CN102605438B - Manufacture method of washable mulberry silkworm long silk floss with high sericin content - Google Patents
Manufacture method of washable mulberry silkworm long silk floss with high sericin content Download PDFInfo
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Abstract
The invention provides a manufacture method of washable mulberry silkworm long silk floss with high sericin content. The method is characterized in that in a mulberry silkworm silk refining process, firstly, mulberry silkworm blank botton is fast prepared in alkaline environment, then, the degumming and the partial sericin temporary curing are realized in acid environment, next, grease is removed in neutral environment, and then, the reset sericin is completely cured in acid environment. The method has the following concrete steps of: 1, blank floss preparation; 2, sericin maintaining primary melting; 3, foaming degreasing; 4, sericin curing re-melting; 5, softening treatment; and 6, impurity removal and floss baking. The method provided by the invention has the advantages that the mass loss of sericin and the hardening of the mulberry silkworm silk floss cannot occur in the subsequent treatment and subsequent water washing process, the sericin content is high, the silk fiber intensity is high, the compression rebonding rate is high, the antibacterium, mould-proof and worm-eaten prevention effects are realized, the service life is long, and all characteristics of pure natural mulberry silkworm silk are realized.
Description
Technical field
The present invention relates to a kind of preparation method of silkworm long filament silk floss, is that a kind of content of silk gum is high specifically, can wash again the preparation method of silkworm long filament silk floss.
Background technology
Silk circle insider all know: the natural antibacterial of silk, mildew-resistant, Anti-moth-eating function are mainly to be brought into play by the silk gum self character of silk, as the T-shirt that summer, dress contained silk, its collar can be not smelly in the situation that making soaked with sweat, and main cause is exactly that silkworm silk gum has played antibacterial, antibacterial action.If the silk gum of silk product entirely comes out or is destroyed, just lost this function, also just no longer antibacterial, mildew-resistant, Anti-moth-eating.Also there is on the market at present different types of cocoon silk quilt of washing, but all more or less have some defects, affected the promotion and application that can wash cocoon silk quilt.At present, in the refining process that goes silk gum and degrease technique of silkworm long filament silk floss, mostly adopt alkaline medium and high temperature to realize the concise of silk silk floss and come unstuck and degrease both at home and abroad, gained silkworm long filament silk floss has following three kinds of results:
The first is not too white at silk cocoon intrinsic colour, utilizes special purpose machinery to select the yellow spotted cocoon or the dupion quick filature slabbing under 65 ℃ of left and right, caustic soda water infiltration condition that get off to make embryo silk floss reeling mill, because base silk floss is more black, need to use hydrogen peroxide bleaching.And bleaching must will utilize high temperature, high base number first the silk gum on silk to be removed to below 3%, then carry out high-load hydrogen peroxide bleaching, make like this silk silk floss very white, departed from the natural color of silk, very popular on the market.The silk floss just making has like this greatly reduced the utilization rate of silk cocoon not to be said, also in follow-up cocoon silk quilt is used, easily produces static and is easily stained with dirt, thereby lose the due antistatic feature of mulberry silk.Also because of silk gum recoverable amount very little, the continuous moisture retention variation of silk, for skin care, repairs the function of keratoderma and has a greatly reduced quality, and has lost the health cares such as the due natural skin care of mulberry silk.The functions such as this silk silk floss can be washed after processing by softener, but after washing several times, content of silk gum can be still less more, antibacterial, the mildew-resistant that silk is natural will exhaust, the compression resilience variation that silk itself is excellent, and warmth retention property declines;
The second is namely pure dupion or the bonscocoons of use in the situation that silk cocoon intrinsic colour is whiter, become the continuous stage of base with the quick filature of special purpose machinery, with the first, be the same, just in practicing process processed, reduced the consumption of hydrogen peroxide, reduced the experienced time processed, the continuous content of silk gum of silk making is higher, general content of silk gum can remain on 5% left and right, this silk is continuous continuous with the softener with hydrophobic grouping (for example with there being agent silicon class emulsion) processing silk, allow the appearance of silk fiber be coated one deck oil film shape material, such silk is continuous soft, touch up comfortable, silk floss is difficult for getting wet, so just can wash.Shortcoming is: because the reason of oil film, silk hygroscopicity is poor, and moisture retention is bad, and maintaining skin is had a greatly reduced quality.Also, because of too soft, compression resilience is poor, is exactly that warmth retention property is bad, can only make thin quilt;
The third is also in the situation that silk cocoon intrinsic colour is whiter, and institute base is continuous or cry the continuous string bag of craft without hydrogen peroxide bleaching, the preparation method of Here it is existing manual silk silk floss.This silk floss has retained the most natural characteristic of silk, and as careful use, level of comfort can be fine.Yet manual silk silk floss also has a fatal shortcoming, do not allow when drawing cocoon silk quilt silk tire exactly silk fiber disconnect as far as possible, in silk floss processed, retained silk silk gum (yes tries out for generations as far as possible, can not be unable to say for certain), content of silk gum is in 10% left and right, such high-load silk gum, again not through any other PROCESS FOR TREATMENT, silk gum is very easily soluble in water, once silk gum contacts with sweat and do not dry in time or the reason such as make moist, will make that silk gum is water-soluble to be become sticky colloid substance and cause and harden or local caking;
In above three kinds of results, first two can make can wash silk silk floss, by existing standard, can incorporate Grade A into, is mainly that softener has been added, and compression rebound rate is difficult to reach excellent grading index; But shortcoming is that contained silk gum amount is low, only has 3-5%, has affected quality and the service life of product.The third is to belong to the silk silk floss that can not wash, by present cocoon silk quilt standard, but can be classified as high-class product, and compression resilience is best, and maximum shortcoming is to wash.But in reality, with the higher cocoon silk quilt of this content of silk gum, grown having a good chance of hardening service time, because be in use difficult to avoid quilt not make moist or part is not soaked by sweat, also can run into picture child wets the bed, large ill or the special circumstances such as vomiting, the elderly's gatism of being drunk.If it is pretty troublesome that silkworm long filament is renovated, turned over and also become staple fibre, uncertainly can find producer to renovate to you, thereby affect the extensive use of cocoon silk quilt purposes.Silk industry is thought: the best silkworm long filament silk floss of washing must reach this standard: content of silk gum, between 5-15%, evenly and is stably solidificated on mulberry silk fiber; Under 30 ℃ of water temperatures, neutral detergent condition, with after cylinder class washing of drum type washing machine 20 times, content of silk gum will retain more than 60% on former basis, the compression rebound rate of silk seldom or constant, it is little that hygroscopicity hydrofuge follows the indexs such as pure natural mulberry silk is approaching, antibacterial, mildew-resistant and outward appearance etc. to change.
Summary of the invention
For overcoming the above-mentioned defect of going silk gum and degrease technique of existing silkworm long filament silk floss, the invention provides a kind of content of silk gum high, the continuous preparation method of silkworm long filament that can wash again, gained silkworm long filament silk floss is unlikely to silk gum and runs off in a large number and harden in follow-up processing and later water-washing process, and content of silk gum is high, and silk fiber intensity is high, compression rebound rate is high, antibacterial, mildew-resistant, Anti-moth-eating, long service life, has advantages of that pure natural mulberry silk is all.
For solving its technical problem, the technical solution used in the present invention is: first under 100 ℃ of high temperature, sour environment, in the softening mulberry silk base silk floss that comes unstuck, with the little molecule of acidity, protect glue and just practice the free group of the temporary transient grafting part of agent silk gum, allow the decreased solubility of silk gum, when content of silk gum reaches 15%, silk gum viscosity between silk fiber declines, coherent silk fiber is dissociated smoothly, so just on silk, retain in the silk gum of high-load and the flexibility of maintenance mulberry silk simultaneously and average out; Again with the sodium carbonate liquor that dilute by the experienced liquid in experienced barrel
ph value is adjusted to neutrality, do not stop therebetween to stir, the acid solution that makes to practice in liquid and continuous sheet fully reacts with sodium carbonate, utilizes the expansive force of Bubble formation that grease unnecessary in continuous sheet is entered to experienced liquid from extruding the while between silk fiber by surfactant A ES emulsification, is removed subsequently in cleaning; Then will contain 15% silk gum, carry out concise except the solid glue scouring agent of silk floss utilization of degrease, after a large amount of silk gum is solidificated on mulberry silk fiber by graft reaction, then it is continuous through soft treatment, oven dry, to make a kind of content of silk gum silkworm long filament high, that can wash again; Concrete production method comprises the steps: the continuous preparation of 1. bases; 2. protecting glue just practices; 3. foaming oil removing; 4. solid glue is practiced again; 5. soft treatment; 6. removal of impurities is dried continuous.
Compared with prior art, because the present invention first makes fast mulberry silk base silk floss under alkaline environment, under sour environment, realize again and coming unstuck and part silk gum temporarily solidifies, then under neutral environment, remove grease, then under sour environment, remaining silk gum is completely curing; Therefore advantage of the present invention is: mulberry silk is unlikely to silk gum and runs off in a large number and harden in follow-up processing and later water-washing process, and content of silk gum is high, and silk fiber intensity is high, compression rebound rate is high, antibacterial, mildew-resistant, Anti-moth-eating, long service life, has all features of pure natural mulberry silk.
The specific embodiment
Below in conjunction with embodiment, the present invention is further described:
Embodiment: a kind of content of silk gum is high, the continuous preparation method of silkworm long filament that can wash again, in mulberry silk refining process, first under alkaline environment, make fast mulberry silk base continuous, under sour environment, realize again and coming unstuck and part silk gum temporarily solidifies, then under neutral environment, remove grease, then under sour environment, remaining silk gum is completely curing; It comprises the steps:
1, base is continuous prepares: by the silk cocoon of purchase, by manual grading skill, be dupion, bonscocoons, yellow spotted cocoon; The upper strata husks that dupion or bonscocoons adopt cocoon-peeling machine to peel silk cocoon off in batches make light dupion or bonscocoons standby, yellow spotted cocoon is separately used as him; Light dupion or bonscocoons are put into the silk floss machine hopper with cylinder, adopt 65 ℃,
pthe caustic soda water spray of H value 10.5, the cylinder of rotation drives silk cocoon to spin upside down or do circumference and rolls, silk cocoon outer surface is subject to after caustic soda water spray, the rapid partial solution of silk gum from, because the shearing force that rotation produces pulls out the thread head on silk cocoon be bonded on the wall of cylinder outer or on a layer at once, silk on each silk cocoon all can be along with drum rotating is pulled out fast, and be evenly distributed in cylinder periphery; When silk cocoon rolling is reeled off raw silk from cocoons, also because of manually by silk cocoon with axial stirring, the silk layer producing also can keep a kind of crisscross structure, continue after 5-8 minute like this, on cylinder, just make the thin tubular base silk floss that one deck silk is evenly arranged, shut down, close spray liquid, along drum shaft to cutting off continuous sheet, lift cutting section, along cylinder periphery, pull out, just make the rectangle embryo of feel as sheep tripe continuous, base silk floss is soaked and within 12 hours, removes unnecessary caustic soda and dirt with clear water, and pending use is cleaned, is dried in pack, now the continuous content of silk gum of base 20% left and right;
2, protecting glue just practices: in practicing bucket, add the running water of practicing bucket volume 2/3rds, with acid guarantor's glue just experienced agent JL002 by running water
ph value is adjusted to 3.4-3.5, add the pending base of running water weight 10% continuous, add the continuous weight in wet base 1-2% of base surfactant A ES(need first adjust rare, then add in proportion), pass into steam, be heated to boiling, be incubated 25 minutes and can pull open into smoothly even silk floss shape to the continuous softness of base, stop heating;
3, foaming oil removing: continue to maintain experienced liquid temp constant, with the sodium carbonate liquor that dilute by the experienced liquid in experienced bucket
ph value is adjusted to neutrality, do not stop therebetween to stir, make to practice acid solution in liquid and continuous sheet fully and sodium carbonate react, utilize the expansive force of Bubble formation that grease unnecessary in continuous sheet is entered to experienced liquid by AES emulsification from extruding between silk fiber simultaneously, this process maintains 2.5-3.5 minute, then continuous sheet is pulled out from practice bucket and put into cleaning machine and clean to water clearly, after drying, just can consolidate glue, now content of silk gum is 15% left and right;
4, solid glue is practiced again: first add the running water of practicing bucket 2/3rds, add solid glue scouring agent JL008 extremely
ph value reaches 4.0, joins for practicing liquid, passes into steam heated to boiling, the packed continuous sheet of just practicing after oil removing dries is put in white silk bucket to practice the ratio of liquid weight 10%, 100 ℃ of insulations, stirred once every 5 minutes therebetween, after 30 minutes, continuous sheet were pulled out and were put into cleaning machine cleaning extremely
pit is neutral that H value is, and dries and treat follow-up soft treatment use, now content of silk gum 15% left and right;
5, soft treatment: add 2/3rds running water in soft treatment pond, by steam heated to 35 ℃, adjust with glacial acetic acid
ph value to 4.0, adds wet silk floss to weigh the spun silk softener TH404A of 1-2%, and the mulberry silk that last process is processed is put in soft pond and kept 1 hour, pulls drying out, now content of silk gum 15% left and right;
6, removal of impurities is dried continuous: the mulberry silk of drying is taken out from bag, wash, remove a little pupa bits and impurity in silk floss, then put into 50 ℃ of continuous rooms of above baking and dry, just become a kind of content of silk gum high, the continuous finished product of silkworm long filament that can wash again.
Claims (2)
1. a content of silk gum is high, the continuous preparation method of silkworm long filament that can wash again, it is characterized in that: first under 100 ℃ of high temperature, sour environment, in the softening mulberry silk base silk floss that comes unstuck, with the little molecule of acidity, protect glue and just practice the free group of the temporary transient grafting part of agent silk gum, allow the decreased solubility of silk gum, when content of silk gum reaches 15%, silk gum viscosity between silk fiber declines, coherent silk fiber is dissociated smoothly, so just on silk, retain in the silk gum of high-load and the flexibility of maintenance mulberry silk simultaneously and average out; With the sodium carbonate liquor diluting, the pH value of practicing the experienced liquid in bucket is adjusted to neutrality again, do not stop therebetween to stir, make to practice acid solution in liquid and continuous sheet fully and sodium carbonate react, utilize the expansive force of Bubble formation that grease unnecessary in continuous sheet is entered to experienced liquid by surfactant A ES emulsification from extruding between silk fiber simultaneously, in cleaning, be removed subsequently; Then will contain 15% silk gum, carry out concise except the solid glue scouring agent of silk floss utilization of degrease, after a large amount of silk gum is solidificated on mulberry silk fiber by graft reaction, then it is continuous through soft treatment, oven dry, to make a kind of content of silk gum silkworm long filament high, that can wash; Concrete production method comprises the steps: the continuous preparation of 1. bases; 2. protecting glue just practices; 3. foaming oil removing; 4. solid glue is practiced again; 5. soft treatment; 6. removal of impurities is dried continuous.
2. a kind of content of silk gum according to claim 1 is high, the continuous preparation method of silkworm long filament that can wash again, it is characterized in that: production stage 3 foaming oil removings are: continue to maintain experienced liquid temp constant, with the sodium carbonate liquor diluting, the pH value of practicing the experienced liquid in bucket is adjusted to neutrality, do not stop therebetween to stir, make to practice acid solution in liquid and continuous sheet fully and sodium carbonate react, this process maintains 2.5-3.5 minute, then continuous sheet is pulled out from practice bucket and put into cleaning machine and clean to water clear, after drying, just can consolidate glue, now content of silk gum is 15% left and right.
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Families Citing this family (8)
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| CN103628145A (en) * | 2012-08-27 | 2014-03-12 | 南充银海丝绸有限公司 | Frison fixation bleaching refining process |
| CN103225171B (en) * | 2013-01-28 | 2015-03-04 | 横县桂华茧丝绸有限责任公司 | Manufacturing method of tailorable silk floss |
| CN103349460B (en) * | 2013-06-14 | 2015-05-06 | 屠晓明 | Manufacture method of machine washable silk quilt |
| CN104762756B (en) * | 2015-04-24 | 2017-01-11 | 嘉兴学院 | Natural silk facial mask base cloth and preparation method thereof |
| CN106758191A (en) * | 2016-12-12 | 2017-05-31 | 广西江缘茧丝绸有限公司 | Mulberry silk fiber deoils and protects the process of glue |
| CN110387586A (en) * | 2019-06-17 | 2019-10-29 | 浙江蚕缘家纺有限公司 | A kind of solidifying degumming of silk technique of silk |
| CN110720800A (en) * | 2019-10-15 | 2020-01-24 | 安徽珂欣茧业有限公司 | Silk and down composite quilt and processing technology thereof |
| CN112826286B (en) * | 2021-01-07 | 2023-12-05 | 浙江蚕缘家纺股份有限公司 | Silk quilt capable of being washed |
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Denomination of invention: Manufacture method of washable mulberry silkworm long silk floss with high sericin content Effective date of registration: 20170719 Granted publication date: 20140319 Pledgee: Changde Caixin technology Company limited by guarantee Pledgor: Changde Royalsilk Products Co., Ltd. Registration number: 2017430000046 |
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