CN102618256A - High frequency electronic discharge lamp water coating powder for machine spray coating and preparation and spray coating method thereof - Google Patents

High frequency electronic discharge lamp water coating powder for machine spray coating and preparation and spray coating method thereof Download PDF

Info

Publication number
CN102618256A
CN102618256A CN2012100513215A CN201210051321A CN102618256A CN 102618256 A CN102618256 A CN 102618256A CN 2012100513215 A CN2012100513215 A CN 2012100513215A CN 201210051321 A CN201210051321 A CN 201210051321A CN 102618256 A CN102618256 A CN 102618256A
Authority
CN
China
Prior art keywords
powder
spray coating
high frequency
dusting
frequency electronic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN2012100513215A
Other languages
Chinese (zh)
Inventor
林伟河
吴克锐
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
GUANGDONG SHUNXIANG ENERGY-SAVING LIGHTING TECHNOLOGY Co Ltd
Original Assignee
GUANGDONG SHUNXIANG ENERGY-SAVING LIGHTING TECHNOLOGY Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by GUANGDONG SHUNXIANG ENERGY-SAVING LIGHTING TECHNOLOGY Co Ltd filed Critical GUANGDONG SHUNXIANG ENERGY-SAVING LIGHTING TECHNOLOGY Co Ltd
Priority to CN2012100513215A priority Critical patent/CN102618256A/en
Publication of CN102618256A publication Critical patent/CN102618256A/en
Priority to PCT/CN2012/086409 priority patent/WO2013127226A1/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K11/00Luminescent, e.g. electroluminescent, chemiluminescent materials
    • C09K11/02Use of particular materials as binders, particle coatings or suspension media therefor
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K11/00Luminescent, e.g. electroluminescent, chemiluminescent materials
    • C09K11/08Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials

Abstract

The invention discloses high frequency electronic discharge lamp water coating powder for machine spray coating and a preparation and spray coating method thereof. The high frequency electronic discharge lamp water coating powder is composed of nanometer alumina, three primary color fluorescent powder, polyethylene oxide, a surfactant, a dispersing agent, ethanolamine and deionized water. The environment temperature is controlled from 20 DEG C to 30 DEG C, the humidity is 50%-65%, the nanometer alumina, the three primary color fluorescent powder and the deionized water are placed in a stirring barrel to be stirred for 2 hours, the polyethylene oxide is arranged in the stirring barrel to be stirred for 4 hours, finally the surfactant, the dispersing agent and the ethanolamine are placed in the stirring barrel to be stirred for 1 hour, and the high frequency electronic discharge lamp water coating powder can be used for spray coating after standing for 1 hour. The powder is dried by roasting at the temperature of 100 DEG C to 150 DEG C in a machine spray coating process and is roasted at the high temperature of 500 DEG C to 550 DEG C for 15 minutes in a powder roasting furnace. The high frequency electronic discharge lamp water coating powder is simple in preparation, capable of saving cost, suitable for automatic machine spray coating and capable of effectively achieving large batch production of high frequency electronic discharge lamps.

Description

A kind of machine spraying is with the dusting of electrodeless lamp water and preparation and spraying method
Technical field
The invention belongs to electrodeless lamp technical field, relate in particular to and a kind ofly be applicable to that the spraying of multiple machine is with the dusting of electrodeless lamp water and preparation and spraying method.
Background technology
Electrodeless lamp is formed and principle of work: electrodeless lamp is made up of radio-frequency generator, coupling mechanism and bulb three parts.It is that EM field through high frequency generator of electrodeless lamp is coupled in the lamp with the induced mode, makes the gas avalanche ionization in the bulb, forms plasma body.The plasma-excited atom gives off ultraviolet ray when returning ground state.The fluorescent material of bulb inner wall receives ultraviolet ray excited generation visible light.
In the technology of electrodeless lamp, coating process plays a crucial role in whole process procedure, and the control of dusting link puts in place, and the electrodeless lamp of competence exertion hangs down characteristics such as light decay, energy-efficient, high-color rendering.Manual dusting is adopted in traditional electrodeless lamp production, and speed is slow, coat-thickness is inhomogeneous, yield rate is low, can't realize producing in enormous quantities.In the prior art; Chinese patent CN201010216444.0 discloses the prescription and the working method of electrodeless lamp powder batching, it is characterized in that, the weight ratio of said batching combination is: three primary colors fluorescent powder: skimmer: rubber powder: aluminum oxide: dispersion agent: thanomin: plasma water=333:1:4:3:5:10:1000; This invention preparation easily; Can effectively improve the luminosity factor of fluorescent tube, help the work-ing life of prolonging lamp tube, but it is many to invent the fluorescent material consumption of filling a prescription; Cost is higher, and can't be used for the machine spraying.
Summary of the invention
The objective of the invention is to overcome the deficiency of prior art, provide the spraying of a kind of machine with the dusting of electrodeless lamp water and preparation and spraying method, technology is simple, make things convenient for production operation, practice thrift cost, suitable machine sprays automatically, realizes the production in enormous quantities of electrodeless lamp.
Above-mentioned purpose of the present invention is achieved through following technical scheme:
A kind of machine spraying is made up of the component of counting by weight percentage as follows: nano aluminium oxide 0.5%~1%, three primary colors fluorescent powder 3%~4%, polyethylene oxide 1%~2%, tensio-active agent 1%~2%, dispersion agent 1%~2%, thanomin 0.5%~1%, deionized water 88%~92% with the dusting of electrodeless lamp water.
Because nano aluminium oxide and three primary colors fluorescent powder price are higher, the two content is less in the said batching, provides cost savings.Through adding a spot of polyethylene oxide, increase the caking ability of batching, make coat-thickness thinner, be applicable to the machine spraying.
The spraying of described machine is with the preparation method of electrodeless lamp water dusting: envrionment temperature is controlled to be 20 ℃-30 ℃, and humidity 50%-65% was put in the agitation vat nano aluminium oxide, three primary colors fluorescent powder and deionized water into stirring 2 hours; Add polyethylene oxide again, restir 4 hours; Adding tensio-active agent, dispersion agent, thanomin at last stirred 1 hour; Leave standstill after 1 hour and can be used for dusting.
Above-mentioned machine spraying is with the preparation method of electrodeless lamp water dusting, and the optimum environment temperature is controlled to be 24 ℃-28 ℃, and humidity is 52 ℅-62 ℅.
The spraying of described machine is with the spraying method of electrodeless lamp water dusting, and the machine spraying process is starched above-mentioned powder with 100 ℃~150 ℃ temperature and dried, and passes through the baking powder stove again with 500 ℃~550 ℃ high bakes 15 minutes.
Compared with prior art, the present invention has following beneficial effect:
1. preparation is simple, and used nano aluminium oxide and three primary colors fluorescent powder content are few, can effectively practice thrift cost;
2. powder slurry degree of adhesion is high, and coating is thin, is applicable to that machine sprays automatically;
3. production technique is simple, and is easy to operate, can effectively realize the production in enormous quantities of electrodeless lamp.
Embodiment
Below in conjunction with specific embodiment the present invention is done further explanation, but embodiment does not do any qualification to the present invention.
Embodiment 1:
In temperature is 20 ℃-30 ℃, and humidity is that the optimum environment temperature is controlled to be 24 ℃-28 ℃ in 50%-65% the environment, and humidity is 52 ℅-62 ℅.Get nano aluminium oxide 100g, three primary colors fluorescent powder 400g, polyethylene oxide 200g, tensio-active agent 200g, dispersion agent 200g, thanomin 100g, deionized water 9200g.At first nano aluminium oxide and deionized water are put into and at the uniform velocity stirred in the agitation vat 1 hour, leave standstill after 1 hour and in this solution, add three primary colors fluorescent powder, stirred fast again 2 hours; Add polyethylene oxide then, stirred fast again 4 hours, fully fused; Adding tensio-active agent, dispersion agent, thanomin at last successively stirred 1 hour; Leaving standstill 1 hour rear can be used for dusting.The machine spraying process is dried it with 100 ℃~150 ℃ temperature, again through the baking powder stove with 500 ℃~550 ℃ high bakes 15 minutes, process lamp after light efficiency can reach 75Lm/w, colour rendering index >=80.
Embodiment 2:
In temperature is 20 ℃-30 ℃, and humidity is that the optimum environment temperature is controlled to be 24 ℃-28 ℃ in 50%-65% the environment, and humidity is 52 ℅-62 ℅.Get nano aluminium oxide 50g, three primary colors fluorescent powder 300g, polyethylene oxide 100g, tensio-active agent 100g, dispersion agent 100g, thanomin 50g, deionized water 9000g.At first nano aluminium oxide and deionized water are put into and at the uniform velocity stirred in the agitation vat 1 hour, leave standstill after 1 hour and in this solution, add three primary colors fluorescent powder, stirred fast again 2 hours; Add polyethylene oxide then, stirred fast again 4 hours, fully fused; Adding tensio-active agent, dispersion agent, thanomin at last successively stirred 1 hour; Leaving standstill 1 hour rear can be used for dusting.The machine spraying process is dried it with 100 ℃~150 ℃ temperature, again through the baking powder stove with 500 ℃~550 ℃ high bakes 17 minutes, process lamp after light efficiency can reach 74Lm/w, colour rendering index >=78.
Embodiment 3:
In temperature is 20 ℃-30 ℃, and humidity is that the optimum environment temperature is controlled to be 24 ℃-28 ℃ in 50%-65% the environment, and humidity is 52 ℅-62 ℅.Get nano aluminium oxide 75g, three primary colors fluorescent powder 350g, polyethylene oxide 150g, tensio-active agent 150g, dispersion agent 150g, thanomin 75g, deionized water 9100g.At first nano aluminium oxide and deionized water are put into and at the uniform velocity stirred in the agitation vat 1 hour, leave standstill after 1 hour and in this solution, add three primary colors fluorescent powder, stirred fast again 2 hours; Add polyethylene oxide then, stirred fast again 4 hours, fully fused; Adding tensio-active agent, dispersion agent, thanomin at last successively stirred 1 hour; Leaving standstill 1 hour rear can be used for dusting.The machine spraying process is dried it with 100 ℃~150 ℃ temperature, again through the baking powder stove with 500 ℃~550 ℃ high bakes 15 minutes, process lamp after light efficiency can reach 74Lm/w, colour rendering index >=80.

Claims (4)

1. a machine spraying is with the dusting of electrodeless lamp water; It is characterized in that, form: nano aluminium oxide 0.5%~1%, three primary colors fluorescent powder 3%~4%, polyethylene oxide 1%~2%, tensio-active agent 1%~2%, dispersion agent 1%~2%, thanomin 0.5%~1%, deionized water 88%~92% by the component of counting by weight percentage as follows.
2. method for preparing the spraying of the described machine of claim 1 with the dusting of electrodeless lamp water; It is characterized in that; Envrionment temperature is controlled to be 20 ℃-30 ℃, and humidity 50%-65% is put nano aluminium oxide, three primary colors fluorescent powder and deionized water in the agitation vat into and to be stirred 2 hours; Add polyethylene oxide again, restir 4 hours; Adding tensio-active agent, dispersion agent, thanomin at last stirred 1 hour; Leave standstill after 1 hour and can be used for dusting.
3. machine spraying according to claim 2 is characterized in that with the preparation method of electrodeless lamp water dusting the optimum environment temperature is controlled to be 24 ℃-28 ℃, and humidity is 52 ℅-62 ℅.
4. method that sprays the spraying of the described machine of claim 1 with the dusting of electrodeless lamp water; It is characterized in that; The machine spraying process is dried above-mentioned powder slurry with 100 ℃~150 ℃ temperature earlier, passes through the baking powder stove again with 500 ℃~550 ℃ high bakes 15 minutes.
CN2012100513215A 2012-03-01 2012-03-01 High frequency electronic discharge lamp water coating powder for machine spray coating and preparation and spray coating method thereof Pending CN102618256A (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
CN2012100513215A CN102618256A (en) 2012-03-01 2012-03-01 High frequency electronic discharge lamp water coating powder for machine spray coating and preparation and spray coating method thereof
PCT/CN2012/086409 WO2013127226A1 (en) 2012-03-01 2012-12-12 Machine-sprayed electrodeless-lamp water powder and preparation and spraying methods thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2012100513215A CN102618256A (en) 2012-03-01 2012-03-01 High frequency electronic discharge lamp water coating powder for machine spray coating and preparation and spray coating method thereof

Publications (1)

Publication Number Publication Date
CN102618256A true CN102618256A (en) 2012-08-01

Family

ID=46558473

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2012100513215A Pending CN102618256A (en) 2012-03-01 2012-03-01 High frequency electronic discharge lamp water coating powder for machine spray coating and preparation and spray coating method thereof

Country Status (2)

Country Link
CN (1) CN102618256A (en)
WO (1) WO2013127226A1 (en)

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102965097A (en) * 2012-11-22 2013-03-13 安徽世林电光源设备有限公司 Preparation method of fluorescent powder suspension solution for straight tube fluorescent lamp
WO2013127226A1 (en) * 2012-03-01 2013-09-06 广东顺祥节能照明科技有限公司 Machine-sprayed electrodeless-lamp water powder and preparation and spraying methods thereof
CN103775873A (en) * 2014-01-08 2014-05-07 南京琦光光电科技有限公司 LED lamp with purple light transformed into white light and manufacturing method thereof
CN104073135A (en) * 2014-07-14 2014-10-01 邓勇 Water-based coating material for glass pipe fluorescent lamp, as well as preparation method and coating method of water-based coating material
CN104629715A (en) * 2015-03-05 2015-05-20 广东顺祥节能照明科技有限公司 High-luminous-efficiency electrodeless lamp blending powder as well as preparation method and application thereof
CN105315862A (en) * 2014-07-18 2016-02-10 深圳市乔麟光电有限公司 Preparation method of cold cathode ultraviolet lamp coating liquid
CN105349010A (en) * 2015-12-11 2016-02-24 周妙思 Electrodeless lamp water coating powder and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04110389A (en) * 1990-08-31 1992-04-10 Nec Home Electron Ltd Fluorescent lamp
CN1525516A (en) * 1998-07-08 2004-09-01 ���µ�����ҵ��ʽ���� Plasma display panel manufacturing method for manufacturing a plasma display panel with superior picture quality, a manufacturing apparatus, and a phosphor ink
CA2550481A1 (en) * 2005-09-29 2007-03-29 Osram Sylvania Inc. Method of making ceramic discharge vessels using stereolithography
CN101892044A (en) * 2010-07-02 2010-11-24 冯福坤 Formula and production method of electrodeless lamp powder batching

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4340512A (en) * 1979-10-01 1982-07-20 North American Philips Corporation Method of providing a universal coating for fluorescent lamps
CN100372050C (en) * 2004-10-28 2008-02-27 谢寅 Cold cathode decorative lamp and cold cathode fluorescent lamp tube
CN100558846C (en) * 2005-04-01 2009-11-11 松下电器产业株式会社 The renovation process of fluor and luminescent lamp
CN101867007A (en) * 2010-05-11 2010-10-20 电子科技大学 Preparation method of LED lamp fluorescent powder layer
CN102618256A (en) * 2012-03-01 2012-08-01 广东顺祥节能照明科技有限公司 High frequency electronic discharge lamp water coating powder for machine spray coating and preparation and spray coating method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04110389A (en) * 1990-08-31 1992-04-10 Nec Home Electron Ltd Fluorescent lamp
CN1525516A (en) * 1998-07-08 2004-09-01 ���µ�����ҵ��ʽ���� Plasma display panel manufacturing method for manufacturing a plasma display panel with superior picture quality, a manufacturing apparatus, and a phosphor ink
CA2550481A1 (en) * 2005-09-29 2007-03-29 Osram Sylvania Inc. Method of making ceramic discharge vessels using stereolithography
CN101892044A (en) * 2010-07-02 2010-11-24 冯福坤 Formula and production method of electrodeless lamp powder batching

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
何志明: "Al2O3-Polyox 水涂法", 《中国照明电器》, no. 9, 31 December 2002 (2002-12-31), pages 14 - 16 *
艾海等: "水涂粉材料及工艺", 《中国照明电器》, no. 5, 31 December 1998 (1998-12-31) *

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2013127226A1 (en) * 2012-03-01 2013-09-06 广东顺祥节能照明科技有限公司 Machine-sprayed electrodeless-lamp water powder and preparation and spraying methods thereof
CN102965097A (en) * 2012-11-22 2013-03-13 安徽世林电光源设备有限公司 Preparation method of fluorescent powder suspension solution for straight tube fluorescent lamp
CN103775873A (en) * 2014-01-08 2014-05-07 南京琦光光电科技有限公司 LED lamp with purple light transformed into white light and manufacturing method thereof
CN103775873B (en) * 2014-01-08 2017-01-11 南京琦光光电科技有限公司 LED lamp with purple light transformed into white light and manufacturing method thereof
CN104073135A (en) * 2014-07-14 2014-10-01 邓勇 Water-based coating material for glass pipe fluorescent lamp, as well as preparation method and coating method of water-based coating material
CN104073135B (en) * 2014-07-14 2016-06-01 邓勇 Glass tubing fluorescent lamp water-based coating material and its preparation method and coating method
CN105315862A (en) * 2014-07-18 2016-02-10 深圳市乔麟光电有限公司 Preparation method of cold cathode ultraviolet lamp coating liquid
CN104629715A (en) * 2015-03-05 2015-05-20 广东顺祥节能照明科技有限公司 High-luminous-efficiency electrodeless lamp blending powder as well as preparation method and application thereof
CN104629715B (en) * 2015-03-05 2017-01-11 广东顺祥节能照明科技有限公司 High-luminous-efficiency electrodeless lamp blending powder as well as preparation method and application thereof
CN105349010A (en) * 2015-12-11 2016-02-24 周妙思 Electrodeless lamp water coating powder and preparation method thereof

Also Published As

Publication number Publication date
WO2013127226A1 (en) 2013-09-06

Similar Documents

Publication Publication Date Title
CN102618256A (en) High frequency electronic discharge lamp water coating powder for machine spray coating and preparation and spray coating method thereof
CN102212360B (en) Field emission fluorescent material and preparation method thereof
CN104087284B (en) A kind of preparation method of electrostatic fluorescent material
CN102703066A (en) Fluorosilicate fluorescent powder and preparation method thereof
CN104449355A (en) Method for preparing high temperature resistant diffuse reflection coating
CN1664052A (en) Silicon oxide coated fluorescent powder and its coating method
CN104560043A (en) Energy-saving lamp fluorescent powder
CN105199729A (en) NaSrPO4:xEu<3+> red phosphor powder for LED (Light Emitting Diode) and preparation method thereof
CN104212443B (en) The preparation method of short persistence zinc manganese silicate fluorescent material
CN101892044B (en) Formula and production method of electrodeless lamp powder batching
CN102942925A (en) NaEu(MoO4)2-x(WO4)x-type fluorescent microcrystals and chemical solution preparation method thereof
CN102516982B (en) Illuminating lamp, blended powder for illuminating lamp thereof and its production method
CN105295916B (en) A kind of silicate green fluorescent powder and its preparation method and application
CN104629715B (en) High-luminous-efficiency electrodeless lamp blending powder as well as preparation method and application thereof
CN102176405A (en) High-brightness high-frequency electrodeless lamp
CN110172345B (en) Rare earth fluorescent powder prepared by doping graphene nano composite material and preparation method thereof
CN101404235B (en) Fluorescent powder coating technique for high-frequency electrodeless lamp
CN105199731B (en) A kind of LED NaLaMgWO6:xSm3+Red fluorescence powder and preparation method thereof
CN102888219A (en) Method for preparing rare-earth aluminate blue-green fluorescent powder for energy-saving lamp
CN112094643B (en) Mn (manganese)4+Fluoride-doped narrow-band red fluorescent powder and preparation method and application thereof
CN102061168A (en) Method for improving luminosity of europium-doped yttrium oxide red fluorescent powder
CN101818066B (en) Method for preparing fluorescent powder
CN105349010A (en) Electrodeless lamp water coating powder and preparation method thereof
CN105176526A (en) Preparation method of low-voltage and high-brightness orange red zinc-sulfate-based fluorescent material
CN105038793A (en) Y2O3:Eu<3+> red powder having high specific surface area and preparation method thereof

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C12 Rejection of a patent application after its publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20120801