CN102584183B - Two-piece ceramic bulb shell and manufacturing method thereof - Google Patents
Two-piece ceramic bulb shell and manufacturing method thereof Download PDFInfo
- Publication number
- CN102584183B CN102584183B CN201210021529.2A CN201210021529A CN102584183B CN 102584183 B CN102584183 B CN 102584183B CN 201210021529 A CN201210021529 A CN 201210021529A CN 102584183 B CN102584183 B CN 102584183B
- Authority
- CN
- China
- Prior art keywords
- bulb shell
- base substrate
- piece
- thin
- slurry
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Images
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J9/00—Apparatus or processes specially adapted for the manufacture, installation, removal, maintenance of electric discharge tubes, discharge lamps, or parts thereof; Recovery of material from discharge tubes or lamps
- H01J9/24—Manufacture or joining of vessels, leading-in conductors or bases
- H01J9/26—Sealing together parts of vessels
- H01J9/265—Sealing together parts of vessels specially adapted for gas-discharge tubes or lamps
- H01J9/266—Sealing together parts of vessels specially adapted for gas-discharge tubes or lamps specially adapted for gas-discharge lamps
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J61/00—Gas-discharge or vapour-discharge lamps
- H01J61/02—Details
- H01J61/30—Vessels; Containers
- H01J61/302—Vessels; Containers characterised by the material of the vessel
Landscapes
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Ceramic Products (AREA)
Abstract
The invention belongs to the technical field of the preparation of electric light source materials, and particularly relates to a two-piece ceramic bulb shell and a manufacturing method thereof. The method comprises the steps as follows: a, a pair of green bodies of the ceramic bulb shell, which is in the same shape, is formed, wherein each green body comprises a capillary tube (1) and a cavity body (2); b, combining rings (3) are formed on combining surfaces of the cavity bodies; c, thin layers of slurry used for bonding are printed on the surfaces of the combining rings of the green bodies to be butted of the bulb shell; d, the two green bodies of the bulb shell are positioned through a fixture, so as to bond the slurry on the surfaces of the combining rings together; e, the connected bulb shell is dried, the green bodies bonded together are taken out after the slurry is dried, and after the connected bulb shell is roasted at a high temperature, the ceramic bulb shell with a two-piece structure is finally formed. The manufacturing method has the advantages of simple process, reliable butt joint manner, and no deformation and no dislocation of an appearance formed by butting the green bodies, and the like, and the integral transparent rate cannot be influenced after the bulb shell is roasted at a high temperature.
Description
Technical field
The invention belongs to electric source material preparing technical field, relate in particular to a kind of two-piece-dress ceramic bulb shell and preparation method thereof.
Background technology
Two-piece-dress cell-shell generally adopts the mode of interference fit to achieve a butt joint at present, as shown in Figure 1, first distinguish two base substrates of moulding, the concaveconvex structure that has coupling at the butted part of two base substrates, the base substrate of two kinds of different structures is burned in advance under different temperatures according to shrinkage, more pre-two burned biscuits are docked, then carries out high temperature sintering, butted part combines by the mode of interference fit, realizes air-tightness docking.
There is in the last few years the method that another two-piece-dress cell-shell realization connects, it is exactly a kind of ceramic body that contains more jointing material of moulding, the shape of two base substrates is identical, under green state to two ceramic bodies being combined in fixture after the faying face thermoplastic of ceramic body, carry out again binder removal, sintering, realize the air-tightness docking of ceramic bulb shell.
Two-piece-dress cell-shell adopts the mode of interference fit to dock by shrinkage difference in sintering process and realizes, therefore need two kinds of shrinkage differences of moulding and the different base substrate of interface structure, then also to select different calcined temperatures to carry out pre-burning, process more complicated, control difficulty larger, the cell-shell that interference fit connects in addition need increase wall thickness, so also can affect cell-shell light transmittance, and in each assembling and sintering step, the defects such as the dislocation of ceramic bulb shell assembly or adhesion and air-tightness may occur.
The method that adopts the mode heating to dock two-piece-dress cell-shell is by a pair of base substrate that contains a large amount of jointing materials of moulding, by heating binding site, make base substrate fusing, two assemblies are combined and realized under external force, therefore in follow-up technique, be difficult to drain a large amount of bond materials in base substrate, it is the fatal problem that affects performance that impurity is contained in transparent alumina ceramics cell-shell inside, base substrate is heated and conducts whole deliquescing in addition, also add and will apply External Force Acting, in docking operation, be easy to occur the situation of blank deformation.
Summary of the invention
For the shortcoming of prior art, the object of this invention is to provide a kind of technique simple, docking mode is reliable, and base substrate docking outward appearance is without the manufacture method of the two-piece-dress ceramic bulb shell of distortion, dislocation;
In addition, the present invention also provides the ceramic bulb shell that above-mentioned manufacture method obtains.
For achieving the above object, technical scheme of the present invention is: a kind of manufacture method of two-piece-dress ceramic bulb shell, and it comprises the following steps:
A, the ceramic bulb shell base substrate that a pair of shape of moulding is identical, base substrate is comprised of capillary and cavity;
B, at faying face moulding one circle of cavity in conjunction with circle;
C, the thin-layer sizing agent at combination circle surface printing one deck of cell-shell base substrate to be docked for boning;
D, by Special tooling clamp, two cell-shell base substrates are positioned, make to be bonded together in conjunction with the surperficial slurry of circle;
E, the cell-shell of connection is dried, after slurry drying, takes out the base substrate being bonded together; Through high temperature sintering, be finally shaped to two-piece-dress ceramic bulb shell.
In steps d, described fixture comprise diameter than the thin draw point of capillary inner diameter and with the base of ceramic body cambered surface coupling; By print slurry a base substrate capillary down, be fixed in the fixture designing, the cavity of getting again the base substrate that another one is printed on slurry inserts in draw point down, by two base substrates accurately being located through the draw point of capillary endoporus, and under cell-shell base substrate self gravitation or external force, depress and make to be bonded together in conjunction with the surperficial slurry of circle.
In step b, the height of described combination circle evagination part is 0.5～1.0mm.In step c, adopt film printing or transfer-print technology at combination circle surface printing one deck of cell-shell base substrate to be docked the thin-layer sizing agent for boning, slurry thickness is 0.03～0.05mm.
In step c, the main component of thin-layer sizing agent is the alumina powder identical with cell-shell base substrate composition, also add 2 ~ 5% glycerine, 3 ~ 6% terpinols, 1 ~ 4% dioctyl phthalate, 0.5 ~ 2% phthalic acid didecyl ester, 1 ~ 3% epoxy resin, 0.1 ~ 0.5% polyamide wax and 0.1 ~ 0.5% rilanit special, and adopt slurry technology of preparing to be prepared into meet the slurry of the viscosity 30000 ~ 40000mPa * S of film printing needs.
In step e, 50～80 ℃ of heat drying temperature, the time is 10～30min; Or be placed in air and be dried, the time is 100～150min.
In step a, cavity is semielliptical type, dome-type or half cast; Cell-shell base substrate is by dry-pressing or isostatic compaction.
Meanwhile, the present invention also provides a kind of two-piece-dress ceramic bulb shell, comprises two cavitys and is located at respectively the capillary on cavity end, wherein, on the faying face of two cavitys, be equipped with in conjunction with circle, and be provided with thin-layer sizing agent in conjunction with circle, two cavitys are bonded together by thin-layer sizing agent.
The height of described combination circle evagination part is 0.5～1.0mm; Described thin-layer sizing agent thickness is 0.03～0.05mm; Described cavity is semielliptical type, dome-type or half cast.
Compared with prior art, beneficial effect of the present invention is,
1. cell-shell base substrate of the present invention, by dry-pressing or isostatic compaction, only contains a small amount of bonding agent, just with the organic substance draining in base substrate;
2. the cavity faying face of cell-shell base substrate has increased by a circle in conjunction with circle, has increased the bond area of bonding, has guaranteed Cohesion reliability;
3. thin-layer sizing agent main component is identical with cell-shell composition, two cell-shell base substrates can well be connected together, due to when bonding base substrate or dry-pressing or the green state that waits static pressure to go out, without any heating or through pre-burning process, there will not be base substrate because of the deformation heating or pre-burning brings;
4. while boning, adopt fixture location, two base substrates are fixed on same draw point, and axiality is guaranteed, and there will not be the situation of docking dislocation.
Accompanying drawing explanation
Fig. 1 is the structural representation of prior art two-piece-dress cell-shell interference fit;
Fig. 2 is the structural representation of ceramic bulb shell base substrate of the present invention;
Fig. 3 is the enlarged diagram of A part in Fig. 2;
Fig. 4 is the structural representation of fixture;
Fig. 5 is the structural representation of ceramic bulb shell base substrate docking;
Fig. 6 is the structural representation of a plurality of fixture stations;
Fig. 7 is the structural representation of the ceramic bulb shell after moulding;
When Fig. 8 is printing thin-layer sizing agent, bad body is placed station schematic diagram.
Embodiment
As shown in Figure 1, the invention discloses a kind of forming method of two-piece-dress ceramic bulb shell, it comprises the following steps:
Wherein, the main component of thin-layer sizing agent is the alumina powder identical with cell-shell base substrate composition, also add 2 ~ 5% glycerine, 3 ~ 6% terpinols, 1 ~ 4% dioctyl phthalate, 0.5 ~ 2% phthalic acid didecyl ester, 1 ~ 3% epoxy resin, 0.1 ~ 0.5% polyamide wax and 0.1 ~ 0.5% rilanit special, and adopt slurry technology of preparing to be prepared into meet the slurry of the viscosity 30000 ~ 40000mPa * S of film printing needs.
In above-mentioned steps, for handled easily and high efficiency production, can be on one flat plate according to a lot of this fixture stations of physical dimension processing of cell-shell base substrate, as Fig. 6 shows, after waiting the cell-shell of all stations all to bond, whole move in drying box dry.
Slurry curing temperature, the time is adjustable, can dry by normal temperature, also can heating, drying.50～80 ℃ of heat drying temperature, the time is 10～30min; If be placed in air, be dried, the time is 100～150min.
The cell-shell base substrate having bondd is owing to only containing a small amount of bonding agent, after the binder removal of short period, just can enter sintering furnace sintering, make ceramic bulb shell reach solid density, the hexagonal structure that inner grain growth is certain size, finally becomes a two-piece-dress translucent alumina ceramics cell-shell, and cell-shell discharge cavity is spheroid shape, ball-type or cast, the central part of discharge cavity protrudes a circle, but do not affect integral light-transmitting performance, respectively there is one section of capillary at discharge cavity two ends, as shown in Figure 7.
Below in conjunction with embodiment, the present invention is conducted further description.
1, use as requested mist projection granulating the static pressure such as high purity aluminium oxide employing a collection of cell-shell base substrate of method moulding.
2, configure a collection of slurry, main component is high-purity alumina powder, add 3% glycerine, 4.5% terpinol, 2% dioctyl phthalate, 1% phthalic acid didecyl ester, 2% epoxy resin, 0.3% polyamide wax, 0.25% rilanit special, testing size viscosity is at 32000mPa * S, and the slurry sealing preparing is kept at uniform rotation on the turntable in insulating box.
3, by the base substrate capillary of forming down, cavity puts in conjunction with circle direction upward the fixture showing as Fig. 8, and employing film printing technology is the surface printing last layer grout bed of material in conjunction with circle at base substrate cavity, the about 0.04mm of testing size layer thickness.
4, the base substrate that prints slurry is got to half and from the fixture of Fig. 8, transferred in the special fixture of Fig. 6, remaining general base substrate fixedly docks by the steel core pin through endoporus capillaceous with the base substrate of transferring in Fig. 6 fixture one by one.
5, use base substrate all to connecting in rear air, to place 10min.
6, standing time to after fixture is transferred in drying box dry together with base substrate, Temperature Setting is at 65 ℃, time 20min takes out the to be heated and high temperature sinterings such as placement after dry.
7, by above method, prepare after the base substrate that a collection of bonding is good, these are bondd a collection of concentrate to put in air furnace after 420 ℃ of insulations are got rid of bonding agent less in base substrate in 2.5 hours enter again 1800 ℃ of high temperature sinterings in hydrogen furnace, the cell-shell that makes to have bondd reaches into the solid density of porcelain, become the ceramic bulb shell of translucent two-piece-dress structure, discharge cavity is spheroid shape, the central part of discharge cavity protrudes a circle, but does not affect integral light-transmitting performance, and respectively there is one section of capillary at discharge cavity two ends.
Claims (10)
1. a manufacture method for two-piece-dress ceramic bulb shell, is characterized in that, comprises the following steps:
A. the identical ceramic bulb shell base substrate of a pair of shape of moulding, base substrate is comprised of capillary (1) and cavity (2);
B. in the faying face moulding one circle combination of cavity, enclose (3);
C. the thin-layer sizing agent for boning at combination circle surface printing one deck of cell-shell base substrate to be docked;
D. by fixture, two cell-shell base substrates are positioned, make to be bonded together in conjunction with the surperficial slurry of circle;
E. the cell-shell of connection is dried, after slurry drying, takes out the base substrate being bonded together; Finally be shaped to two-piece-dress ceramic bulb shell;
In step c, thin-layer sizing agent and cell-shell base substrate main component are alumina powder, thin-layer sizing agent also adds 2 ~ 5% glycerine, 3 ~ 6% terpinols, 1 ~ 4% dioctyl phthalate, 0.5 ~ 2% phthalic acid didecyl ester, 1 ~ 3% epoxy resin, 0.1 ~ 0.5% polyamide wax and 0.1 ~ 0.5% rilanit special, and adopts slurry technology of preparing to be prepared into meet the thin-layer sizing agent of the viscosity 30000 ~ 40000mPaS of film printing needs.
2. the manufacture method of two-piece-dress ceramic bulb shell according to claim 1, is characterized in that, in steps d, described fixture comprises the draw point that diameter is thinner than capillary inner diameter (4) and the base (5) being coupled with ceramic body cambered surface; By print slurry a base substrate capillary down, be fixed in the fixture designing, the cavity of getting again the base substrate that another one is printed on slurry inserts in draw point down, by two base substrates accurately being located through the draw point of capillary endoporus, and under cell-shell base substrate self gravitation or external force, depress and make to be bonded together in conjunction with the surperficial slurry of circle.
3. the manufacture method of two-piece-dress ceramic bulb shell according to claim 1, is characterized in that, in step b, the height of described combination circle (3) evagination part is 0.5 ~ 1.0mm.
4. the manufacture method of two-piece-dress ceramic bulb shell according to claim 1, it is characterized in that, in step c, adopt film printing or transfer-print technology at combination circle surface printing one deck of cell-shell base substrate to be docked the thin-layer sizing agent for boning, slurry thickness is 0.03 ~ 0.05mm.
5. the manufacture method of two-piece-dress ceramic bulb shell according to claim 1, is characterized in that, in step e, and 50 ~ 80 ℃ of heat drying temperature, the time is 10 ~ 30min; Or be placed in air and be dried, the time is 100 ~ 150min.
6. the manufacture method of two-piece-dress ceramic bulb shell according to claim 1, is characterized in that, in step a, cell-shell base substrate is by dry-pressing or isostatic compaction.
7. a two-piece-dress ceramic bulb shell, comprise two cavitys (2) and be located at respectively the capillary (1) on cavity (2) end, it is characterized in that, on the faying face of two cavitys (2), be equipped with in conjunction with circle (3), and in conjunction with circle (3), be provided with thin-layer sizing agent, two cavitys are bonded together by thin-layer sizing agent;
Wherein, thin-layer sizing agent and cell-shell base substrate main component are alumina powder, thin-layer sizing agent also adds 2 ~ 5% glycerine, 3 ~ 6% terpinols, 1 ~ 4% dioctyl phthalate, 0.5 ~ 2% phthalic acid didecyl ester, 1 ~ 3% epoxy resin, 0.1 ~ 0.5% polyamide wax and 0.1 ~ 0.5% rilanit special, and adopts slurry technology of preparing to be prepared into meet the thin-layer sizing agent of the viscosity 30000 ~ 40000mPaS of film printing needs.
8. two-piece-dress ceramic bulb shell according to claim 7, is characterized in that, the height of described combination circle (3) evagination part is 0.5 ~ 1.0mm.
9. two-piece-dress ceramic bulb shell according to claim 7, is characterized in that, described thin-layer sizing agent thickness is 0.03 ~ 0.05mm.
10. two-piece-dress ceramic bulb shell according to claim 7, is characterized in that, described cavity (2) is semielliptical type, dome-type or half cast.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210021529.2A CN102584183B (en) | 2012-01-31 | 2012-01-31 | Two-piece ceramic bulb shell and manufacturing method thereof |
| PCT/CN2012/071486 WO2013113178A1 (en) | 2012-01-31 | 2012-02-23 | Twinset ceramic blister and manufacturing method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210021529.2A CN102584183B (en) | 2012-01-31 | 2012-01-31 | Two-piece ceramic bulb shell and manufacturing method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102584183A CN102584183A (en) | 2012-07-18 |
| CN102584183B true CN102584183B (en) | 2014-04-02 |
Family
ID=46473523
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210021529.2A Expired - Fee Related CN102584183B (en) | 2012-01-31 | 2012-01-31 | Two-piece ceramic bulb shell and manufacturing method thereof |
Country Status (2)
| Country | Link |
|---|---|
| CN (1) | CN102584183B (en) |
| WO (1) | WO2013113178A1 (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102898173B (en) * | 2012-08-27 | 2014-10-08 | 潮州三环（集团）股份有限公司 | Two-piece ceramic bulb shell molding and docking method |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1031552A (en) * | 1987-08-24 | 1989-03-08 | 胡望江 | A kind of Cemedine for lamp bulb and preparation method |
| JP2000173556A (en) * | 1998-12-09 | 2000-06-23 | Matsushita Electronics Industry Corp | Electric light bulb and mobile lamp |
| CN101652830A (en) * | 2007-03-30 | 2010-02-17 | 奥斯兰姆有限公司 | Component for an electric lamp with outer bulb |
| WO2011057916A1 (en) * | 2009-11-10 | 2011-05-19 | Osram Gesellschaft mit beschränkter Haftung | High-pressure discharge lamp having a single socket |
| CN102169806A (en) * | 2010-12-31 | 2011-08-31 | 王凯 | High-pressure gas discharge lamp |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6620272B2 (en) * | 2001-02-23 | 2003-09-16 | Osram Sylvania Inc. | Method of assembling a ceramic body |
| CN101410348B (en) * | 2006-03-24 | 2013-01-09 | 日本碍子株式会社 | Sintered body, light emitting tube and process for manufacturing the same |
| CN201532933U (en) * | 2009-08-06 | 2010-07-21 | 海宁新光阳光电有限公司 | Arc tube of ceramic metal halide lamp |
-
2012
- 2012-01-31 CN CN201210021529.2A patent/CN102584183B/en not_active Expired - Fee Related
- 2012-02-23 WO PCT/CN2012/071486 patent/WO2013113178A1/en active Application Filing
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1031552A (en) * | 1987-08-24 | 1989-03-08 | 胡望江 | A kind of Cemedine for lamp bulb and preparation method |
| JP2000173556A (en) * | 1998-12-09 | 2000-06-23 | Matsushita Electronics Industry Corp | Electric light bulb and mobile lamp |
| CN101652830A (en) * | 2007-03-30 | 2010-02-17 | 奥斯兰姆有限公司 | Component for an electric lamp with outer bulb |
| WO2011057916A1 (en) * | 2009-11-10 | 2011-05-19 | Osram Gesellschaft mit beschränkter Haftung | High-pressure discharge lamp having a single socket |
| CN102169806A (en) * | 2010-12-31 | 2011-08-31 | 王凯 | High-pressure gas discharge lamp |
Also Published As
| Publication number | Publication date |
|---|---|
| WO2013113178A1 (en) | 2013-08-08 |
| CN102584183A (en) | 2012-07-18 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| KR101510658B1 (en) | Dye-sensitized solar cell and method for manufacturing the same | |
| CN105021326A (en) | One-piece ceramic capacitance pressure transducer and manufacture method | |
| CN102584183B (en) | Two-piece ceramic bulb shell and manufacturing method thereof | |
| CN105424231B (en) | A kind of high-precision ceramic pressure sensor | |
| CN104924412B (en) | The connection method of reaction sintering silicon carbide ceramic biscuit | |
| CN103585897B (en) | Multi-channel ceramic/metal composite membrane and preparation method thereof | |
| CN104217860B (en) | A kind of superhigh temperature long-life low-pressure liquid aluminium electrolutic capacitor and its manufacture method | |
| JPS6237683A (en) | Tool for baking ceramic | |
| CN105428035A (en) | Electronic element and production method thereof | |
| CN204054661U (en) | A kind of annulus pasting mould of enhancing productivity | |
| CN107021774B (en) | Glass-based composite sealing material for flat-plate oxygen sensor and sealing method thereof | |
| CN102249695A (en) | Manufacturing method of arc tube for ceramic metal halide lamp | |
| CN101008482B (en) | Matrix used in metallized ceramic light-reflecting cup and manufacture method thereof | |
| CN108447964A (en) | The manufacturing method and LED lamp of LED component | |
| CN114942091A (en) | Ceramic capacitance pressure sensor and preparation method thereof | |
| TWM456284U (en) | Casing | |
| CN101172865A (en) | Hollow ceramic ball and method for producing the same | |
| CN217079497U (en) | Novel glazed tile with multiple glazes | |
| CN205960081U (en) | Exempt from a formula aluminium and change nickel electrode lug | |
| CN201887726U (en) | Multiple row-arrangement composite substrate, frequency device group and frequency device | |
| CN214032255U (en) | High thermal shock nature sealing glass prefab | |
| CN101814349B (en) | Moulding mould for thermistors and method for manufacturing thermistors | |
| CN204165404U (en) | A kind of target sintering support plate | |
| CN219370704U (en) | Sintering die for glass sealing insulator | |
| CN204831647U (en) | Ceramic condenser formula pressure sensor |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| ASS | Succession or assignment of patent right |
Owner name: YANG CHAOPING Free format text: FORMER OWNER: CHAOZHOU CHAOHAO ELECTRIC LIGHT SOURCE CO., LTD. Effective date: 20130306 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20130306 Address after: 521000 Guangdong Province, Chaozhou city Xiangqiao District Xiangqiao North Road No. 9, 2 Yang CuO Xiang Applicant after: Yang Chaoping Address before: 521000 No. 45, South Road, Xiangqiao District, Guangdong, Chaozhou Applicant before: Chaozhou Zhaohao Electric Light Source Co., Ltd. |
|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20140402 Termination date: 20170131 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |