CN102443198A - Ginger volatile oil-beta-cyclodextrin inclusion compound and preparation method thereof - Google Patents
Ginger volatile oil-beta-cyclodextrin inclusion compound and preparation method thereof Download PDFInfo
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- CN102443198A CN102443198A CN2010105037413A CN201010503741A CN102443198A CN 102443198 A CN102443198 A CN 102443198A CN 2010105037413 A CN2010105037413 A CN 2010105037413A CN 201010503741 A CN201010503741 A CN 201010503741A CN 102443198 A CN102443198 A CN 102443198A
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- rhizoma zingiberis
- zingiberis recens
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Abstract
The invention discloses a ginger volatile oil-beta-cyclodextrin inclusion compound and a preparation method thereof. Ginger volatile oil is prepared from the following materials in parts by weight in a ratio of beta-cyclodextrin clathrate: ginger volatile oil: absolute ethyl alcohol: petroleum ether: deioned water being (90-110): (15-30): (5-15): (2.0-8.0): (450-650). The preparation method is simple and convenient to operate and low in cost, the obtained finished product has high inclusion rate, the stability of ginger volatile oil is increased, dissipation and deterioration loss of ginger volatile oil can be reduced, and storage capability and long-term quality of ginger volatile oil can be improved.
Description
Technical field
The present invention relates to a kind of food, relate in particular to a kind of Rhizoma Zingiberis Recens volatile oil, Benexate Hydrochloride and preparation technology thereof.
Background technology
As everyone knows; Ginger is the zingiber rhizome, extensively plants in China as a kind of traditional farm crop, and it not only is used as spice and is widely used in foodstuffs industry; And has an extremely important pharmaceutical use; Having induces sweat loose cold, warming middle-JIAO to arrest vomiting, preventing phlegm from forming and stopping coughing, toxicide effect also have appetite stimulator, excited corticocerebral effect.
Ginger flavor is pungent, contains 0.25%～0.3% volatile oil, and staple is gingerol, ginger ketenes, zingiberone etc., has the cold effect of Pulvis Diaphoreticus, clinically is used to treat initial stage common cold caused by wind-cold, exogenous cough etc.Ginger contains the amino acid of needed by human such as natural ginger ketenes, propalanine, L-glutamic acid, Methionin, glycocoll, and the information transmission of cerebral nervous system is had katalysis.Ginger amino acid is through the effect of gingerol and Rhizoma Zingiberis Recens volatile oil; Can arrive cerebral blood vessel to the ginger amino acid transport rapidly; Thereby make brain have enough nutrition; And in time replenish materials such as " wisdom element " hydrogen, oxygen, nitrogen, carbon, and ginger can also reduce content of cholesterol in the blood greatly, and this has brought Gospel to the hyperpietic.Therefore, exploitation and the research for ginger has wide significance.
Summary of the invention
It is higher to the invention provides a kind of inclusion rate, increases the stability of Rhizoma Zingiberis Recens volatile oil, reduces the dissipation and the deterioration losses of Rhizoma Zingiberis Recens volatile oil, improves the storage capability of Rhizoma Zingiberis Recens volatile oil and a kind of Rhizoma Zingiberis Recens volatile oil, Benexate Hydrochloride and the technology thereof of quality at a specified future date.
Another object of the present invention is exactly the technology of preparation Rhizoma Zingiberis Recens volatile oil, Benexate Hydrochloride, and the simple easy handling of technology.
The objective of the invention is to realize in the following manner:
A kind of Rhizoma Zingiberis Recens volatile oil, Benexate Hydrochloride is characterized in that it being to count ratio following raw materials in parts by weight to be prepared from: beta-cyclodextrin: Rhizoma Zingiberis Recens volatile oil: absolute ethyl alcohol: sherwood oil: deionized water=90～110: 15～30: 5～15: 2.0～8.0: 450～650.
Described a kind of Rhizoma Zingiberis Recens volatile oil, Benexate Hydrochloride is characterized in that it being to count ratio following raw materials in parts by weight to be prepared from: beta-cyclodextrin: Rhizoma Zingiberis Recens volatile oil: absolute ethyl alcohol: sherwood oil: deionized water=100: 22: 10: 5.0: 550.
The technology of preparation Rhizoma Zingiberis Recens volatile oil, Benexate Hydrochloride comprises the following steps:
1), raw material is handled: respectively the exsiccant beta-cyclodextrin is dissolved in the deionized water by formulation ratio, stirs, and gained solution is incubated gained A solution at 45 ℃; Rhizoma Zingiberis Recens volatile oil joined make its thorough mixing gained B solution in the absolute ethyl alcohol, for use.
2), inclusion is handled: the slow B solution of gained in the step 1) is joined in the A solution, continue insulation then at 30 ℃, with ultrasonic oscillation 1～2h, make inclusion complete.
3), refrigeration, filter: with step 2) the gained inclusion compound places cold compartment of refrigerator refrigeration 8～10h, will precipitate precipitate again and filter and drain, it is for use to get throw out.
4), carrying out washing treatment: adopt the throw out of petroleum ether above-mentioned steps gained, obtain till the oil stains-less of throw out surface, clean with deionized water wash again.
5), crushing packing: step 4) gained throw out is placed vacuum drier, and pulverize on kibbler dry back, and the gained white powder is finished product, carries out packing after the sterilization getting final product again.
The present invention's effect that has the following advantages: technology of the present invention is simple, and is easy to operate, and cost is low; Gained finished product inclusion rate is higher; Increase the stability of Rhizoma Zingiberis Recens volatile oil, reduce the dissipation and the deterioration losses of Rhizoma Zingiberis Recens volatile oil, improve the storage capability and the quality at a specified future date of Rhizoma Zingiberis Recens volatile oil.
Embodiment
Embodiment 1:
A kind of Rhizoma Zingiberis Recens volatile oil, Benexate Hydrochloride is characterized in that it being to count ratio following raw materials in parts by weight to be prepared from: beta-cyclodextrin: Rhizoma Zingiberis Recens volatile oil: absolute ethyl alcohol: sherwood oil: deionized water=100: 22: 10: 5.0: 550.
The technology of preparation Rhizoma Zingiberis Recens volatile oil, Benexate Hydrochloride comprises the following steps:
1), raw material is handled: respectively the exsiccant beta-cyclodextrin is dissolved in the deionized water by formulation ratio, stirs, and gained solution is incubated gained A solution at 45 ℃; Rhizoma Zingiberis Recens volatile oil joined make its thorough mixing gained B solution in the absolute ethyl alcohol, for use.
2), inclusion is handled: the slow B solution of gained in the step 1) is joined in the A solution, continue insulation then at 30 ℃, with ultrasonic oscillation 1～2h, make inclusion complete.
3), refrigeration, filter: with step 2) the gained inclusion compound places cold compartment of refrigerator refrigeration 8～10h, will precipitate precipitate again and filter and drain, it is for use to get throw out.
4), carrying out washing treatment: adopt the throw out of petroleum ether above-mentioned steps gained, obtain till the oil stains-less of throw out surface, clean with deionized water wash again.
5), crushing packing: step 4) gained throw out is placed vacuum drier, and pulverize on kibbler dry back, and the gained white powder is finished product, carries out packing after the sterilization getting final product again.
Embodiment 2:
A kind of Rhizoma Zingiberis Recens volatile oil, Benexate Hydrochloride are to count ratio following raw materials in parts by weight to be prepared from: beta-cyclodextrin: Rhizoma Zingiberis Recens volatile oil: absolute ethyl alcohol: sherwood oil: deionized water=90: 30: 15: 8.0: 650.Other is with embodiment 1.
Embodiment 3:
A kind of Rhizoma Zingiberis Recens volatile oil, Benexate Hydrochloride are to count ratio following raw materials in parts by weight to be prepared from: beta-cyclodextrin: Rhizoma Zingiberis Recens volatile oil: absolute ethyl alcohol: sherwood oil: deionized water=110: 15: 5: 2.0: 450.Other is with embodiment 1.
Claims (3)
1. a Rhizoma Zingiberis Recens volatile oil, Benexate Hydrochloride is characterized in that it being to count ratio following raw materials in parts by weight to be prepared from: beta-cyclodextrin: Rhizoma Zingiberis Recens volatile oil: absolute ethyl alcohol: sherwood oil: deionized water=90～110: 15～30: 5～15: 2.0～8.0: 450～650.
2. a kind of Rhizoma Zingiberis Recens volatile oil according to claim 1, Benexate Hydrochloride is characterized in that it being to count ratio following raw materials in parts by weight to be prepared from: beta-cyclodextrin: Rhizoma Zingiberis Recens volatile oil: absolute ethyl alcohol: sherwood oil: deionized water=100: 22: 10: 5.0: 550.
3. the technology of preparation Rhizoma Zingiberis Recens volatile oil, Benexate Hydrochloride is characterized in that comprising the following steps:
1), raw material is handled: respectively the exsiccant beta-cyclodextrin is dissolved in the deionized water by formulation ratio, stirs, and gained solution is incubated gained A solution at 45 ℃; Rhizoma Zingiberis Recens volatile oil joined make its thorough mixing gained B solution in the absolute ethyl alcohol, for use.
2), inclusion is handled: the slow B solution of gained in the step 1) is joined in the A solution, continue insulation then at 30 ℃, with ultrasonic oscillation 1～2h, make inclusion complete.
3), refrigeration, filter: with step 2) the gained inclusion compound places cold compartment of refrigerator refrigeration 8～10h, will precipitate precipitate again and filter and drain, it is for use to get throw out.
4), carrying out washing treatment: adopt the throw out of petroleum ether above-mentioned steps gained, obtain till the oil stains-less of throw out surface, clean with deionized water wash again.
5), crushing packing: step 4) gained throw out is placed vacuum drier, and pulverize on kibbler dry back, and the gained white powder is finished product, carries out packing after the sterilization getting final product again.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010105037413A CN102443198A (en) | 2010-10-12 | 2010-10-12 | Ginger volatile oil-beta-cyclodextrin inclusion compound and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010105037413A CN102443198A (en) | 2010-10-12 | 2010-10-12 | Ginger volatile oil-beta-cyclodextrin inclusion compound and preparation method thereof |
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| CN102443198A true CN102443198A (en) | 2012-05-09 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102961713A (en) * | 2012-11-29 | 2013-03-13 | 江西中天医药生物有限公司 | Ginger and garlic enteric-coated tablet and preparation method thereof |
| CN105169410A (en) * | 2015-11-04 | 2015-12-23 | 南京美凯生物科技有限公司 | Ginger essential oil cyclodextrin inclusion compound and preparation method thereof |
| CN108295226A (en) * | 2018-02-13 | 2018-07-20 | 西安医学院 | A kind of preparation method of Rhizoma Zingiberis Recens volatile oil beta-cyclodextrin microballoon |
| CN108904706A (en) * | 2018-09-26 | 2018-11-30 | 河北地邦动物保健科技有限公司 | A kind of compound essential oil and preparation method thereof for treating chicken proventriculitis |
-
2010
- 2010-10-12 CN CN2010105037413A patent/CN102443198A/en active Pending
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102961713A (en) * | 2012-11-29 | 2013-03-13 | 江西中天医药生物有限公司 | Ginger and garlic enteric-coated tablet and preparation method thereof |
| CN102961713B (en) * | 2012-11-29 | 2014-05-28 | 江西中天医药生物有限公司 | Ginger and garlic enteric-coated tablet and preparation method thereof |
| CN105169410A (en) * | 2015-11-04 | 2015-12-23 | 南京美凯生物科技有限公司 | Ginger essential oil cyclodextrin inclusion compound and preparation method thereof |
| CN108295226A (en) * | 2018-02-13 | 2018-07-20 | 西安医学院 | A kind of preparation method of Rhizoma Zingiberis Recens volatile oil beta-cyclodextrin microballoon |
| CN108904706A (en) * | 2018-09-26 | 2018-11-30 | 河北地邦动物保健科技有限公司 | A kind of compound essential oil and preparation method thereof for treating chicken proventriculitis |
| CN108904706B (en) * | 2018-09-26 | 2021-05-07 | 河北地邦动物保健科技有限公司 | Compound essential oil for treating chicken proventriculitis and preparation method thereof |
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Application publication date: 20120509 |