CN102524657B - Production method of full cream stable bran powder - Google Patents
Production method of full cream stable bran powder Download PDFInfo
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- CN102524657B CN102524657B CN201210007481XA CN201210007481A CN102524657B CN 102524657 B CN102524657 B CN 102524657B CN 201210007481X A CN201210007481X A CN 201210007481XA CN 201210007481 A CN201210007481 A CN 201210007481A CN 102524657 B CN102524657 B CN 102524657B
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Abstract
The invention relates to a method for producing full cream stable bran powder. According to the method, fresh rice bran is used as raw materials, and a double-screw extruding machine is used as a main reactor for preparing a full cream stable bran product. The method has the advantages that the production step is simple, the product stability is good, the waste emission is avoided, and the method belongs to a novel energy-saving and emission-reduction stable production and processing method for full cream bran.
Description
Technical field
The present invention relates to a kind of method of suitability for industrialized production full cream stable bran powder, belong to the deep processing of farm products category.Particularly, the present invention relates to adopt Twin-Screw Extrusion Technology to produce the method for Full-cream stable rice bran.
Background technology
Rice bran is the accessory substance of rice processing, and it is yellow that fresh rice bran is, and a meter fragrance is arranged, and has the flakey irregular structure, accounts for 6～8wt% of paddy total amount.Fresh rice bran is nutritious, but fresh rice bran is difficult for storage, and reason is: (1) rice milling process makes original rice bran oil and lipase separated in cell be in contact with one another, and is hydrolyzed rapidly, causes becoming sour; (2) stand the further oxidation of peroxidase, produce niff; (3) the harmful worm's ovum be mingled with in fresh rice bran and the vital movement of microorganism also can be accelerated the rice bran bad change of becoming sour.Therefore, fresh rice bran is not easy to extract in time rice bran oil and is applied to field of food, the necessary above-mentioned lipase of passivation and peroxidase, and kill harmful worm's ovum and microorganism, after rice bran stabilization is processed, rice bran just is convenient to carry out deep development.
At present, the industrial method that is applied to stabilizing rice bran has heat treating process, method of chemical treatment, biological enzyme and extrusion, though this several method can be realized the full-cream stabilisation of rice bran, but lipase active suppresses not exclusively, rice bran after processing generally can only be stored 1～2 month, can not directly apply in field of food.The industrial method of at present common several stabilizing rice brans specifically describes as follows:
Heat treating process: heat treating process is that the method by heating makes the lipase deactivation in rice bran, and the microorganism in simultaneously can the deactivation rice bran, to reach the purpose of stabilizing rice bran.At present, this technology is due to the restriction that is subject to heating material temperature and mode of heating etc., and shelf time is only the two weeks left and right.
Method of chemical treatment: method of chemical treatment is to add pH value or the ionic strength that chemical reagent changes rice bran in rice bran, to reach the activity of lipase in inhibition or passivation rice bran.Often by spraying hydrochloric acid or interpolation sodium pyrosulfite and/or sodium sulfite, undertaken.The method of chemical treatment equipment investment is little, but, owing to having added chemical reagent in product, has limited the range of application of rice bran at field of food, and the method is used acid simultaneously, higher to equipment requirement.
Biological enzyme: biological enzyme is to utilize biology enzyme to make the lipase inactivation in rice bran, so that the stable method of rice bran, its principle is with naturally occurring fat hydrolase in vegetable protein enzymatic inactivation rice bran.The shortcoming of biological enzyme is that production cost is too high, and the vigor of enzyme is unstable and very easily descend, and production technology is difficult to control, and is not suitable for suitability for industrialized production.
Extrusion: current extrusion comparative maturity, can suppress the activity of lipase and peroxidase, be generally used for preprocess method that rice bran oil extracts but not the method for stabilizing rice bran, the rice bran shelf time after processing was no longer than 2 months.
Simultaneously, at present extrusion extruder used is single-screw extrusion machine, and its operation principle is to rely on frictional force on material and barrel to be greater than the conveying that frictional force on material and screw rod realizes material, and the two difference is larger, and transfer efficiency is higher; If material sticks on screw rod, can not be fed forward; If material properties makes its frictional force to barrel less, can't in single-screw extrusion machine, complete extruding.In addition, single-screw extrusion machine is only squeezing action and rubbing action to the mechanism of material, lacks the effects such as mixing, shearing, and this has just limited the application of single-screw extrusion machine.But, need the effects such as high temperature, high pressure, high shear, high mixing as the extrusion process of stablizing the fresh rice bran raw material, and single-screw extrusion machine be can not be completed alone these effects, therefore, single-screw extrusion machine is not suitable for being applied to the stabilization processes of full-cream rice bran.
After the industrial method of the fresh rice bran stabilisation therefore, existed at present exists rice bran to process, the storage life falls short of, production cost is high, production technology is difficult to control, be not suitable for suitability for industrialized production, be not suitable for application at field of food, also or to the shortcomings such as requirement height of equipment.
For solving the above-mentioned problems in the prior art, the present inventor is furtherd investigate, found that: adopting Twin-Screw Extrusion Technology to produce Full-cream stable rice bran is most economical, the most promising method at present, the full cream stable bran powder of producing by method of the present invention has that color and luster is good, dissolubility is good, shelf time can reach the characteristics more than 12 months, is suitable as novel food additives; The method has not only been invented a kind of antihunt means of full-cream rice bran, has broken rice bran and can only, as the conventional use of feed, also start the new way of paddy processing industry rice bran comprehensive utilization.
Summary of the invention
The purpose of this invention is to provide a kind of full cream stable bran powder product.In full cream stable bran powder of the present invention, by weight percentage, the content of free fatty is less than 10wt%; If the vigor of peroxidase in fresh rice bran is considered as to 100%, the vigor of peroxidase residual enzyme is less than 4%, and shelf time reached more than 12 months, can be applicable in field of food.
Full cream stable bran powder color and luster of the present invention is pale yellow, have roasted nuts fragrance; Absorption more easy to digest; The Soluble Fiber increased content.
Prepare full cream stable bran powder product of the present invention according to following methods and equipment.
Another object of the present invention is to provide the method for the production of full cream stable bran powder, it is raw material that described method be take fresh full-cream rice bran, adopt Twin-Screw Extrusion Technology, the twin (double) screw extruder of take is prepared as main reactor, by cleaning, screens, modified, extruding, dries and pulverize five steps and prepare full cream stable bran powder.
Utilizing the method for suitability for industrialized production full cream stable bran powder of the present invention, have that production stage is simple, product stability good, no waste discharge, is a kind of full-cream rice bran stabilization production and processing method of novel energy-saving emission-reducing.
A further object of the present invention is to provide the equipment for the production of full cream stable bran powder, and described equipment comprises cleaning screening plant, modifying device, pressurizing unit, drying unit and reducing mechanism.
The specific embodiment
In the present invention, described fresh rice bran can be the fresh rice bran from output in the processing of the paddy such as japonica rice, long-grained nonglutinous rice, glutinous rice, but is not limited to this.In present specification, described fresh rice bran refers in process of manufacture that 6 hours with interior rice bran.
As a first aspect of the present invention, the present invention relates to a kind of full cream stable bran powder.In full cream stable bran powder of the present invention, by weight percentage, free fatty is less than 10%; If the vigor of peroxidase in fresh rice bran is considered as to 100%, the vigor of residual peroxide enzyme is less than 4%; Shelf time can reach more than 12 months.
Particularly, in described full cream stable bran powder, by weight percentage, free fatty is less than 10%; Soluble Fiber content is increased to 10～20% by 2～5%.If the vigor of peroxidase in fresh rice bran is considered as to 100%, the vigor of residual peroxide enzyme is less than 4%.Shelf time can reach more than 12 months.
More preferably, in described full cream stable bran powder, by weight percentage, free fatty is less than 10%; While not adding cellulase, Soluble Fiber content is increased to 10～15% by 2～5%; While adding cellulase, Soluble Fiber content is increased to 15～20% by 2～5%.If the vigor of peroxidase in fresh rice bran is considered as to 100%, the vigor of residual peroxide enzyme is less than 4%.Shelf time can reach more than 12 months.
In addition, full cream stable bran powder of the present invention has following features and advantage:
(1) outward appearance: buff powder, there is strong roasted nuts fragrance.
(2) granularity: 100～500 orders, preferably 100～400 orders, more preferably 150～200 orders.
(3) other quality index: in full cream stable bran powder of the present invention, by weight percentage, protein is 10～14%, and moisture is less than 10%, and starch is 20～25%, and fat is 15～20%, and total reducing sugar is 5～8%, and ash content is less than 8%.
(4) harmful worm's ovum and microbiological indicator: total plate count is less than 1000CFU/g, does not detect bacillus cereus and harmful worm's ovum.
(5) shelf time can reach more than 12 months, and for example shelf time can reach 12～36 months, was preferably 12～24 months, more preferably 12～18 months.
The above-mentioned content assaying method about free fatty, Soluble Fiber, protein, starch, fat, total reducing sugar, ash content is conventional assay method.Particularly, the assay method of described free fatty for example can carry out according to the described method of GB/T 15684-1995; The assay method of described Soluble Fiber for example can carry out according to the described method of GB/T5009.88-2008; Described protein measuring method for example can carry out according to the described method of GB5009.5-2010; The assay method of above-mentioned starch for example can carry out according to the described method of GB/T5009.9-2008; The assay method of above-mentioned fat for example can carry out according to the described method of GB/T5009.6-2003; The assay method of above-mentioned total reducing sugar for example can carry out according to the described method of GB/T5413.5-1997; The assay method of above-mentioned ash content for example can carry out according to the described method of GB/T5009.4-2010.
In addition, the assay method of vigor, total plate count and the bacillus cereus of peroxidase is not particularly limited, as long as can measure reliably These parameters.
Total plate count for example can be carried out according to the described method of GB/T4789.2-2010; Bacillus cereus for example can carry out according to the described method of GB/T4789.14-2003.
Especially, the vigor of peroxidase residual enzyme can be according to VETTER J L, STEINBERG M P.Qualitative determination of peroxidase in sweet corn.J Agric.Food Chem., 1958, (6): the method for putting down in writing in the 39-41 document is measured.
Particularly, the vigour-testing method of peroxidase residual enzyme can carry out as follows: accurately weighing 8g sample is placed in the conical flask of 250mL, then adds sodium hydrogen phosphate-citric acid solution of 250mL pH 6.5.Sample is placed in after the thermostat vibration 30min of 28 ℃ to the Centrifuge Cup of transferring to 250mL, the centrifugal 10min of 3000r/min.Get supernatant 10mL, be diluted to cushioning liquid in the volumetric flask of 250mL, then the aliquot sample of drawing 25mL is in small beaker, another part of 25mL sample is as blank.Add the o-phenylenediamine solution (every 4h upgrades once and is dissolved in 95% ethanol) of following reagent: 1mL 1% and the hydroperoxidation liquid of 1mL 0.3% for sample, add fast the saturated solution of sodium bisulfite cessation reaction of 2mL after reacting 5min.Add o-phenylenediamine solution and the saturated solution of sodium bisulfite of 2mL of 1mL 1% in blank, then add immediately the hydroperoxidation liquid of 1mL 0.3%.The light absorption value of working sample under 430nm.The vigor computing formula of peroxidase:
The vigor of peroxidase=(A/B) * (250/10) * (250/25)
In formula: A---light absorption value
B---sample dry weight (g)
The vigor of peroxidase residual enzyme (%)=(after adopting the inventive method to process, the vigor of sample peroxidase/employing the inventive method is processed the vigor of front sample peroxidase) * 100%
Especially, harmful worm's ovum is such as can be according to Zhu Bangxiong etc., in rice the generation of sitophilus zea-mais with control research, foodstuff preservation, in 2009 (5), 12～16 document, record method is measured:
Particularly, the assay method of harmful worm's ovum is as follows: get the raw material rice bran with stable after each 1.0kg of rice bran, in 30 ℃ ± 1 ℃ of temperature, relative humidity 82%～86%, raise 47 days, every 2 days sieve rice brans 1 time, check new emergence adult and by its timely removing.It is 2.5mm, the 1.5mm of lower floor that insect jigs the aperture, upper strata, and during the sieve worm, the convolution time is not less than 3min.After sieve, in conjunction with hand, pick up and separate insect and rice bran, analysis of accounts.
As a second aspect of the present invention, the present invention relates to the method for a kind of suitability for industrialized production full cream stable bran powder of the present invention, described method be take fresh rice bran as raw material, comprises cleaning screening, modified, extruding, dries and pulverize five steps.
Particularly, method of the present invention comprises the steps:
(1) cleaning screening: the fresh rice bran of output in the rice process of take is raw material, and described fresh rice bran clear up to screening, removes the impurity in described fresh rice bran, obtains clearing up the rice bran after screening;
(2) modified: as the rice bran after the described cleaning of step (1) screening to be mixed with water, then pass into water vapour and make the starch part gelatinization in rice bran, obtain the rice bran after modified;
(3) extruding: the described rice bran after modified of step (2) is pushed to the rice bran after the preparation extruding;
(4) dry: the rice bran after the extruding that step (3) is obtained, through microwave drying, obtains dried rice bran;
(5) pulverize: the dried rice bran that step (4) is obtained, through pulverizing, obtains full cream stable bran powder.
Wherein, in step (2), except thering is modified effect, also have the effect that makes the pre-gelatinization of starch concurrently.
In step (3), due to squeezing action, make the protein denaturation in rice bran, fibrous fracture, Soluble Fiber content increases, and generally can reach 10～20wt%; Simultaneously, by the lipase in rice bran and peroxide enzymatic inactivation, with effects such as certain sterilization, deinsectization ovum.
Wherein, in step (4), the rice bran after the extruding that step (3) is obtained, through microwave drying, further reduces moisture, when moisture is significantly descended, make the effects such as the vigor passivation of stable on heating peroxidase and further sterilizing, deinsectization ovum.
More specifically, in method of the present invention, described step (2) is carried out as follows: in the rice bran after the described cleaning screening first obtained in step (1), the water that adds the rice bran weight 10～30% after described screening, fully mix, moisture is evenly distributed in rice bran, pass into again water vapour, material is directly contacted with steam, further regulate the moisture of material, regulate the temperature of material simultaneously, this process is a continuous process, it is so-called modified process, refining temperature is controlled at 50～100 ℃, 1～40 minute modified time, 6～60 rev/mins of modifying device rotating speeds, obtain the rice bran after modified.
Described step (3) is carried out under the following conditions: adopt double screw extruder to carry out described extrusion step, the screw slenderness ratio of described double screw extruder (L/D) is (18～52): 1,5～500 rev/mins of screw speeds, be divided into a plurality of districts in extruder, be preferably 5～13Ge districts, each district's temperature does not wait, 50～180 ℃ of its scopes; Each district's pressure does not wait, its scope-0.06～40MPa, the rice bran after being pushed.
Rice bran after above-mentioned extruding, moisture is between 16～40wt%, and starch burn degree is between 30～90%.
Described step (4) is carried out under the following conditions: adopt microwave drying to dewater in the rice bran after extruding, microwave power is 10～60kW, and microwave frequency is 2450 ± 25MHz, and microwave heating time is 0.6～20 minute, and microwave heating temperature is 50～100 ℃.
The granularity of the full cream stable bran powder after described step (5) is pulverized is 100～500 orders.
Preferably, the method for suitability for industrialized production full cream stable bran powder of the present invention comprises the steps:
(1) cleaning screening: the foreign material such as the assorted powder of the chaff in rice bran, rice crushed rices, rice husk chip are separated, guarantee in rice bran that the impurity such as the assorted powder of the chaff that causes easy moldy metamorphism and affect the rice bran quality, rice crushed rices, rice husk separate with raw rice bran, make to be less than 2wt% containing the crushed rices rate in rice bran, can't check the rice husk chip, obtain the rice bran after cleaning is screened.
(2) it is modified: during the garbled raw rice bran of cleaning obtained in step (1) is transported to modifying device, in modified step, material is continuously stirred, mix and push ahead equably, then, the water that adds again 10～30wt% of described garbled rice bran weight, fully mix, moisture is evenly distributed in rice bran, adding water vapour directly contacts with rice bran again, make refining temperature (, the temperature of rice bran after steam directly heats) be controlled at 50～100 ℃, the modified time is 1～30 minute, the modifying device rotating speed is 15～60 rev/mins, obtain the rice bran after modified.
By modified step, can make the rice bran after cleaning screening complete the modified and pre-gelatinization of starch simultaneously, starch burn degree reaches 30～60%, obtains the rice bran after modified.
(3) extruding: step (2) is obtained modified after rice bran, adopt double screw extruder to be extruded, the condition of described double screw extruder is as follows: screw slenderness ratio (L/D) is (25～45): 1,180～500 rev/mins of screw speeds, 50～180 ℃ of extruder Nei Ge district temperature, each district's pressure is-0.06～25MPa, the rice bran after being pushed.
Rice bran after extruding, moisture is between 18～30wt%, and starch burn degree is between 30～90%.
(4) dry: the rice bran after the extruding that step (3) is obtained, adopt the microwave continuous drier drying to dewater, obtain dried rice bran.The condition of baking step is as follows: microwave power is 10～60kW, and microwave frequency is 2450 ± 25MHz, and microwave heating time is 1～18 minute, and microwave heating temperature is 50～100 ℃.
After baking step is processed, the moisture of rice bran is down to below 10%.
(5) pulverize: adopt impact grinding, the dried bran powder of step (4) gained is broken to 100～400 order granularities, obtain full cream stable bran powder.
More preferably, the method that the present invention prepares full cream stable bran powder comprises the following steps:
(1) cleaning screening: the foreign material such as the assorted powder of the chaff in rice bran, rice crushed rices, rice husk chip are separated, guarantee in rice bran that the impurity such as the assorted powder of the chaff that causes easy moldy metamorphism and affect the rice bran quality, rice crushed rices, rice husk separate with raw rice bran, make to be less than 1wt% containing the crushed rices rate in rice bran, can't check the rice husk chip, obtain the fresh rice bran after cleaning is screened.
(2) modified: the rice bran after the cleaning screening first step (1) obtained is transported in modifying device, the water that adds again 10～30wt% of the rice bran weight after described screening, fully mix, moisture is evenly distributed in rice bran, pass into again water vapour rice bran is directly contacted with steam, make refining temperature be controlled at 60～80 ℃, 2～20 minutes modified time, the modifying device rotating speed is 18～30 rev/mins, obtains the rice bran after modified.
By modified process, can make rice bran complete the modified and pre-gelatinization of starch in modifying device, starch burn degree reaches 40～50%, obtains the rice bran after modified.
(3) extruding: step (2) is obtained modified after rice bran, adopt double screw extruder to carry out described extrusion step, the condition of described double screw extruder is as follows: screw slenderness ratio (L/D) is (30～40): 1, screw speed is 240～400 rev/mins, 60～160 ℃ of extruder Nei Ge district temperature, each district's pressure-0.06～10MPa, obtain pushing rear rice bran.
Rice bran after extruding, moisture is between 18～30wt%, and starch burn degree is between 30～90%.
(4) dry: the rice bran after the extruding that step (3) is obtained, adopt the microwave continuous drier drying to dewater, obtain dried rice bran.The condition of baking step is as follows: microwave power is 30～60kW, and microwave frequency used is 2450 ± 25MHz, and microwave heating time is between 2～16 minutes, and microwave heating temperature is between 50～100 ℃.
After baking step is processed, the moisture of rice bran is down to below 10%.
(5) pulverize: adopt impact grinding, the dried bran powder of step (4) gained is broken to 150～200 order granularities, obtain full cream stable bran powder.
In addition, in described step (2), with respect to the rice bran weight after modified, further can add the cellulase of 1～5wt%, prepare the full cream stable bran powder that Soluble Fiber content reaches 15～20wt%.
Wherein, described cellulase can be complex cellulase.Particularly, described cellulase can comprise circumscribed 1,4 beta-glucanase, Endo-β-glucanase, beta-glucosidase or their any combination etc.; More preferably, described cellulase is zytase or zytase and the combination that is selected from one or more enzymes in circumscribed 1,4 beta-glucanase, Endo-β-glucanase, beta-glucosidase.
As a third aspect of the present invention, the present invention relates to the equipment of a kind of suitability for industrialized production full cream stable bran powder of the present invention, described equipment comprises cleaning screening plant, modifying device, pressurizing unit, drying unit and reducing mechanism.
More specifically, the equipment of suitability for industrialized production full cream stable bran powder of the present invention comprises:
(1) cleaning screening plant: described cleaning screening plant can be selected any device that can make the rice material chaff can access fine cleaning effect.
For example, can adopt traditional vibratory sieve as the cleaning screening plant.The cleaning sieve of cleaning screening plant is by forming at the bottom of upper and lower two layer screen, for example, according to the size of sieve number at the bottom of situation adjustment (, increase or the reduce) two layer screen of raw material rice bran simultaneously.At the bottom of upper sieve, the order number of screen cloth is less than the order number of screen cloth at the bottom of lower screen, and for example, at the bottom of upper sieve, the order number of screen cloth is 20～40 orders, and at the bottom of lower screen, the order number of screen cloth is 40～60 orders, but is not limited to this.
(2) modifying device: described modifying device be single shaft adjustable with the footpath rotating speed, with the quality-adjusting device of paddle formula, material is from entering the quality-adjusting device entrance to leaving the quality-adjusting device outlet, process adds water-wet, water vapour directly heats, and remains good stirring and the even processes such as conveying without dead angle.The temperature of modifying device is controlled at 50～100 ℃, and the modified time is 1～40 minute, and the modifying device rotating speed is 6～60 rev/mins;
Preferably, the temperature of modifying device is controlled at 15～60 rev/mins of 50～100 ℃, the rotating speed of 1～30 minute modified time, modifying device;
More preferably, the temperature of modifying device is controlled at 18～30 rev/mins of 60～80 ℃, the rotating speed of 2～20 minutes modified time, modifying device.
In modifying device, the degree of filling of material can be adjusted between 40～60%.
In the present invention, the effect of modifying device, except modified, also has the effect of the pre-gelatinization of starch concurrently.
(3) pressurizing unit: described pressurizing unit adopts twin (double) screw extruder, is preferably the full engagement type twin (double) screw extruder of rotating Vortex.
The parameter of described twin (double) screw extruder is as follows: described screw slenderness ratio (L/D) is (18～52): 1, and 5～500 rev/mins of screw speeds, be divided into a plurality of districts in extruder, be preferably 5～13Ge districts; Each district's temperature does not wait, 50～180 ℃ of its scopes; Each district's pressure does not wait, its scope-0.06～40MPa;
Preferably, described screw slenderness ratio (L/D) is (25～45): 1, and 180～500 rev/mins of screw speeds, temperature 50～180 ℃，Ge district pressure in extruder Nei Ge district are-0.06～25MPa;
More preferably, screw slenderness ratio (L/D) is (30～40): 1, and 240～400 rev/mins of screw speeds, the pressure in temperature 60～160 ℃，Ge districts, extruder Nei Ge district is between-0.06～10MPa.
(4) drying unit: described drying unit is microwave dryer, and microwave power used is 10～60kW, is preferably 30～60kW; Microwave frequency used is 2450 ± 25MHz; Microwave heating time is 0.6～20 minute, is preferably 1～18 minute, more preferably 2～16 minutes; Microwave heating temperature is between 50～100 ℃.
(5) reducing mechanism: described reducing mechanism is the impact grinding pulverizer, and the obtainable granularity of pulverising mill is 100～500 orders, is preferably 100～400 orders, more preferably 150～200 orders.
Embodiment
Below by the specific embodiment, further illustrate the present invention, be understandable that, the specific embodiment of the present invention can not form any restriction to protection domain of the present invention.
The production of the full cream stable bran powder that embodiment 1 Soluble Fiber content is low
Can obtain by following steps the full cream stable bran powder that Soluble Fiber content is low:
(1) straight ensuing fresh rice bran on paddy machining production line husk rice operation, directly be transported to full-cream rice bran and stablize job shop.Conveying capacity with 200kg/h enters the cleaning screening machine continuously, and the cleaning sieve of cleaning screening machine is by forming at the bottom of upper and lower two layer screen, and the sieve number at the bottom of upper sieve is 20 orders, and the sieve number at the bottom of lower screen is 40 orders.When the two-layer screen of rice bran process, at first the impurity that rice husk chip etc. are large lived by filter at the bottom of upper sieve, rice bran and tiny impurity bleed at the bottom of lower screen, while carrying out screen at the bottom of the process lower screen again, rice bran is filtered, and tiny impurity leaks down, the impurity such as the assorted powder of the chaff in the removal rice bran, rice crushed rices, rice husk chip, make to be less than 1.5wt% containing the crushed rices rate in rice bran, rice husk chip≤0.05wt%, obtain the raw material rice bran 180kg/h after cleaning is screened.
(2) rice bran after step (1) screening is fed in quality-adjusting device continuously to the XDHS400 quality-adjusting device that the quality-adjusting device of use is produced for Harbin modern dairy industry machinery Co., Ltd.Then, the water that adds again the rear rice bran weight 10% of screening, fully mix, passing into water vapour directly contacts with rice bran again, make refining temperature (being the temperature of rice bran after steam directly heats) be controlled at 65 ℃, the modified time is 10 minutes, and the quality-adjusting device rotating speed is 20 rev/mins, makes the pre-gelatinization degree of starch in rice bran reach 55%.
(3) step (2) is obtained modified after rice bran in twin (double) screw extruder (model: THJ-52, manufacturer: machinery Co., Ltd of the sincere alliance in Nanjing), complete extruding, stabilization processes.Screw slenderness ratio (L/D) is 52: 1, screw speed is 320 rev/mins, district's temperature 60 C, two district's temperature 65 ℃, tri-district's temperature 70 Cs, 100 ℃ of 120 ℃ of ,Shi of four district's temperature 90 ℃, five district's temperature 105 ℃, six district's temperature 120 ℃, seven district's temperature 135 ℃, eight district's temperature 145 ℃, nine district's temperature 155 ℃, ten district's temperature, mono-district's temperature, 95 ℃ of 100 ℃ of ,Shi of No.12 District temperature, tri-district's temperature in extruder; The pressure be subject in material Zai Ge district is: San Zhi 9th district, and pressure is by the promotion of normal pressure to 7MPa, and ten Zhi Shi mono-district pressure releases, to normal pressure, then are inhaled vacuum to-0.05MPa, obtain the rice bran after extrusion stability.
(4) adopt microwave continuous drier to remove the excessive moisture of the rear rice bran of extruding, microwave power is 60kW, and microwave frequency is 2450MHz, and microwave heating time is 5 minutes, and microwave heating temperature is 90 ℃, and after processing, the moisture of product is down to below 10wt%.
(5) adopt Type Impact Superfine Mill (model: LHJ/Y, manufacturer: Weifang powder technology equipment just far away Co., Ltd), be granular rice bran after pushing and pulverize, obtain the full cream stable bran powder product that Soluble Fiber content is low, product granularity can reach 100 orders.
Then, adopt the described method of GB 5009.5-2010 to measure the protein content of prepared full cream stable bran powder product; Adopt the described method of GB/T 5009.3-2010 to measure the moisture of prepared full cream stable bran powder product; Adopt the described method of GB/T5009.9-2008 to measure the content of starch of prepared full cream stable bran powder product; Adopt the described method of GB/T 5009.6-2003 measure prepared full cream stable bran powder product fat content; Adopt the described method of GB/T5413.5-1997 to measure the total sugar content of prepared full cream stable bran powder product; Adopt the described method of GB/T5009.4-2010 to measure the content of ashes of prepared full cream stable bran powder product; Adopt the described method of GB/T 15684-1995 to measure the free fatty acid content of prepared full cream stable bran powder product; Adopt the described method of GB/T5009.88-2008 to measure the Soluble Fiber content of prepared full cream stable bran powder product.
In addition, the assay method of vigor, total plate count and the bacillus cereus of peroxidase is not particularly limited, as long as can measure reliably These parameters.
Total plate count for example can be carried out according to the described method of GB/T4789.2-2010; Bacillus cereus for example can carry out according to the described method of GB/T4789.14-2003.
Especially, the vigor of peroxidase residual enzyme can be according to VETTER J L, STEINBERG M P.Qualitative determination of peroxidase in sweet corn.J Agric.Food Chem., 1958, (6): the method for putting down in writing in the 39-41 document is measured.
Particularly, the vigour-testing method of peroxidase residual enzyme can carry out as follows: accurately weighing 8g sample is placed in the conical flask of 250mL, then adds sodium hydrogen phosphate-citric acid solution of 250mL pH 6.5.Sample is placed in after the thermostat vibration 30min of 28 ℃ to the Centrifuge Cup of transferring to 250mL, the centrifugal 10min of 3000r/min.Get supernatant 10mL, be diluted to cushioning liquid in the volumetric flask of 250mL, then the aliquot sample of drawing 25mL is in small beaker, another part of 25mL sample is as blank.Add the o-phenylenediamine solution (every 4h upgrades once and is dissolved in 95% ethanol) of following reagent: 1mL 1% and the hydroperoxidation liquid of 1mL 0.3% for sample, add fast the saturated solution of sodium bisulfite cessation reaction of 2mL after reacting 5min.Add o-phenylenediamine solution and the saturated solution of sodium bisulfite of 2mL of 1mL 1% in blank, then add immediately the hydroperoxidation liquid of 1mL 0.3%.The light absorption value of working sample under 430nm.The vigor computing formula of peroxidase:
The vigor of peroxidase=(A/B) * (250/10) * (250/25)
In formula: A---light absorption value
B---sample dry weight (g)
The vigor of peroxidase residual enzyme (%)=(after adopting the inventive method to process, the vigor of sample peroxidase/employing the inventive method is processed the vigor of front sample peroxidase) * 100%
Especially, harmful worm's ovum is such as can be according to Zhu Bangxiong etc., in rice the generation of sitophilus zea-mais with control research, foodstuff preservation, in 2009 (5), 12～16 document, record method is measured:
Particularly, the assay method of harmful worm's ovum is as follows: get the raw material rice bran with stable after each 1.0kg of rice bran, in 30 ℃ ± 1 ℃ of temperature, relative humidity 82%～86%, raise 47 days, every 2 days sieve rice brans 1 time, check new emergence adult and by its timely removing.It is 2.5mm, the 1.5mm of lower floor that insect jigs the aperture, upper strata, and during the sieve worm, the convolution time is not less than 3min.After sieve, in conjunction with hand, pick up and separate insect and rice bran, analysis of accounts.
The indices of the full cream stable bran powder that gained Soluble Fiber content is low is as follows:
1, outward appearance: buff powder, there is strong roasted nuts fragrance.
2, granularity: 100 orders.
3, other quality index: in the full cream stable bran powder of the present embodiment, by weight percentage, protein 10～14wt%, moisture is less than 10wt%, starch 20～25wt%, fat 15～20wt%, total reducing sugar 5～8wt%, ash content is less than 8wt%, and free fatty acid level is less than 10wt%, and Soluble Fiber content is at 10～15wt%.The content of above composition can slightly change along with the difference of rice variety, the place of production and processing technology.
If 4 are considered as 100% by the vigor of peroxidase in fresh rice bran, the vigor of the residual peroxide enzyme of the full cream stable bran powder that this embodiment obtains is less than 4%.
5, harmful worm's ovum and microbiological indicator: total plate count is less than 1000CFU/g, does not detect bacillus cereus and harmful worm's ovum.
6,, under normal temperature, the storage life is 12 months.
The production of the full cream stable bran powder that embodiment 2 Soluble Fiber content are high
Can obtain by following steps the full cream stable bran powder that Soluble Fiber content is high:
(1) straight ensuing fresh rice bran on paddy machining production line husk rice operation, directly be transported to full-cream rice bran and stablize job shop.Conveying capacity with 200kg/h enters the cleaning screening machine continuously, and the cleaning sieve of cleaning screening machine is by forming at the bottom of upper and lower two layer screen, and the sieve number at the bottom of upper sieve is 20 orders, and the sieve number at the bottom of lower screen is 40 orders.When the two-layer screen of rice bran process, at first the impurity that rice husk chip etc. are large lived by filter at the bottom of upper sieve, rice bran and tiny impurity bleed at the bottom of lower screen, while carrying out screen at the bottom of the process lower screen again, rice bran is filtered, and tiny impurity leaks down, the impurity such as the assorted powder of the chaff in the removal rice bran, rice crushed rices, rice husk chip, make to be less than 1.5wt% containing the crushed rices rate in rice bran, rice husk chip≤0.05wt%, obtain the raw material rice bran 180kg/h after cleaning is screened.
(2) rice bran after step (1) screening is fed in quality-adjusting device continuously to the XDHS400 quality-adjusting device that the quality-adjusting device of use is produced for Harbin modern dairy industry machinery Co., Ltd.Then, then add the water that screens rear rice bran weight 15%, fully mix, simultaneously, with respect to the rice bran weight after screening, cellulase (the plant composite hydrolytic enzyme of interpolation 5wt%
L, 100FBG/g, letter (China) Investment Co., Ltd of Novi), passing into water vapour directly contacts with rice bran again, make refining temperature (being the temperature of rice bran after steam directly heats) be controlled at 65 ℃, the modified time is 40 minutes, and the quality-adjusting device rotating speed is 15 rev/mins, makes the pre-gelatinization degree of starch in rice bran reach 60%.
(3) step (2) is obtained modified after rice bran in twin (double) screw extruder (model: THJ-52, manufacturer: Nanjing machinery Co., Ltd of sincere alliance), complete extruding, stabilization processes, screw slenderness ratio (L/D) is 52: 1, screw speed is 420 rev/mins, in extruder, district's temperature is 65 ℃, two 65 ℃ of district's temperature, three 65 ℃ of district's temperature, four 65 ℃ of district's temperature, five 75 ℃ of district's temperature, six 95 ℃ of district's temperature, seven 115 ℃ of district's temperature, eight 135 ℃ of district's temperature, nine 145 ℃ of district's temperature, ten 155 ℃ of district's temperature, 11 110 ℃ of district's temperature, 100 ℃ of No.12 District temperature, 13 100 ℃ of district's temperature.The pressure be subject in material Zai Ge district is: district's pressure is normal pressure; Er Zhi 6th district, pressure rises to 10MPa by normal pressure; Qi Zhi tenth district, pressure remains on 10MPa; 11st district, pressure is-0.05MPa; 12 Zhi Shi 3rd district, pressure is normal pressure, obtains afterwards the rice bran after extrusion stability.
(4) adopt microwave continuous drier to remove the excessive moisture of the rice bran after pushing, microwave power is 60kW, and microwave frequency is 2450MHz, and microwave heating time is 8 minutes, and microwave heating temperature is 90 ℃, and after processing, the moisture of product is down to below 10wt%.
(5) adopt Type Impact Superfine Mill (model: LHJ/Y, manufacturer: Weifang powder technology equipment just far away Co., Ltd), be granular rice bran after pushing and pulverize, obtain the full cream stable bran powder product that Soluble Fiber content is low, product granularity reaches 200 orders.
The measuring method of indices is identical with embodiment 1.
The full cream stable bran powder that gained Soluble Fiber content is high, its indices is as follows:
1, outward appearance: buff powder, there is strong roasted nuts fragrance.
2, granularity: 200 orders.
3, other quality index: in the full cream stable bran powder of the present embodiment, by weight percentage, protein 10～14wt%, moisture is less than 10wt%, starch 20～25wt%, fat 15～20wt%, total reducing sugar 5～8wt%, ash content is less than 8wt%, and free fatty acid level is less than 10wt%, and Soluble Fiber content is at 15～20wt%.The content of above composition can slightly change along with the difference of rice variety, the place of production and processing technology.
If 4 are considered as 100% by the vigor of peroxidase in fresh rice bran, the vigor of the residual peroxide enzyme of the full cream stable bran powder that this embodiment obtains is less than 4%.
5, harmful worm's ovum and microbiological indicator: total plate count is less than 1000CFU/g, does not detect bacillus cereus and harmful worm's ovum.
6,, under normal temperature, the storage life is 12 months.
The production of the full cream stable bran powder that embodiment 3 Soluble Fiber content are high
Can obtain by following steps the full cream stable bran powder that Soluble Fiber content is high:
(1) straight ensuing fresh rice bran on paddy machining production line husk rice operation, directly be transported to full-cream rice bran and stablize job shop.Conveying capacity with 200kg/h enters the cleaning screening machine continuously, and the cleaning sieve of cleaning screening machine is by forming at the bottom of upper and lower two layer screen, and at the bottom of upper sieve, the order number of screen cloth is 20 orders, and at the bottom of lower screen, the order number of screen cloth is 40 orders.When the two-layer screen of rice bran process, at first the impurity that rice husk chip etc. are large lived by filter at the bottom of upper sieve, rice bran and tiny impurity bleed at the bottom of lower screen, while carrying out screen at the bottom of the process lower screen again, rice bran is filtered, and tiny impurity leaks down, the impurity such as the assorted powder of the chaff in the removal rice bran, rice crushed rices, rice husk chip, make to be less than 1.5wt% containing the crushed rices rate in rice bran, rice husk chip≤0.05wt%, obtain the raw material rice bran (180kg/h) after cleaning is screened.
(2) rice bran after step (1) screening is fed in quality-adjusting device continuously to the XDHS400 quality-adjusting device that the quality-adjusting device of use is produced for Harbin modern dairy industry machinery Co., Ltd.Then, then add the water that screens rear rice bran weight 15%, fully mix, simultaneously, with respect to the rice bran weight after screening, cellulase (the plant composite hydrolytic enzyme of interpolation 5wt%
L, 100FBG/g, letter (China) Investment Co., Ltd of Novi), passing into water vapour directly contacts with rice bran again, make refining temperature (being the temperature of rice bran after steam directly heats) be controlled at 65 ℃, the modified time is 40 minutes, and the quality-adjusting device rotating speed is 15 rev/mins, makes the pre-gelatinization degree of starch in rice bran reach 60%.
(3) step (2) is obtained modified after rice bran in twin (double) screw extruder (model: THJ-52, manufacturer: Nanjing machinery Co., Ltd of sincere alliance), complete extruding, stabilization processes, screw slenderness ratio (L/D) is 52: 1, screw speed is 420 rev/mins, in extruder, district's temperature is 65 ℃, two 65 ℃ of district's temperature, three 65 ℃ of district's temperature, four 65 ℃ of district's temperature, five 75 ℃ of district's temperature, six 95 ℃ of district's temperature, seven 115 ℃ of district's temperature, eight 135 ℃ of district's temperature, nine 145 ℃ of district's temperature, ten 155 ℃ of district's temperature, 11 110 ℃ of district's temperature, 100 ℃ of No.12 District temperature, 13 100 ℃ of district's temperature.The pressure be subject in material Zai Ge district is: district's pressure is normal pressure; Er Zhi 5th district, pressure rises to 40MPa by normal pressure; Liu Zhi seven district's pressure are down to 20MPa again; Ba Zhi is down to 7MPa in 9th district again; Tenth district are down to normal pressure ，Shi mono-district's pressure again; 12 Zhi Shi 3rd district, pressure is normal pressure, obtains afterwards the rice bran after extrusion stability.
(4) adopt microwave continuous drier to remove the excessive moisture of the rice bran after pushing, microwave power is 60kW, and microwave frequency is 2450MHz, and microwave heating time is 8 minutes, and microwave heating temperature is 90 ℃, and after processing, the moisture of product is down to below 10wt%.
(5) adopt Type Impact Superfine Mill (model: LHJ/Y, Weifang powder technology equipment just far away Co., Ltd produces), be granular rice bran after pushing and pulverize, obtain the full cream stable bran powder product that Soluble Fiber content is low, product granularity reaches 200 orders.
The measuring method of indices is identical with embodiment 1.
The full cream stable bran powder that gained Soluble Fiber content is high, its indices is as follows:
1, outward appearance: buff powder, there is strong roasted nuts fragrance.
2, granularity: 200 orders.
3, other quality index: in the full cream stable bran powder of the present embodiment, by weight percentage, protein 10～14wt%, moisture is less than 10wt%, starch 20～25wt%, fat 15～20wt%, total reducing sugar 5～8wt%, ash content is less than 8wt%, and free fatty acid level is less than 10wt%, and Soluble Fiber content is at 15～20wt%.The content of above composition can slightly change along with the difference of rice variety, the place of production and processing technology.
If 4 are considered as 100% by the vigor of peroxidase in fresh rice bran, the vigor of the residual peroxide enzyme of the full cream stable bran powder that this embodiment obtains is less than 4%.
5, harmful worm's ovum and microbiological indicator: total plate count is less than 1000CFU/g, does not detect bacillus cereus and harmful worm's ovum.
6,, under normal temperature, the storage life is 12 months.
Described now embodiment of the present invention in detail, clearly can do a lot of improvement and variation for a person skilled in the art and can not deviate from essence spirit of the present invention.All these changes and improvements are all within protection scope of the present invention.
The accompanying drawing explanation
The flow diagram of a kind of embodiment of Fig. 1 full cream stable bran powder production technology.
Claims (8)
1. the method for a suitability for industrialized production full cream stable bran powder, described method be take fresh rice bran as raw material, comprises cleaning screening, modified, extruding, dries and pulverize five steps:
(1) cleaning screening: the fresh rice bran of output in the rice process of take is raw material, and described fresh rice bran clear up to screening, removes the impurity in described fresh rice bran, obtains clearing up the rice bran after screening;
(2) modified: as the rice bran after the described cleaning of step (1) screening to be mixed with water, then pass into water vapour and make the starch part gelatinization in rice bran, obtain the rice bran after modified;
(3) extruding: the described rice bran after modified of step (2) is pushed to the rice bran after the preparation extruding;
(4) dry: the rice bran after the extruding that step (3) is obtained, through microwave drying, obtains dried rice bran;
(5) pulverize: the dried rice bran that step (4) is obtained, through pulverizing, obtains full cream stable bran powder.
2. the method for claim 1, wherein
Described step (2) is carried out as follows: in the rice bran after the described cleaning screening first obtained in step (1), the water that adds the rice bran weight 10～30% after described screening, fully mix, moisture is evenly distributed in rice bran, pass into again water vapour, material is directly contacted with steam, make refining temperature be controlled at 50～100 ℃, 1～40 minute modified time, 6～60 rev/mins of modifying device rotating speeds, obtain the rice bran after modified;
Described step (3) is carried out under the following conditions: adopt double screw extruder to carry out described extrusion step, the screw slenderness ratio of described double screw extruder (L/D) is (18～52): 1,5～500 rev/mins of screw speeds, be divided into a plurality of districts in extruder, each district's temperature does not wait, 50～180 ℃ of temperature ranges; Each district's pressure does not wait, pressure limit-0.06～40MPa, the rice bran after being pushed;
Described step (4) is carried out under the following conditions: adopt microwave drying to dewater in the rice bran after extruding, microwave power is 10～60kW, and microwave frequency is 2450 ± 25MHz, and microwave heating time is 0.6～20 minute, and microwave heating temperature is 50～100 ℃.
3. method as claimed in claim 2, wherein, be divided into 5～13Ge districts in described extruder.
4. the method for a suitability for industrialized production full cream stable bran powder, described method comprises the steps:
(1) cleaning screening: the assorted powder of the chaff in rice bran, rice crushed rices, rice husk chip foreign material are separated, guarantee in rice bran that the assorted powder of the chaff that causes easy moldy metamorphism and affect the rice bran quality, rice crushed rices, rice husk impurity separate with raw rice bran, make to be less than 2wt% containing the crushed rices rate in rice bran, can't check the rice husk chip, obtain the rice bran after cleaning is screened;
(2) it is modified: during the garbled raw rice bran of cleaning obtained in step (1) is transported to modifying device, in modified step, material is continuously stirred, mixes and pushes ahead equably, then, the water that adds again 10～30wt% of described garbled rice bran weight, fully mix, moisture is evenly distributed in rice bran, adding water vapour directly contacts with rice bran again, make refining temperature be controlled at 50～100 ℃, the modified time is 1～30 minute, the modifying device rotating speed is 15～60 rev/mins, obtains the rice bran after modified;
(3) extruding: step (2) is obtained modified after rice bran, adopt double screw extruder to be extruded, the condition of described double screw extruder is as follows: screw slenderness ratio (L/D) is (25～45): 1,180～500 rev/mins of screw speeds, 50～180 ℃ of extruder Nei Ge district temperature, each district's pressure is-0.06～25MPa, the rice bran after being pushed;
(4) dry: the rice bran after the extruding that step (3) is obtained, adopt microwave continuous drier to be dried under following drying condition: microwave power is 10～60kW, microwave frequency is 2450 ± 25MHz, and microwave heating time is 1～18 minute, and microwave heating temperature is 50～100 ℃;
(5) pulverize: adopt impact grinding, the dried bran powder of step (4) gained is broken to 100～400 order granularities, obtain full cream stable bran powder.
5. the method for a suitability for industrialized production full cream stable bran powder, described method comprises the steps:
(1) cleaning screening: the assorted powder of the chaff in rice bran, rice crushed rices, rice husk chip foreign material are separated, guarantee in rice bran that the assorted powder of the chaff that causes easy moldy metamorphism and affect the rice bran quality, rice crushed rices, rice husk impurity separate with raw rice bran, make to be less than 1wt% containing the crushed rices rate in rice bran, can't check the rice husk chip, obtain the fresh rice bran after cleaning is screened;
(2) modified: the rice bran after the cleaning screening first step (1) obtained is transported in modifying device, the water that adds again 10～30wt% of the rice bran weight after described screening, fully mix, moisture is evenly distributed in rice bran, pass into again water vapour rice bran is directly contacted with steam, make refining temperature be controlled at 60～80 ℃, 2～20 minutes modified time, the modifying device rotating speed is 18～30 rev/mins, obtains the rice bran after modified;
(3) extruding: step (2) is obtained modified after rice bran, adopt double screw extruder to carry out described extrusion step, the condition of described double screw extruder is as follows: screw slenderness ratio (L/D) is (30～40): 1, screw speed is 240～400 rev/mins, 60～160 ℃ of extruder Nei Ge district temperature, each district's pressure-0.06～10MPa, obtain pushing rear rice bran;
(4) dry: the rice bran after the extruding that step (3) is obtained, adopt microwave continuous drier to be dried under following drying condition: microwave power is 30～60kW, microwave frequency used is 2450 ± 25MHz, microwave heating time is between 2～16 minutes, and microwave heating temperature is between 50～100 ℃;
(5) pulverize: adopt impact grinding, the dried bran powder of step (4) gained is broken to 150～200 order granularities, obtain full cream stable bran powder.
6. method as described as claim 1～5 any one, wherein, in described step (2), with respect to the rice bran weight after modified, further add the cellulase of 1～5wt%.
7. method as claimed in claim 6, wherein, described cellulase is circumscribed 1,4 beta-glucanase, Endo-β-glucanase, beta-glucosidase or their any combination.
8. method as claimed in claim 6, wherein, described cellulase is zytase, or described cellulase is zytase and the combination that is selected from one or more enzymes in circumscribed 1,4 beta-glucanase, Endo-β-glucanase, beta-glucosidase.
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| CN201210007481XA CN102524657B (en) | 2012-01-11 | 2012-01-11 | Production method of full cream stable bran powder |
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| CN201210007481XA CN102524657B (en) | 2012-01-11 | 2012-01-11 | Production method of full cream stable bran powder |
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| CN203768327U (en) * | 2013-07-24 | 2014-08-13 | 郑州远洋油脂工程技术有限公司 | Fresh rice bran pretreatment device |
| CN104304444A (en) * | 2014-10-28 | 2015-01-28 | 武汉轻工大学 | Method for continuously stabilizing rice bran by adopting tunnel-type microwave |
| CN104939266B (en) * | 2015-05-11 | 2018-04-17 | 西南大学 | A kind of rice bran enzyme deactivation stabilization treatment method |
| CN110447821A (en) * | 2019-09-05 | 2019-11-15 | 沈阳师范大学 | A kind of stable state full fat rice bran nutrient buccal tablet and its processing method |
| CN110495612A (en) * | 2019-09-17 | 2019-11-26 | 广东海洋大学 | A kind of production method of seawater rice chaff cellulose powder |
| CN112535255A (en) * | 2020-12-02 | 2021-03-23 | 吉林省蚕业科学研究院 | Preparation method and application of rice bran powder |
| CN112704183A (en) * | 2020-12-07 | 2021-04-27 | 无锡新禾创工食品科技有限公司 | Preparation method and application of edible full-fat rice bran |
| CN113925113A (en) * | 2021-10-19 | 2022-01-14 | 江苏奥迈生物科技有限公司 | Feed for increasing rice bran consumption of daily ration of bred animals and rice bran treatment method thereof |
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