CN102531788A - Pesticide granule for controlling soil insects of peanut and preparation method thereof - Google Patents
Pesticide granule for controlling soil insects of peanut and preparation method thereof Download PDFInfo
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- CN102531788A CN102531788A CN2012100140031A CN201210014003A CN102531788A CN 102531788 A CN102531788 A CN 102531788A CN 2012100140031 A CN2012100140031 A CN 2012100140031A CN 201210014003 A CN201210014003 A CN 201210014003A CN 102531788 A CN102531788 A CN 102531788A
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Abstract
The invention discloses a pesticide granule for controlling soil insects of peanuts and a preparation method thereof. The pesticide granule contains the following ingredients in percentage by weight: 0.5-15% of carbosulfan as active ingredient, 30-70% of a carrier fertilizer, 0.1-2% of a sustained release agent, 0.1-10% of a binder, 0.1-0.5% of a coating agent, and the balance of fillers. The preparation method comprises the following steps of: thoroughly mixing the above ingredients, granulating by film-coating method, oven-drying and sieving to obtain the final product of pesticide granule. The application of the pesticide granule achieves synchronization of applying the fertilizer and killing soil insects such as white grubs, cutworms, wireworms and mole crickets; and overcomes the problem in the prior art that users apply pesticides and fertilizers separately and repeatedly.
Description
Technical field
The present invention relates to a kind of fertilizer granules that is used to prevent and treat peanut soil pest and preparation method thereof.
Background technology
In recent years, peanut soil pest harm increases the weight of day by day, has become subterranean pest-insects such as the important factor, the especially grub that influences the peanut growth, cutworm, wireworm, mole cricket and has taken place seriously peanut yield have been constituted serious threat.According to statistics, peanut is caused harm because of subterranean pest-insect and is generally caused the underproduction 20%～40%, and the serious underproduction 70～80%, even total crop failure cause the peanut downgrade to be unable to estimate especially.
At present, the main medicament that is used to prevent and treat peanut soil pest has terbufos, carbofuran, Chlorpyrifos 94, carbosulfan, Avrmectin etc., and wherein terbufos and carbofuran belong to riskiest pesticide, can not satisfy the needs of agriculture nuisanceless production.
Carbosulfan applaud again granville carbosulfan, year winter, the spy that sleeps peacefully, to be that carbofuran is low poison one of kind, per os toxicity is medium, percutaneous toxicity is low, no aggregate toxicity, do not have lopsided, carcinogenic and mutagenesis.Lower to natural enemy and beneficial organism toxicity, be carbamate chemicals for agriculture, i.e. the low verivate that poisons of carbofuran agricultural chemicals belongs to highly effective and safe, insecticidal/acaricidal agent easy to use, is one of comparatively ideal alternative kind of carbofuran.Its lethality is strong, and instant effect has stomach toxicity and action of contace poison.Characteristics are that fat-soluble, interior absorption is good, seepage force is strong, effect rapid, residual low, long residual effect, safe in utilization etc. is arranged, all effective to adult and larva, harmless to crop.
In traditional peanut cultivation technology, mostly the application method of the sterilant of control subterranean pest-insect is ditch spread, spreads manuer in holes or converts water and irritate root, increases peasant's labour intensity and work number of times, and the utilization ratio of pesticide active ingredient is not high yet; Simultaneously, in the traditional agricultural production technology, applying fertilizer and sterilant separate, and twice or the way of use of insecticide and fertilizer repeatedly, have increased peasant's labour intensity and work number of times, are unfavorable for agricultural development.
The inventor furthers investigate the formulation and the insecticidal mechanism of carbosulfan; Make full use of carbosulfan can in the good characteristic of absorption, it is combined with fertilizer, process fertilizer granules; Applied once can be accomplished fertilising and desinsection two procedures simultaneously; Avoid dispenser in the past and the situation that fertilising can not take into account, saved time and manual work, improved production efficiency.
Carbosulfan is combined to process fertilizer granules and uses and still not have report with fertilizer.
Summary of the invention
Technical problem to be solved: the present invention is directed to the prior art deficiency provides a kind of carbosulfan to combine with the science of fertilizer and a kind of fertilizer granules of preventing and treating peanut soil pest of developing; Applied once both can apply fertilizer; Satisfy the needs that peanut grows; Can kill subterranean pest-insects such as grub, cutworm, wireworm, mole cricket again, overcome that user under the prior art condition wants twice or the way of use of insecticide and fertilizer repeatedly.
The present invention also provides the preparation method of above-mentioned fertilizer granules.
Technical scheme: a kind of fertilizer granules of preventing and treating peanut soil pest of the present invention is made up of following raw material: carbosulfan, carrier fertilizer, sustained release dosage, sticker, coating agent, filler.
In insecticide fertilizer granule gross weight, wherein: carbosulfan 0.5%～15%, carrier fertilizer 30%～70%, sustained release dosage 0.1%～2%, sticker 0.1%～10%, coating agent 0.1～0.5%, all the other are filler.
Described carrier fertilizer is one or more the mixing in ammonium chloride, ammonium sulfate, urea, Repone K, potassium magnesium sulfate, phosphoric acid fine particle calcium carbonate, superphosphate of lime, the monoammonium phosphate; Nitrogen element nutrient content in the carrier fertilizer is 5%～15% of a fertilizer granules gross weight; Phosphorus element content is 5%～15% of an insecticide fertilizer granule gross weight, and potassium element content is 5%～15% of insecticide fertilizer granule gross weight.Calcium element content is 0%～10% of an insecticide fertilizer granule gross weight, and magnesium element content is 0%～10% of an insecticide fertilizer granule gross weight.
Described carrier fertilizer also contains Zinc Sulphate Monohydrate and borax, and its zinc element content is 0%～2% of fertilizer granules gross weight, and boron content is 0%～2% of an insecticide fertilizer granule gross weight.
Described sustained release dosage is Z 150PH or gum arabic.
Described sticker is one or more the mixing in attapulgite, paraffin, rosin, pasted starch, XG 550, CMC 99.5, NATROSOL 250, the methylcellulose gum.
Described coating agent is one or more the mixing in Z 150PH, Vinylpyrrolidone polymer, vibrin, vinylformic acid synthetic polymer, vinyl resin membrane-forming agent, butadiene resin membrane-forming agent, polyurethane film-forming agent, the cellulose nitrate membrane-forming agent.
Described filler is a kaolin.
A kind of preparation method who prevents and treats the fertilizer granules of peanut soil pest: after in airtight stirred pot, mixing the former medicine of 0.5%～15% carbosulfan, 30%～70% carrier fertilizer, 0.1%～2% sustained release dosage, 0.1%～10% sticker, 0.1%～0.5% coating agent, surplus filler; Add in the granulating equipment and carry out the granulation of coating method; Under 80 ℃～100 ℃ conditions, be dried to the particle water cut less than 3%; Screening; Size range 2000um～4000um through after the assay was approved, promptly obtains required fertilizer granules; The powder sieving thing is back to stirred pot after crushed to be mixed again; Unacceptable product is back to stirred pot after the check analysis reason mixes again; Mix and adopt the method for fractional steps; Carrier fertilizer or the filler that the lower starting material of component concentration mix certain mass earlier again with other mixing of materials, to guarantee the homogeneity of product content, drying temperature is at 80 ℃～100 ℃; The variation of strict controlled temperature and fluctuation are in order to avoid the decomposition and the loss of agricultural chemicals, fertilizer composition.
Compared with prior art, the present invention has following unusual effect.
Fertilizer granules of the present invention; Combine to develop a kind of fertilizer granules of preventing and treating peanut soil pest that forms with the science of fertilizer through the insecticide ingredient carbosulfan; Applied once both can apply fertilizer, and satisfied the needs that peanut grows, and can kill subterranean pest-insects such as grub, cutworm, wireworm, mole cricket again; Overcome that user under the prior art condition wants twice or the way of use of insecticide and fertilizer repeatedly; Alleviate peasant's labour intensity and work number of times, saved time and manual work, improved production efficiency.
Fertilizer granules of the present invention also has good control effect to peanut root-knot nematode.
Fertilizer granules of the present invention adopts current up-to-date slow release method, guarantees that effectively the science of agricultural chemicals, fertilizer discharges, and guarantees desinsection, fertilising double effects, prolongs the lasting period of product, improves drug effect and agricultural chemicals utilization ratio, reduces the waste of agricultural chemicals, fertilizer.Therefore this technology effectively, science, make rational use of resources, the protection environment has great significance, and the agricultural input that reduces the user and the increasing both production and income of agricultural are also played positive pushing effect.
Safety, low toxicity, low risk are used conveniently in fertilizer granules formulation of the present invention environmental protection.
In order better to verify practical application effect of the present invention, the field control effectiveness test effect of insecticide fertilizer granule of the present invention is described with the field efficacy instance below.
Supply the reagent agent: (1) test medicine: 3% carbosulfan fertilizer granules.(2) contrast medicament: 5% carbosulfan granule.
Controlling object: peanut soil pest.
Application method: 3% carbosulfan fertilizer granules of the present invention is used as base manure; Contrast medicament 5% carbosulfan granule is spreaded manuer in holes.
Test design.
Test-results: test-results is seen table 1～5.Test-results shows; 3% carbosulfan fertilizer granules mu improves along with the increase of consumption the preventive effect of peanut soil pest (grub, cutworm, wireworm, mole cricket) with 5000 grams, 5833 grams, 6667 grams, behind the medicine behind 15 days, medicine 30 days average preventive effect be superior to contrasting medicament 5% carbosulfan granule.
3% carbosulfan fertilizer granules mu is respectively 22.9%, 26.9%, 28.3% with the stimulation ratio of 5000 grams, 5833 grams, 6667 grams.Finding in the process of the test has the poisoning phenomenon and non-rake is marked biological detrimentally affect.
Table 1,3% carbosulfan fertilizer granules control peanut grub test of pesticide effectiveness result.
Table 2,3% carbosulfan fertilizer granules control peanut cutworm test of pesticide effectiveness result.
Table 3,3% carbosulfan fertilizer granules control peanut wireworm test of pesticide effectiveness result.
Table 4,3% carbosulfan fertilizer granules control peanut mole cricket test of pesticide effectiveness result.
The effect of increasing production of table 5, the 3% carbosulfan fertilizer granules peanut test of pesticide effectiveness.
Fertilizer granules preparing method's of the present invention production technique is ripe, can produce fertilizer granules up-to-standard, effect stability according to product standard.Be checking constant product quality property, carried out the heat storage stability test of product: under 54 ℃ ± 2 ℃ conditions, stored 14 days the rate of decomposition of mensuration effective constituent, moisture, pH value etc.Test-results table 6 shows that constant product quality property is good, the requirement of each item index conformance with standard.
Table 6,3% carbosulfan fertilizer granules heat storage stability test-results.
Description of drawings
Fig. 1 is technological process of production figure of the present invention.
Embodiment
As shown in Figure 1; According to a kind of preparation method who prevents and treats the fertilizer granules of peanut soil pest of the present invention, by weight percentage, after in airtight stirred pot, mixing the former medicine of 0.5%～15% carbosulfan, 30%～70% carrier fertilizer, 0.1%～2% sustained release dosage, 0.1%～10% sticker, 0.1%～0.5% coating agent, surplus filler; Add in the granulating equipment and carry out the granulation of coating method; Under 80 ℃～100 ℃ conditions, be dried to the particle water cut, screening, size range 2000um～4000um less than 3%; Through after the assay was approved, promptly obtain required fertilizer granules; The powder sieving thing is back to stirred pot after crushed to be mixed again; Unacceptable product is back to stirred pot after the check analysis reason mixes again; Mix and adopt the method for fractional steps; Carrier fertilizer or the filler that the lower starting material of component concentration mix certain mass earlier again with other mixing of materials, to guarantee the homogeneity of product content, drying temperature is at 80 ℃～100 ℃; The variation of strict controlled temperature and fluctuation are in order to avoid the decomposition and the loss of agricultural chemicals, fertilizer composition.
Can be made into the different fertilizer granules of active constituent content; By the gross weight of fertilizer granules, activeconstituents carbosulfan 0.5%～15%, fertilizer component nitrogen element nutrient content is 5%～15% of a fertilizer granules gross weight; Phosphorus element content is 5%～15% of an insecticide fertilizer granule gross weight; Potassium element content is 5%～15% of insecticide fertilizer granule gross weight, and calcium element content is 0%～10% of an insecticide fertilizer granule gross weight, and magnesium element content is 0%～10% of an insecticide fertilizer granule gross weight; Zinc element content is 0%～2% of fertilizer granules gross weight, and boron content is 0%～2% of an insecticide fertilizer granule gross weight.
Claims (8)
1. fertilizer granules of preventing and treating peanut soil pest, it is characterized in that: activeconstituents is a carbosulfan, in the fertilizer granules gross weight; Wherein: carbosulfan 0.5%～15%; Carrier fertilizer 30%～70%, sustained release dosage 0.1%～2%, sticker 0.1%～10%; Coating agent 0.1～0.5%, surplus are filler.
2. a kind of fertilizer granules of preventing and treating peanut soil pest according to claim 1; It is characterized in that: described carrier fertilizer is one or more the mixing in ammonium chloride, ammonium sulfate, urea, Repone K, potassium magnesium sulfate, phosphoric acid fine particle calcium carbonate, superphosphate of lime, the monoammonium phosphate; Nitrogen element nutrient content in the carrier fertilizer is 5%～15% of a fertilizer granules gross weight; Phosphorus element content is 5%～15% of an insecticide fertilizer granule gross weight, and potassium element content is 5%～15% of insecticide fertilizer granule gross weight; Calcium element content is 0%～10% of an insecticide fertilizer granule gross weight, and magnesium element content is 0%～10% of an insecticide fertilizer granule gross weight.
3. a kind of fertilizer granules of preventing and treating peanut soil pest according to claim 1; It is characterized in that: described carrier fertilizer also contains Zinc Sulphate Monohydrate and borax; Its zinc element content is 0%～2% of fertilizer granules gross weight, and boron content is 0%～2% of an insecticide fertilizer granule gross weight.
4. a kind of fertilizer granules of preventing and treating peanut soil pest according to claim 1 is characterized in that: described sustained release dosage is Z 150PH or gum arabic.
5. a kind of fertilizer granules of preventing and treating peanut soil pest according to claim 1 is characterized in that: described sticker is one or more the mixing in attapulgite, paraffin, rosin, pasted starch, XG 550, CMC 99.5, NATROSOL 250, the methylcellulose gum.
6. a kind of fertilizer granules of preventing and treating peanut soil pest according to claim 1 is characterized in that: described coating agent is one or more the mixing in Z 150PH, Vinylpyrrolidone polymer, vibrin, vinylformic acid synthetic polymer, vinyl resin membrane-forming agent, butadiene resin membrane-forming agent, polyurethane film-forming agent, the cellulose nitrate membrane-forming agent.
7. a kind of fertilizer granules of preventing and treating peanut soil pest according to claim 1, it is characterized in that: described filler is a kaolin.
8. a preparation method who prevents and treats the fertilizer granules of peanut soil pest is: after in airtight stirred pot, mixing the former medicine of 0.5%～15% carbosulfan, 30%～70% carrier fertilizer, 0.1%～2% sustained release dosage, 0.1%～10% sticker, 0.1%～0.5% coating agent, surplus filler; Add in the granulating equipment and carry out the granulation of coating method; Under 80 ℃～100 ℃ conditions, be dried to the particle water cut less than 3%; Screening; Size range 2000um～4000um through after the assay was approved, promptly obtains required fertilizer granules; The powder sieving thing is back to stirred pot after crushed to be mixed again; Unacceptable product is back to stirred pot after the check analysis reason mixes again; Mix and adopt the method for fractional steps; Carrier fertilizer or the filler that the lower starting material of component concentration mix certain mass earlier again with other mixing of materials, to guarantee the homogeneity of product content, drying temperature is at 80 ℃～100 ℃; The variation of strict controlled temperature and fluctuation are in order to avoid the decomposition and the loss of agricultural chemicals, fertilizer composition.
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| CN2012100140031A CN102531788A (en) | 2012-01-17 | 2012-01-17 | Pesticide granule for controlling soil insects of peanut and preparation method thereof |
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| CN103058790A (en) * | 2012-12-29 | 2013-04-24 | 广东中迅农科股份有限公司 | Cyfluthrin drug fertilizer granules and preparation method thereof |
| CN103058767A (en) * | 2012-12-29 | 2013-04-24 | 广东中迅农科股份有限公司 | Flubendiamide drug fertilizer granules and preparation method thereof |
| CN103058788A (en) * | 2012-12-29 | 2013-04-24 | 广东中迅农科股份有限公司 | Chlorfenapyr drug fertilizer granules and preparation method thereof |
| CN103102219A (en) * | 2013-01-27 | 2013-05-15 | 成都科利隆生化有限公司 | Pesticide-fertilizer mixer for controlling rice pests |
| CN103102218A (en) * | 2013-01-27 | 2013-05-15 | 成都科利隆生化有限公司 | Pesticide-fertilizer mixer for controlling rice stem borers and preparation method of pesticide-fertilizer mixer |
| CN103102224A (en) * | 2013-03-11 | 2013-05-15 | 叶长东 | Insecticide-fertilizer composition containing benfuracarb |
| CN103130568A (en) * | 2013-01-27 | 2013-06-05 | 成都科利隆生化有限公司 | Thiamethoxam insecticide-fertilizer mixture and preparing method thereof |
| CN103351212A (en) * | 2013-06-07 | 2013-10-16 | 安徽金阳环保肥业有限公司 | Special composite fertilizer for peanuts |
| CN103518567A (en) * | 2013-06-27 | 2014-01-22 | 山东省花生研究所 | Method for environment-friendly prevention and control of underground peanut insects |
| CN104311368A (en) * | 2014-10-22 | 2015-01-28 | 肥东县花生原种场 | Soil improved organic fertilizer for peanut planting and preparation method thereof |
| CN104311344A (en) * | 2014-10-22 | 2015-01-28 | 肥东县花生原种场 | Organic peanut planting controlled-release functional fertilizer and preparation method thereof |
| CN105237203A (en) * | 2015-10-13 | 2016-01-13 | 山东锦鸿源生态农业有限责任公司 | Long-acting biological medicine fertilizer for peanuts and preparation method of long-acting biological medicine fertilizer |
| CN105360177A (en) * | 2015-12-13 | 2016-03-02 | 沈阳金诚科技有限公司 | Preparation method of Azadirachta indica sustained-release insecticide-fertilizer granules |
| CN106116801A (en) * | 2016-06-20 | 2016-11-16 | 河南中天恒信生物化学科技有限公司 | A kind of bean field medicine fertilizer granule and preparation method thereof |
| CN108863640A (en) * | 2018-06-27 | 2018-11-23 | 安徽瑞然生物药肥科技有限公司 | A kind of medicine fertilizer, preparation method and application method preventing and treating fruit tree iron deficiency disease disease |
| CN108892566A (en) * | 2018-07-31 | 2018-11-27 | 合肥浦邦农业科技有限公司 | A kind of novel film-coated and slow release fertilizer and preparation method thereof |
| CN111995470A (en) * | 2020-09-11 | 2020-11-27 | 成都云图控股股份有限公司 | Mineral source fulvic acid slow release fertilizer and preparation method thereof |
| CN112273392A (en) * | 2020-11-03 | 2021-01-29 | 中诚国联（河南）生物科技有限公司 | Application of insecticide-fertilizer granules containing clothianidin and imidacloprid in controlling peanut grubs |
| CN115745693A (en) * | 2022-11-25 | 2023-03-07 | 中国农业大学 | Pesticide slow-release pesticide fertilizer granules and preparation method and application thereof |
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| CN103058767A (en) * | 2012-12-29 | 2013-04-24 | 广东中迅农科股份有限公司 | Flubendiamide drug fertilizer granules and preparation method thereof |
| CN103058788A (en) * | 2012-12-29 | 2013-04-24 | 广东中迅农科股份有限公司 | Chlorfenapyr drug fertilizer granules and preparation method thereof |
| CN103058790A (en) * | 2012-12-29 | 2013-04-24 | 广东中迅农科股份有限公司 | Cyfluthrin drug fertilizer granules and preparation method thereof |
| CN103102219A (en) * | 2013-01-27 | 2013-05-15 | 成都科利隆生化有限公司 | Pesticide-fertilizer mixer for controlling rice pests |
| CN103102218A (en) * | 2013-01-27 | 2013-05-15 | 成都科利隆生化有限公司 | Pesticide-fertilizer mixer for controlling rice stem borers and preparation method of pesticide-fertilizer mixer |
| CN103130568A (en) * | 2013-01-27 | 2013-06-05 | 成都科利隆生化有限公司 | Thiamethoxam insecticide-fertilizer mixture and preparing method thereof |
| CN103102224A (en) * | 2013-03-11 | 2013-05-15 | 叶长东 | Insecticide-fertilizer composition containing benfuracarb |
| CN103102224B (en) * | 2013-03-11 | 2014-08-27 | 叶长东 | Insecticide-fertilizer composition containing benfuracarb |
| CN103351212B (en) * | 2013-06-07 | 2015-07-29 | 安徽金阳环保肥业有限公司 | One cultivates peanut composite fertilizer special |
| CN103351212A (en) * | 2013-06-07 | 2013-10-16 | 安徽金阳环保肥业有限公司 | Special composite fertilizer for peanuts |
| CN103518567A (en) * | 2013-06-27 | 2014-01-22 | 山东省花生研究所 | Method for environment-friendly prevention and control of underground peanut insects |
| CN103518567B (en) * | 2013-06-27 | 2015-09-16 | 山东省花生研究所 | A kind of method of green prevention and control peanut soil pest |
| CN104311368A (en) * | 2014-10-22 | 2015-01-28 | 肥东县花生原种场 | Soil improved organic fertilizer for peanut planting and preparation method thereof |
| CN104311344A (en) * | 2014-10-22 | 2015-01-28 | 肥东县花生原种场 | Organic peanut planting controlled-release functional fertilizer and preparation method thereof |
| CN105237203A (en) * | 2015-10-13 | 2016-01-13 | 山东锦鸿源生态农业有限责任公司 | Long-acting biological medicine fertilizer for peanuts and preparation method of long-acting biological medicine fertilizer |
| CN105237203B (en) * | 2015-10-13 | 2018-07-27 | 山东锦鸿源生态农业有限责任公司 | A kind of long-acting peanut biological medicine fertilizer and preparation method thereof |
| CN105360177A (en) * | 2015-12-13 | 2016-03-02 | 沈阳金诚科技有限公司 | Preparation method of Azadirachta indica sustained-release insecticide-fertilizer granules |
| CN106116801A (en) * | 2016-06-20 | 2016-11-16 | 河南中天恒信生物化学科技有限公司 | A kind of bean field medicine fertilizer granule and preparation method thereof |
| CN108863640A (en) * | 2018-06-27 | 2018-11-23 | 安徽瑞然生物药肥科技有限公司 | A kind of medicine fertilizer, preparation method and application method preventing and treating fruit tree iron deficiency disease disease |
| CN108892566A (en) * | 2018-07-31 | 2018-11-27 | 合肥浦邦农业科技有限公司 | A kind of novel film-coated and slow release fertilizer and preparation method thereof |
| CN111995470A (en) * | 2020-09-11 | 2020-11-27 | 成都云图控股股份有限公司 | Mineral source fulvic acid slow release fertilizer and preparation method thereof |
| CN112273392A (en) * | 2020-11-03 | 2021-01-29 | 中诚国联（河南）生物科技有限公司 | Application of insecticide-fertilizer granules containing clothianidin and imidacloprid in controlling peanut grubs |
| CN115745693A (en) * | 2022-11-25 | 2023-03-07 | 中国农业大学 | Pesticide slow-release pesticide fertilizer granules and preparation method and application thereof |
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Application publication date: 20120704 |