin B Natural products COC(=O)C1(O)OCC23C(O)CC(OC(=O)C(=CC)C)C4(COC(C(O)C(C)(C12)C56OC5(C)C7CC6OC8OC=CC78O)C34)C(=O)OC KAJFOBKSQVMLSY-UHFFFAOYSA-N 0.000 abstract 3
- FTNJWQUOZFUQQJ-UZTPERQESA-N azadirachtin B Chemical compound C([C@@H]([C@]1(C=CO[C@H]1O1)O)[C@]2(C)O3)[C@H]1[C@]23[C@]1(C)[C@H](O)[C@H](OC[C@@]2([C@@H](C[C@H]3OC(=O)C(\C)=C\C)OC(C)=O)C(=O)OC)[C@@H]2[C@]32CO[C@@](C(=O)OC)(O)[C@@H]12 FTNJWQUOZFUQQJ-UZTPERQESA-N 0.000 abstract 3
- 206010059866 Drug resistance Diseases 0.000 abstract 1
- 241000238631 Hexapoda Species 0.000 description 23
- 241000196324 Embryophyta Species 0.000 description 17
- 239000000839 emulsion Substances 0.000 description 17
- 235000013399 edible fruits Nutrition 0.000 description 15
- 238000012360 testing method Methods 0.000 description 13
- 240000009088 Fragaria x ananassa Species 0.000 description 12
- 238000000034 method Methods 0.000 description 12
- 235000016623 Fragaria vesca Nutrition 0.000 description 11
- 235000011363 Fragaria x ananassa Nutrition 0.000 description 11
- 240000000233 Melia azedarach Species 0.000 description 10
- 235000007688 Lycopersicon esculentum Nutrition 0.000 description 9
- 240000003768 Solanum lycopersicum Species 0.000 description 9
- 230000008859 change Effects 0.000 description 9
- 230000012010 growth Effects 0.000 description 9
- 241000244206 Nematoda Species 0.000 description 8
- 240000007087 Apium graveolens Species 0.000 description 7
- 235000015849 Apium graveolens Dulce Group Nutrition 0.000 description 7
- 235000010591 Appio Nutrition 0.000 description 7
- 240000008067 Cucumis sativus Species 0.000 description 7
- 235000010799 Cucumis sativus var sativus Nutrition 0.000 description 7
- 239000003814 drug Substances 0.000 description 7
- 239000000203 mixture Substances 0.000 description 7
- 239000000126 substance Substances 0.000 description 7
- 235000013311 vegetables Nutrition 0.000 description 7
- 238000005516 engineering process Methods 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 239000002366 mineral element Substances 0.000 description 6
- 241000233866 Fungi Species 0.000 description 5
- 230000000443 biocontrol Effects 0.000 description 5
- 230000007613 environmental effect Effects 0.000 description 5
- 239000005645 nematicide Substances 0.000 description 5
- 230000003449 preventive effect Effects 0.000 description 5
- 241000894006 Bacteria Species 0.000 description 4
- 241000607479 Yersinia pestis Species 0.000 description 4
- 238000009395 breeding Methods 0.000 description 4
- 230000001488 breeding effect Effects 0.000 description 4
- 229940079593 drug Drugs 0.000 description 4
- 235000013305 food Nutrition 0.000 description 4
- 230000036039 immunity Effects 0.000 description 4
- 239000002917 insecticide Substances 0.000 description 4
- 230000007774 longterm Effects 0.000 description 4
- 238000012545 processing Methods 0.000 description 4
- 238000003860 storage Methods 0.000 description 4
- 241000186361 Actinobacteria <class> Species 0.000 description 3
- 240000005343 Azadirachta indica Species 0.000 description 3
- 208000005374 Poisoning Diseases 0.000 description 3
- 239000003905 agrochemical Substances 0.000 description 3
- 230000001580 bacterial effect Effects 0.000 description 3
- 238000003967 crop rotation Methods 0.000 description 3
- 230000006378 damage Effects 0.000 description 3
- 238000013461 design Methods 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- 230000018109 developmental process Effects 0.000 description 3
- 230000005611 electricity Effects 0.000 description 3
- 210000002468 fat body Anatomy 0.000 description 3
- 230000035558 fertility Effects 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 230000010534 mechanism of action Effects 0.000 description 3
- 244000005700 microbiome Species 0.000 description 3
- 230000035699 permeability Effects 0.000 description 3
- 231100000572 poisoning Toxicity 0.000 description 3
- 230000000607 poisoning effect Effects 0.000 description 3
- 108090000623 proteins and genes Proteins 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 208000035240 Disease Resistance Diseases 0.000 description 2
- 102000002322 Egg Proteins Human genes 0.000 description 2
- 108010000912 Egg Proteins Proteins 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 235000013500 Melia azadirachta Nutrition 0.000 description 2
- 241001465754 Metazoa Species 0.000 description 2
- 244000088415 Raphanus sativus Species 0.000 description 2
- 235000006140 Raphanus sativus var sativus Nutrition 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 230000000853 biopesticidal effect Effects 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000013043 chemical agent Substances 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 239000012895 dilution Substances 0.000 description 2
- 238000010790 dilution Methods 0.000 description 2
- 238000003912 environmental pollution Methods 0.000 description 2
- 239000000284 extract Substances 0.000 description 2
- 210000000087 hemolymph Anatomy 0.000 description 2
- 230000005764 inhibitory process Effects 0.000 description 2
- 231100000053 low toxicity Toxicity 0.000 description 2
- 230000007246 mechanism Effects 0.000 description 2
- 238000000386 microscopy Methods 0.000 description 2
- 239000005416 organic matter Substances 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 210000004681 ovum Anatomy 0.000 description 2
- 230000024241 parasitism Effects 0.000 description 2
- 230000002265 prevention Effects 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 239000004016 soil organic matter Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 238000002560 therapeutic procedure Methods 0.000 description 2
- 231100000419 toxicity Toxicity 0.000 description 2
- 230000001988 toxicity Effects 0.000 description 2
- 150000003648 triterpenes Chemical class 0.000 description 2
- 239000002569 water oil cream Substances 0.000 description 2
- HDTRYLNUVZCQOY-UHFFFAOYSA-N α-D-glucopyranosyl-α-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OC1C(O)C(O)C(O)C(CO)O1 HDTRYLNUVZCQOY-UHFFFAOYSA-N 0.000 description 1
- IKJQENAHDRKFKL-UHFFFAOYSA-N 3-Epimeliantriol Natural products OC1OC(C(O)C(C)(O)C)CC1C1C2(C)CCC3C4(C)CCC(O)C(C)(C)C4CC=C3C2(C)CC1 IKJQENAHDRKFKL-UHFFFAOYSA-N 0.000 description 1
- 241000234282 Allium Species 0.000 description 1
- 235000005254 Allium ampeloprasum Nutrition 0.000 description 1
- 240000006108 Allium ampeloprasum Species 0.000 description 1
- 235000002732 Allium cepa var. cepa Nutrition 0.000 description 1
- 240000002234 Allium sativum Species 0.000 description 1
- 239000004382 Amylase Substances 0.000 description 1
- 102000013142 Amylases Human genes 0.000 description 1
- 108010065511 Amylases Proteins 0.000 description 1
- 241001124076 Aphididae Species 0.000 description 1
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 1
- 208000035143 Bacterial infection Diseases 0.000 description 1
- 235000006008 Brassica napus var napus Nutrition 0.000 description 1
- 235000011299 Brassica oleracea var botrytis Nutrition 0.000 description 1
- 235000001169 Brassica oleracea var oleracea Nutrition 0.000 description 1
- 240000003259 Brassica oleracea var. botrytis Species 0.000 description 1
- 235000010149 Brassica rapa subsp chinensis Nutrition 0.000 description 1
- 235000000536 Brassica rapa subsp pekinensis Nutrition 0.000 description 1
- 241000499436 Brassica rapa subsp. pekinensis Species 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 235000002566 Capsicum Nutrition 0.000 description 1
- 240000008574 Capsicum frutescens Species 0.000 description 1
- 241001674939 Caulanthus Species 0.000 description 1
- 241001465977 Coccoidea Species 0.000 description 1
- 241000254173 Coleoptera Species 0.000 description 1
- 241001427559 Collembola Species 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 235000005983 Crescentia cujete Nutrition 0.000 description 1
- 241000219112 Cucumis Species 0.000 description 1
- 235000015510 Cucumis melo subsp melo Nutrition 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 108090000371 Esterases Proteins 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- 229920002527 Glycogen Polymers 0.000 description 1
- 244000299452 Gouania lupuloides Species 0.000 description 1
- 235000000292 Gouania lupuloides Nutrition 0.000 description 1
- 241000255967 Helicoverpa zea Species 0.000 description 1
- 240000008415 Lactuca sativa Species 0.000 description 1
- 235000003228 Lactuca sativa Nutrition 0.000 description 1
- 240000007741 Lagenaria siceraria Species 0.000 description 1
- 235000009797 Lagenaria vulgaris Nutrition 0.000 description 1
- 241000255777 Lepidoptera Species 0.000 description 1
- 102000004882 Lipase Human genes 0.000 description 1
- 108090001060 Lipase Proteins 0.000 description 1
- 239000004367 Lipase Substances 0.000 description 1
- 241000594033 Liriomyza bryoniae Species 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 241000158723 Melia Species 0.000 description 1
- 241000243784 Meloidogyne arenaria Species 0.000 description 1
- 241000243787 Meloidogyne hapla Species 0.000 description 1
- 241000243786 Meloidogyne incognita Species 0.000 description 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
- 108091005804 Peptidases Proteins 0.000 description 1
- 244000046052 Phaseolus vulgaris Species 0.000 description 1
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 1
- 102000004160 Phosphoric Monoester Hydrolases Human genes 0.000 description 1
- 108090000608 Phosphoric Monoester Hydrolases Proteins 0.000 description 1
- 241000242594 Platyhelminthes Species 0.000 description 1
- 239000004365 Protease Substances 0.000 description 1
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 description 1
- 241000606701 Rickettsia Species 0.000 description 1
- 241001419253 Spathiphyllum cochlearispathum Species 0.000 description 1
- 241001454293 Tetranychus urticae Species 0.000 description 1
- 241001414989 Thysanoptera Species 0.000 description 1
- HDTRYLNUVZCQOY-WSWWMNSNSA-N Trehalose Natural products O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-WSWWMNSNSA-N 0.000 description 1
- 241000700605 Viruses Species 0.000 description 1
- 241001532014 Xanthorrhoea Species 0.000 description 1
- FJJCIZWZNKZHII-UHFFFAOYSA-N [4,6-bis(cyanoamino)-1,3,5-triazin-2-yl]cyanamide Chemical compound N#CNC1=NC(NC#N)=NC(NC#N)=N1 FJJCIZWZNKZHII-UHFFFAOYSA-N 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000011149 active material Substances 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- HDTRYLNUVZCQOY-LIZSDCNHSA-N alpha,alpha-trehalose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-LIZSDCNHSA-N 0.000 description 1
- 235000019418 amylase Nutrition 0.000 description 1
- 230000008485 antagonism Effects 0.000 description 1
- 239000003242 anti bacterial agent Substances 0.000 description 1
- 230000001887 anti-feedant effect Effects 0.000 description 1
- 230000002609 anti-worm Effects 0.000 description 1
- 229940088710 antibiotic agent Drugs 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 229960005070 ascorbic acid Drugs 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 208000022362 bacterial infectious disease Diseases 0.000 description 1
- 239000011324 bead Substances 0.000 description 1
- 230000006399 behavior Effects 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 210000004556 brain Anatomy 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 239000001390 capsicum minimum Substances 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 238000012512 characterization method Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 229930002875 chlorophyll Natural products 0.000 description 1
- 235000019804 chlorophyll Nutrition 0.000 description 1
- ATNHDLDRLWWWCB-AENOIHSZSA-M chlorophyll a Chemical compound C1([C@@H](C(=O)OC)C(=O)C2=C3C)=C2N2C3=CC(C(CC)=C3C)=[N+]4C3=CC3=C(C=C)C(C)=C5N3[Mg-2]42[N+]2=C1[C@@H](CCC(=O)OC\C=C(/C)CCC[C@H](C)CCC[C@H](C)CCCC(C)C)[C@H](C)C2=C5 ATNHDLDRLWWWCB-AENOIHSZSA-M 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 238000005056 compaction Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 210000002251 corpora allata Anatomy 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 229930004069 diterpene Natural products 0.000 description 1
- 125000000567 diterpene group Chemical group 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 230000007914 freezing tolerance Effects 0.000 description 1
- 230000005078 fruit development Effects 0.000 description 1
- 125000000524 functional group Chemical group 0.000 description 1
- 230000002538 fungal effect Effects 0.000 description 1
- 230000000855 fungicidal effect Effects 0.000 description 1
- 239000000417 fungicide Substances 0.000 description 1
- 235000004611 garlic Nutrition 0.000 description 1
- 210000004907 gland Anatomy 0.000 description 1
- 229940096919 glycogen Drugs 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 229940088597 hormone Drugs 0.000 description 1
- 239000005556 hormone Substances 0.000 description 1
- 230000036512 infertility Effects 0.000 description 1
- 208000000509 infertility Diseases 0.000 description 1
- 231100000535 infertility Toxicity 0.000 description 1
- 230000000749 insecticidal effect Effects 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 239000010985 leather Substances 0.000 description 1
- 150000002630 limonoids Chemical class 0.000 description 1
- 235000019421 lipase Nutrition 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 231100001225 mammalian toxicity Toxicity 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 244000000010 microbial pathogen Species 0.000 description 1
- 238000009335 monocropping Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 102000039446 nucleic acids Human genes 0.000 description 1
- 108020004707 nucleic acids Proteins 0.000 description 1
- 150000007523 nucleic acids Chemical class 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 235000014571 nuts Nutrition 0.000 description 1
- 210000003101 oviduct Anatomy 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 230000007170 pathology Effects 0.000 description 1
- 238000004181 pedogenesis Methods 0.000 description 1
- 230000029553 photosynthesis Effects 0.000 description 1
- 238000010672 photosynthesis Methods 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 230000008654 plant damage Effects 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 244000144977 poultry Species 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 235000019419 proteases Nutrition 0.000 description 1
- 210000004994 reproductive system Anatomy 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000000241 respiratory effect Effects 0.000 description 1
- 230000029058 respiratory gaseous exchange Effects 0.000 description 1
- 230000033764 rhythmic process Effects 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 239000002688 soil aggregate Substances 0.000 description 1
- 244000000000 soil microbiome Species 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000007790 solid phase Substances 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 150000003505 terpenes Chemical class 0.000 description 1
- 150000003534 tetranortriterpenoids Chemical class 0.000 description 1
- 230000001225 therapeutic effect Effects 0.000 description 1
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
Description
Claims (3)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 201210067320 CN102626092B (zh) | 2012-03-15 | 2012-03-15 | 治疗根结线虫的印楝素水溶剂及其制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 201210067320 CN102626092B (zh) | 2012-03-15 | 2012-03-15 | 治疗根结线虫的印楝素水溶剂及其制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN102626092A true CN102626092A (zh) | 2012-08-08 |
CN102626092B CN102626092B (zh) | 2013-09-11 |
Family
ID=46584624
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN 201210067320 Expired - Fee Related CN102626092B (zh) | 2012-03-15 | 2012-03-15 | 治疗根结线虫的印楝素水溶剂及其制备方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN102626092B (zh) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103371155A (zh) * | 2012-04-13 | 2013-10-30 | 辽宁绿禾农业有限公司 | 治疗果树根癌的印楝素水溶剂及其制备方法 |
CN104094980A (zh) * | 2014-08-06 | 2014-10-15 | 辽宁绿禾农业有限公司 | 治疗韭菜根蛆的印楝素水剂及其制备方法 |
CN108041051A (zh) * | 2017-12-18 | 2018-05-18 | 成都绿金生物科技有限责任公司 | 一种基于印楝素的药肥及其制备方法 |
CN114451427A (zh) * | 2022-02-22 | 2022-05-10 | 合肥高尔生命健康科学研究院有限公司 | 一种含有印楝籽提取物和松脂酸铜的农药杀虫剂 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1593138A (zh) * | 2004-06-18 | 2005-03-16 | 华南农业大学 | 印楝素与氟螨脲混配乳油 |
CN1240290C (zh) * | 2000-04-07 | 2006-02-08 | E·I·D·帕里(印度)有限公司 | 含印度楝种子提取物和糖的组合物 |
CN101703076A (zh) * | 2009-09-22 | 2010-05-12 | 成都绿金高新技术股份有限公司 | 印楝素通用油剂 |
RU2433589C1 (ru) * | 2010-03-30 | 2011-11-20 | Орлов Евгений Александрович | Способ борьбы с личинками кровососущих насекомых |
-
2012
- 2012-03-15 CN CN 201210067320 patent/CN102626092B/zh not_active Expired - Fee Related
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1240290C (zh) * | 2000-04-07 | 2006-02-08 | E·I·D·帕里(印度)有限公司 | 含印度楝种子提取物和糖的组合物 |
CN1593138A (zh) * | 2004-06-18 | 2005-03-16 | 华南农业大学 | 印楝素与氟螨脲混配乳油 |
CN101703076A (zh) * | 2009-09-22 | 2010-05-12 | 成都绿金高新技术股份有限公司 | 印楝素通用油剂 |
RU2433589C1 (ru) * | 2010-03-30 | 2011-11-20 | Орлов Евгений Александрович | Способ борьбы с личинками кровососущих насекомых |
Non-Patent Citations (2)
Title |
---|
张志祥等: "印楝素A和印楝素B的生物活性及增效作用", 《华中农业大学学报》 * |
张志祥等: "印楝素A和印楝素B的稳定性比较", 《南京农业大学学报》 * |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103371155A (zh) * | 2012-04-13 | 2013-10-30 | 辽宁绿禾农业有限公司 | 治疗果树根癌的印楝素水溶剂及其制备方法 |
CN104094980A (zh) * | 2014-08-06 | 2014-10-15 | 辽宁绿禾农业有限公司 | 治疗韭菜根蛆的印楝素水剂及其制备方法 |
CN108041051A (zh) * | 2017-12-18 | 2018-05-18 | 成都绿金生物科技有限责任公司 | 一种基于印楝素的药肥及其制备方法 |
CN114451427A (zh) * | 2022-02-22 | 2022-05-10 | 合肥高尔生命健康科学研究院有限公司 | 一种含有印楝籽提取物和松脂酸铜的农药杀虫剂 |
Also Published As
Publication number | Publication date |
---|---|
CN102626092B (zh) | 2013-09-11 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
Sileshi et al. | Integrating ethno-ecological and scientific knowledge of termites for sustainable termite management and human welfare in Africa | |
Hershenhorn et al. | Weed biocontrol with fungi: past, present and future | |
BR112020014469A2 (pt) | materiais e métodos para tratamento de infecções bacterianas em plantas | |
Sinha et al. | Organic farming by vermiculture: producing safe, nutritive and protective foods by earthworms (Charles Darwin's friends of farmers). | |
JPWO2012124665A1 (ja) | 植物の育成方法およびそれに使用する組成物 | |
CN102077846A (zh) | 一种含阿维菌素和淡紫拟青霉的杀线虫组合物 | |
Sampathkumar et al. | Marine microalgal extracts on cultivable crops as a considerable bio-fertilizer: A Review | |
KR20140040896A (ko) | 은행잎 물 숙성물을 함유하는 살충제 또는 비료 조성물 | |
US10264792B2 (en) | Holistic, cost effective method for management of huang long bing (HLB), phytophthora gummosis, asian citrus psyllid and other serious infestations in citrus and other crops | |
Sinha et al. | Vermiculture for organic horticulture: Producing chemical-free, nutritive & health protective foods by earthworms | |
CN102626092B (zh) | 治疗根结线虫的印楝素水溶剂及其制备方法 | |
Singh et al. | Field efficacy of certain microbial insecticides against Plutella xylostella Linnaeus and Pieris brassicae Linnaeus under cabbage-crop-ecosystem of Manipur | |
CN106508991A (zh) | 一种生物农药及其制备方法 | |
DE602004002293T2 (de) | Eine synergistische fermentierte pflanzenwachstumsfördernde, biokontrolle-zusammensetzung | |
Keshari et al. | Plant parasitic nematodes: a major constraint in fruit production | |
CN102657155A (zh) | 一种锯木屑作载体的杀线虫颗粒剂及其制备方法 | |
CN104663728A (zh) | 防治植物病害的微生物农药组合物 | |
Kumawat et al. | Formulation of biopesticides for insect pests and diseases management in organic farming | |
CN103371155A (zh) | 治疗果树根癌的印楝素水溶剂及其制备方法 | |
Hashem et al. | Impact of some safe agricultural treatments on insect pests, vascular wilt disease management and Roselle (Hibiscus sabdariffa L.) productivity under Siwa Oasis conditions | |
Ali et al. | Response of growth, yield and fruit quality of tomato (Solanum Lycopersicum L.) to different organic fertilizer treatments under two pest control programs against Tuta absoluta in a new valley-Egypt | |
Choudhary et al. | Rhizosphere: Hotspot of soil-microbes-plant interaction | |
Abada et al. | Effect of the combination among compost, bioagents andsoilsolarization on management of strawberry Verticillium wilt | |
Percival et al. | Evaluation of organic, synthetic and physical insecticides for the control of horse chestnut leaf miner (Cameraria ohridella) | |
KR101638833B1 (ko) | 식물 병원균에 대한 항진균 활성 및 대취 분해능을 갖는 리소박터 굼모서스 균주와 이를 함유한 미생물 제제 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
C56 | Change in the name or address of the patentee | ||
CB03 | Change of inventor or designer information |
Inventor after: Liu Ming Inventor after: Zhou Wei Inventor after: Lv Hongyang Inventor before: Liu Ming Inventor before: Ji Mingshan Inventor before: Zhou Wei Inventor before: Lv Hongyang |
|
COR | Change of bibliographic data | ||
CP03 | Change of name, title or address |
Address after: 110000 Liaoning province Shenyang Hunnan Fumin Street 11 No. -1 Patentee after: Liaoning green grain agriculture Limited by Share Ltd. Address before: 110000, Xintiandi, Heping Road, Heping Road, Heping District, Liaoning, Shenyang, room 2302, SOHO Patentee before: LIAONING LYUHE AGRICULTURE Co.,Ltd. |
|
C56 | Change in the name or address of the patentee | ||
CP01 | Change in the name or title of a patent holder |
Address after: 110000 Liaoning province Shenyang Hunnan Fumin Street 11 No. -1 Patentee after: Liaoning Green Wo agricultural science and technology development Limited by Share Ltd. Address before: 110000 Liaoning province Shenyang Hunnan Fumin Street 11 No. -1 Patentee before: Liaoning green grain agriculture Limited by Share Ltd. |
|
CF01 | Termination of patent right due to non-payment of annual fee | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20130911 |