CN102517642B - Non-pollution production method of bamboo fibers - Google Patents

Non-pollution production method of bamboo fibers Download PDF

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Publication number
CN102517642B
CN102517642B CN201110381221.4A CN201110381221A CN102517642B CN 102517642 B CN102517642 B CN 102517642B CN 201110381221 A CN201110381221 A CN 201110381221A CN 102517642 B CN102517642 B CN 102517642B
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bamboo
fibre
bamboos
boiling
production
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CN102517642A (en
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姚文斌
俞伟鹏
张蔚
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Zhejiang A&F University ZAFU
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Zhejiang A&F University ZAFU
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Abstract

The invention provides a non-pollution production method of bamboo fibers, wherein the method is used for producing coarse bamboo fibers with lengths of 60-120 mm and diameters of 0.18-0.35 mm. the method comprises the steps of: firstly, selecting the raw materials; and then, cutting the bamboos into regulated lengths; splitting or flattening the bamboos; adding a reusable neutral softening solution in the bamboos to stew and soften the bamboos; roasting the softened bamboos on a drying machine; directionally opening fibers from the roasted bamboos; drying the bamboos, opening fibers for the second time, classifying and sorting to obtain bamboo fibers with stable quality. The method of the invention has the advantages of non waste liquid drainage during the production process, simple technique, high production efficiency, reliable product quality, and capability of greatly improving the fiber yield and reducing the production cost, so that the method is an ideal method for producing bamboo fibers.

Description

A kind of method of CR production bamboo fibre
[technical field]
The present invention relates to one bamboo stem stalk is raw material, and pollution-free high-efficient is produced the method for bamboo fibre.
[background technology]
Thick bamboo fibre refers to 8 centimetres of average lengths, the bamboo fiber bundle that diameter is about 0.3 millimeter.Because it has that intensity is high, good rigidly and the outstanding advantage such as hygroscopicity and antibiotic property, be widely used in manufacturing the fields such as automotive interior material plate, mattress and building and ornament materials plate.
From bamboo wood, extract intensive processing and the application that bamboo fibre is bamboo wood and opened up brand-new road, caused the extensive concern of international market.Bamboo fibre raw material sources are in natural reproducible resource, and product is biodegradable after using, and meets environmental requirement, is a kind of new material with bright prospects.
Natural bamboo fibres is called again primary bamboo fibre, and it is the fiber of bamboo being directly processed into by methods such as machinery, physics.In process, according to Technology Need, in definite range scale (fineness, length), keep the fiber bundle structure of bamboo wood, only remove the plant tissue outside fibre bundle.Conventionally, natural bamboo fibres is applied with bundle form, and form approaches fibre of flax for textile material fiber.Natural bamboo fibres cross section has been covered with big and small space, can be at transient absorption transpiring moisture.Due to the special construction of natural bamboo fibres, the height of its cross section " hollow ", expert claims that natural bamboo fibres is " can breathe " fiber.Natural bamboo fibres gloss is beautiful, has unique antibacterial deodourizing performance and good ABRASION RESISTANCE, antibiotic property.Why natural bamboo fibres is subject to the favor of international market, not only because natural bamboo fibres source aithullium and meet the tight demand of people's back to nature the more important thing is that it has the unrivaled advantage of other fiber.
At present, 8 centimetres of average lengths, the bamboo fiber bundle (referred to as thick bamboo fibre) that diameter is about 0.3 millimeter adopts first that bamboo wood is softening more, then by mechanical means, bamboo is processed into fibre morphology, then makes after cleaning, dewater, being dried.Open day is on May 7th, 2003, publication number is the preparation method that the Chinese patent of CN1415790A discloses a kind of bamboo fiber from bamboo, this preparation method by sample prepare, soften, wash, roll, wash, urinate oxygen processing, washing, alkali lye kiering, washing, Urea bleaching, pickling, dewater, shake up, the step order such as airing can make bamboo fibre.Open day is on July 2nd, 2008, and the Chinese patent that publication number is CN101210350A discloses a kind of organic processing technique for bamboo fibre, and the step of this organic processing technique for bamboo fibre is as follows: by selection classification, block respectively; According to tabasheer, surf green by bamboo wood burst; Surf green, tabasheer with sub-wire machine after to boiling carry out respectively sub-wire; Through softening; Rinsing; Bleaching; Putting into industry cleans, dries; Dry; Finally arrange dress bag.Open day is on June 1st, 2005, and number for the Chinese patent of CN1621580A discloses a kind of preparation method of bamboo fiber, the method is first made bamboo fiber crops by former bamboo heating, then by the bamboo fiber crops that obtain be placed in 1#, 2# bating liquor hot digestion is made bamboo fiber.Open day is on September 23rd, 2009, number for the Chinese patent of CN101538744A discloses a kind of production method of bamboo fibre, the method by bamboo wood deliver to bamboo fiber opening seperator realize comb untie finely separate, air-flow classification obtains bamboo filamentary fibers; After kiering, bamboo filamentary fibers is drained, then clean afterwards, dewater, oil, dry; Carry out again obtaining crude bamboo fiber after enzyme processing.
It is softening that these patents have substantially all been used alkali electroless medicine to carry out bamboo wood in fiber preparation process, separated bamboo fiber bundle is brought bating liquor into subsequent handling again subsequently, in fiber cleans, chemicals enters cleaning fluid, makes the waste water discharging in process contain a large amount of pollutants and bring severe environmental problem.Obviously, these methods are difficult to meet the production theory requirement of current sustainable environmental protection.Both brought a large amount of pollutants, and made again production cost increase considerably simultaneously.
[summary of the invention]
The technical problem to be solved in the present invention, is to provide a kind of method of CR production bamboo fibre, the method production process non-wastewater discharge, and technique is simple, and prouctiveness is high, and reliable product quality can improve fiber yield greatly, reduces production costs.
The present invention is achieved in that
A method for CR production bamboo fibre, comprises the following steps:
Raw material sorts, and blocks, and cut open or flatten, boiling, bamboo wood orientation is opened fibre, the health that oils, packaging and warehousing; Wherein: described boiling and bamboo wood orientation are opened and between fine step, be also provided with baking procedure, described bamboo wood orientation is opened and finely between health step, is also provided with dry and secondary and opens fibre, classification, screening step with oiling.
Described boiling step is specially: the bamboo wood of cutting open or flattening is delivered in special High Temperature High Pressure digester, added clear water or secondary bating liquor, and bamboo wood is immersed in solution completely, boiling temperature is controlled at 100~130 DEG C, is forced into 2~3kg/cm 2, boiling is after 10 minutes, then adds bating liquor stoste, and bating liquor stoste additional proportion is 1%~5% of clear water or secondary bating liquor, continues boiling 35~50 minutes;
The former formula of liquid of described bating liquor be water, sulfurous acid ammonia, hydrogen sulfate ammonia, carbonic acid ammonia, 30% ammoniacal liquor according to the ratio preparation of mass ratio 100:5:5:5:0.1~3, and the pH value of bating liquor stoste is controlled at PH=6.5~7.5;
Described baking procedure is specially: the bamboo wood after softening is put on drying machine and is toasted, make the weary white in softening bamboo chip surface wrinkling;
Described drying steps is specially: numb shape bamboo fibre is sent into drying machine and be dried;
Described secondary is opened fibre, classification, screening step and is specially: by dried numb shape bamboo fibre deliver to self-control fibre separating machine realize open finely separate, trash separator sifting sort obtains bamboo filamentary fibers and bamboo stalk impurity, wherein bamboo stalk impurity is delivered to assigned address processed with the output belt of setting, and bamboo filamentary fibers recycling flow separator is removed bamboo powder, finally obtain thick bamboo fibre.
Further, the baking temperature of described baking procedure is 50~160 DEG C, and baking time is 5~15 minutes.
Further, the baking temperature of described drying steps is 50~65 DEG C, and be 5~15 minutes drying time, and numb shape bamboo fibre moisture control is 20%~30%.
Tool of the present invention has the following advantages:
In production process, take into full account the difference in same bamboo different parts (bamboo head, bamboo middle part, bamboo taper) performance, gone blue or green in the situation that directly to process through High Temperature High Pressure is softening in de-etiolation not, realized the High-efficient Production of natural bamboo fibres.The bating liquor stoste pH value adopting is neutral, and its softening time is short, and softening efficiency is high, softening process can Precise control, bating liquor stoste adopts the component that contains ammonium ion substantially simultaneously, after bamboo wood boiling is softening, dries, and ammonium ion finally resolves into ammonia volatilization.As everyone knows, ammonium ion can become the fertilizer of plant, is easy to again decompose simultaneously, there is no harm for environment, and therefore this method has realized the non-wastewater discharge of process.
In addition, toasting and be dried is the effective way of bamboo wood physical modification.It can reduce the moisture content that softens bamboo wood to a certain extent, greatly improve the intensity of softening bamboo wood, bamboo wood is had under good viscoelastroplasticity performance under suitable moisture content, obtain and better open fine effect, this process can effectively be avoided out fibrous fracture in fine process, fiber is inhomogeneous even cannot open fibre, and can improve fibre length and fiber yield, guarantees the quality of production of bamboo fibre.
Opening fine scheme by secondary makes the crude fibre form of processing even; fiber percentage of impurity, Dust Capacity are lower, and bamboo fibre is more even, and its production process is reliable; resource utilization is high; environmental pollution is little, and production technology is simple, and prouctiveness is high; constant product quality, reliable; reducing production costs, is the Perfected process of producing bamboo fibre, efficiently solves the efficient large-scale production problem of natural bamboo fibres.
[brief description of the drawings]
The present invention is further illustrated in conjunction with the embodiments with reference to the accompanying drawings.
Fig. 1 is flow chart of the present invention.
[detailed description of the invention]
As described in Figure 1, the method for a kind of CR production bamboo fibre the present invention relates to, comprises the following steps:
Step 1. raw material sorts, and according to the place of production, bamboo classification in age, leaves each batch of bamboo wood in each designation area;
Step 2. is blocked, and bamboo taper, middle part, head is sawed-off according to the length of specifying, and general sawing length can be within the scope of 1-6 meters;
Step 3. is cut open or is flattened, and bamboo wood after blocking adopts and point partly dissects or by 1/4 burst, or directly with flattening machine, bamboo is launched into sheet;
Step 4. boiling, the bamboo wood of cutting open or flattening is delivered in special High Temperature High Pressure digester, add clear water or secondary bating liquor, and bamboo wood is immersed in solution completely, boiling temperature is controlled at 100~130 DEG C, is forced into 2~3kg/cm2, after boiling 10 minutes, add again bating liquor stoste, and bating liquor stoste additional proportion is that 1%~5% of clear water or secondary bating liquor continues boiling 35~50 minutes;
Step 5. is toasted, and the bamboo wood after softening is put on drying machine and is toasted, and baking temperature is 50~160 DEG C, and baking time is 5~15 minutes, makes the weary white in softening bamboo chip surface wrinkling;
Step 6. bamboo wood orientation is opened fibre, baked bamboo wood is sent into continous mode bamboo fiber opening machine and make it under combined deformation effect, realize fiber alignment and separate flattening, stretch, push, reverse, tear etc., finally obtains numb shape bamboo fibre;
Step 7. is dry, numb shape bamboo fibre is sent into drying machine and be dried, and baking temperature is 50~65 DEG C, and be 5~15 minutes drying time, and numb shape bamboo fibre moisture control is 20%~30%;
Step 8. is opened fibre, classification, screening two times, by dried numb shape bamboo fibre deliver to self-control fibre separating machine realize open fine separate, trash separator sifting sort obtains bamboo filamentary fibers and bamboo stalk impurity, wherein bamboo stalk impurity is delivered to assigned address processed with the output belt of setting, and bamboo filamentary fibers recycling flow separator is removed bamboo powder, finally obtain thick bamboo fibre;
Step 9. health that oils, thread bamboo thick bamboo fibre is delivered to health preserving room by conveyer, sprays appropriate health finish, 3-10 days summers of conditioned time, winter 7-15 days;
Step 10. packaging and warehousing, by moisture content and the specification packaging and warehousing as requested of the thick bamboo fibre after health.
Preferably, the former formula of liquid of described bating liquor be water, sulfurous acid ammonia, hydrogen sulfate ammonia, carbonic acid ammonia, 30% ammoniacal liquor according to the ratio preparation of mass ratio 100:5:5:5:0.1~3, and the pH value of bating liquor stoste is controlled at PH=6.5~7.5.
The present invention be directed in prior art and produce bamboo fibre high pollution, work efficiency is low, of poor quality, simultaneously be difficult to again to meet suitability for industrialized production needs and wait the problem of existence, provide a kind of produce diameter at 0.18 millimeter to 0.35 millimeter, length High-efficient Production technology and the technique at the bamboo fiber of 60~120 millimeters.
Method of the present invention has taken into full account the difference in same bamboo different parts (bamboo head, bamboo middle part, bamboo taper) performance in process of production, go blue or green in the situation that directly to process through High Temperature High Pressure is softening in de-etiolation not, realized the High-efficient Production of natural bamboo fibres.The bating liquor stoste pH value adopting is neutral, and its softening time is short, and softening efficiency is high, softening process can Precise control, bating liquor stoste adopts the component that contains ammonium ion substantially simultaneously, after bamboo wood boiling is softening, dries, and ammonium ion finally resolves into ammonia volatilization.As everyone knows, ammonium ion can become the fertilizer of plant, is easy to again decompose simultaneously, there is no harm for environment, and therefore this method has realized the non-wastewater discharge of process.
In addition, toasting and be dried is the effective way of bamboo wood physical modification.It can reduce the moisture content that softens bamboo wood to a certain extent, greatly improve the intensity of softening bamboo wood, bamboo wood is had under good viscoelastroplasticity performance under suitable moisture content, obtain and better open fine effect, this process can effectively be avoided out fibrous fracture in fine process, fiber is inhomogeneous even cannot open fibre, and can improve fibre length and fiber yield, guarantees the quality of production of bamboo fibre.
Opening fine scheme by secondary makes the crude fibre form of processing even; fiber percentage of impurity, Dust Capacity are lower, and bamboo fibre is more even, and its production process is reliable; resource utilization is high; environmental pollution is little, and production technology is simple, and prouctiveness is high; constant product quality, reliable; reducing production costs, is the Perfected process of producing bamboo fibre, efficiently solves the efficient large-scale production problem of natural bamboo fibres.
In a word, the thick bamboo fibre of being produced by the present invention has that long fineness is even, intensity is high, good rigidly, fiber absorb-discharge humid, gas permeability are strong, antibacterial and deodouring performance is especially outstanding, a kind of good and cheap, the natural function fiber of new generation that cost performance is superior, can be widely used in the fields such as weaving, building materials, automobile.
Although more than described the specific embodiment of the present invention; but being familiar with those skilled in the art is to be understood that; our described specific embodiment is illustrative; instead of for the restriction to scope of the present invention; those of ordinary skill in the art are in equivalent modification and the variation done according to spirit of the present invention, all should be encompassed in the scope that claim of the present invention protects.

Claims (3)

1. a method for CR production bamboo fibre, comprises the following steps: raw material sorts, and blocks, and cut open or flatten, boiling, bamboo wood orientation is opened fibre, the health that oils, packaging and warehousing; It is characterized in that: described boiling and bamboo wood orientation are opened and between fine step, be also provided with baking procedure, described bamboo wood orientation is opened and finely between health step, is also provided with dry and secondary and opens fibre, classification, screening step with oiling;
Described boiling step is specially: the bamboo wood of cutting open or flattening is delivered in special High Temperature High Pressure digester, added clear water or secondary bating liquor, and bamboo wood is immersed in solution completely, boiling temperature is controlled at 100~130 DEG C, is forced into 2~3kg/cm 2, boiling is after 10 minutes, then adds bating liquor stoste, and bating liquor stoste additional proportion is 1%~5% of clear water or secondary bating liquor, continues boiling 35~50 minutes;
The former formula of liquid of described bating liquor be water, sulfurous acid ammonia, hydrogen sulfate ammonia, carbonic acid ammonia, 30% ammoniacal liquor according to the ratio preparation of mass ratio 100:5:5:5:0.1~3, and the pH value of bating liquor stoste is controlled at PH=6.5~7.5;
Described baking procedure is specially: the bamboo wood after softening is put on drying machine and is toasted, make the weary white in softening bamboo chip surface wrinkling;
Described drying steps is specially: numb shape bamboo fibre is sent into drying machine and be dried;
Described secondary is opened fibre, classification, screening step and is specially: by dried numb shape bamboo fibre deliver to self-control fibre separating machine realize open finely separate, trash separator sifting sort obtains bamboo filamentary fibers and bamboo stalk impurity, wherein bamboo stalk impurity is delivered to assigned address with the output belt of setting, and bamboo filamentary fibers recycling flow separator is removed bamboo powder, finally obtain thick bamboo fibre.
2. the method for a kind of CR production bamboo fibre according to claim 1, is characterized in that: the baking temperature of described baking procedure is 50~160 DEG C, and baking time is 5~15 minutes.
3. the method for a kind of CR production bamboo fibre according to claim 1, is characterized in that: the baking temperature of described drying steps is 50~65 DEG C, and be 5~15 minutes drying time, and numb shape bamboo fibre moisture control is 20%~30%.
CN201110381221.4A 2011-11-25 2011-11-25 Non-pollution production method of bamboo fibers Active CN102517642B (en)

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Publication number Priority date Publication date Assignee Title
CN103846990B (en) * 2014-02-27 2016-02-17 浙江农林大学暨阳学院 A kind of production method of bamboo fiber of weaving
CN105316770A (en) * 2014-06-30 2016-02-10 天津工业大学 Physical preparation method for bamboo fibers
CN105113023B (en) * 2015-09-23 2017-07-07 浙江农林大学 A kind of method of bamboo Multi-layer technology bamboo fibre
WO2018119834A1 (en) * 2016-12-29 2018-07-05 张毅 Clean production method for bamboo fibres
CN107419429A (en) * 2017-06-21 2017-12-01 福建省长泰县正士餐具有限公司 A kind of technological process of bamboo fiber
CN107457877A (en) * 2017-09-09 2017-12-12 王莉 A kind of production method of environmentally friendly summer sleeping bamboo mat
CN108301050B (en) * 2018-01-26 2019-05-28 国际竹藤中心 A kind of production method of desert afforestation water delivery bamboo fibre line
CN110216756A (en) * 2019-07-04 2019-09-10 湖北崇高交通科技有限公司 Bamboo fibre extracting method, equipment and storage medium
CN113584601B (en) * 2021-08-02 2022-08-26 浙江省林业科学研究院 Preparation method of oriented crimped bamboo fibers

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CN102242403A (en) * 2011-06-15 2011-11-16 浙江农林大学 Production process for linen bamboo fibers, spinnable linen bamboo fibers and bamboo fiber yarns

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CN102242403A (en) * 2011-06-15 2011-11-16 浙江农林大学 Production process for linen bamboo fibers, spinnable linen bamboo fibers and bamboo fiber yarns

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