CN102433075A - Method for quickly preparing special gelatin for candies from raw bone meal - Google Patents
Method for quickly preparing special gelatin for candies from raw bone meal Download PDFInfo
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- CN102433075A CN102433075A CN201110357287XA CN201110357287A CN102433075A CN 102433075 A CN102433075 A CN 102433075A CN 201110357287X A CN201110357287X A CN 201110357287XA CN 201110357287 A CN201110357287 A CN 201110357287A CN 102433075 A CN102433075 A CN 102433075A
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- bone meal
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- raw bone
- alkali lye
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Abstract
The invention belongs to the field of gelatin preparation, and particularly relates to a method for quickly preparing special gelatin for candies from raw bone meal. The method comprises the following process steps of: meal milling, impurity removal through pickling, water washing, gelatin solution extraction, neutralization, rough filtration, fine filtration, and packaging after concentration and drying. According to the method, animal bones are milled into bone meal to increase the specific surface area of the bone meal and increase the reaction speed of the bone meal; and compared with the traditional gelatin production, the method disclosed by the invention has the advantages that: the production cycle is shortened by more than 60 days, and pollution and consumption are reduced. The gelatin prepared by using the method has the advantages of high freezing intensity, moderate viscosity, good transparency and low cost; and the viscosity of the gelatin is matched with the freezing intensity of the gelatin, so that the gelatin is suitable for the field of producing foods such as candies and the like.
Description
One, technical field:
The invention belongs to the gelatin preparation field, particularly a kind of raw bone meal prepares the method for the special-purpose gelatin of candy fast.
Two, background technology
Traditional alkali process is all adopted in China's bone gelatin(e) production at present, and its operational path is: animal bone → skeletal grain → pickling → washing → liming → wash → neutralize → wash → carry glue → filtration → concentrated → drying → pulverizing.Though having, the tradition gelatin goes up century-old history, the technology comparative maturity, and the production cycle is long; Reach 60 days to 90 days, the consumption of various materials is high, and especially water resource waste is serious; What the traditional technology liming was adopted is milk of lime, all has every day a large amount of lime-ash, waste water to produce, and belongs to highly energy-consuming, high pollution industry; And its gelatin product is applied in the candy industry when the time existing viscosity to meet optimality criterion 3.7-4.3mpa.s, the intensity of congealing 120-180g on the low side; And the intensity of congealing is when meeting optimality criterion >=240g, the higher 4.6-5.2mpa.s of viscosity because the viscosity of gelatin do not match with the intensity of congealing, be applied in confectionary products after, be prone to adhesion, influence moulding, can not satisfy the requirement of confectionary products.The patent of invention of publication number CN1977013A discloses the method for a kind of preparation and purifying gelatin, and this method is that the animal bone water is worn into slurry, and the high temperature extracting obtains glue in the acidic solution of PH=2.4-3.9; Again through separating for several times, concentrate, drying obtains gelatin product, this method is processed pulp with the water mill aggregate, water consumption is big; The industrialization difficulty is big; This method is handled without pickling and is sloughed the mineral substance in the aggregate, but directly in acid solution, extracts glue, will have a large amount of impurity in the glue and be difficult to separate; Influence the purity and the performance of gelatin, can not satisfy the requirement of confectionary products.In recent years, have the report enzymolysis process to prepare the method for gelatin, its production cycle shortens, but cost is high, does not appear in the newspapers to be used for confectionery industry.
Three, summary of the invention
The present invention is directed to present manufacturing of gelatin industry and do not have special-purpose gelatin of the confectionery industry of being exclusively used in and the present situation that other gelatin can not satisfy the confectionery industry requirement fully; The just viscosity of gelatin and the unmatched problem of intensity of congealing; The method that a kind of raw bone meal prepares the special-purpose gelatin of candy has fast been proposed; The technical scheme that the present invention takes is: a kind of raw bone meal prepares the method for the special-purpose gelatin of candy fast, it is characterized in that it and is made up of following operation: animal bone abrasive dust → pickling removal of impurities → washing → extracting glue → neutralization → coarse filtration → essence filter → concentrate drying packing; Wherein: the processing condition of animal bone abrasive dust operation are: animal bone is ground to form 40~160 purpose raw bone meals; The processing condition of pickling removal of impurities operation are: will grind good raw bone meal and in temperature is 15 ℃~25 ℃ acid solution, soak 6~12 hours; Slough the impurity such as mineral substance in the raw bone meal; The pH value of acid solution is 1~2.5, and the mass volume ratio of raw bone meal and acid solution is 1g:2~6ml; The processing condition of washing step are: the raw bone meal behind acid soak is used water washing, to the PH=4 that washes water~6; The processing condition of extracting glue operation are: the raw bone meal after will washing in temperature be under 40 ℃~70 ℃ the alkali lye through 5~18 hours extracting glues, the pH value of alkali lye is 8~14, the mass volume ratio of raw bone meal and alkali lye is 1g:4~10ml; In with the processing condition of operation be: the extracting glue is regulated pH value to 5.5~6.5 with acid; The processing condition of coarse filtration operation are: the extracting glue of becoming reconciled in inciting somebody to action with filter filters under 40 ℃~60 ℃ temperature, and gelatin solution is separated with solid residue; The processing condition of smart filter operation are: with the smart filter under 40 ℃~60 ℃ temperature of the gelatin solution after the coarse filtration; The processing condition of concentrate drying packaging process are: essence filtrating is packed with the ordinary method concentrate drying.Wherein acid solution is hydrochloric acid solution or nitric acid or phosphoric acid liquid or Glacial acetic acid min. 99.5 liquid.Alkali lye is the complex liquid of two kinds of alkali lye of Pottasium Hydroxide alkali lye or sodium hydroxide lye or yellow soda ash alkali lye or sodium hydrogencarbonate alkali lye or calcium hydroxide alkali lye or above-mentioned alkali lye.Coarse filtration adopts vacuum filtration and Plate Filtration.Smart filter adopts membrane filtration and IX to filter.The present invention grinds to form bone meal with animal bone, increases the specific surface area of bone meal, improves its speed of response, compares with traditional manufacturing of gelatin, and the production cycle shortened more than 60 days, and has reduced and polluted and consumption; Congeal intensity height, modest viscosity, transparency of products obtained therefrom of the present invention is good, and cost is low, the viscosity of gelatin with congeal strength matching, be suitable for making field of food such as candy.
Four, embodiment
Embodiment 1: a kind of raw bone meal prepares the method for the special-purpose gelatin of candy fast; 1000 gram animal bone are worn into 40 purpose bone meal; In temperature is that 25 ℃, pH value are to soak 12 hours in the salpeter solution of 1,2000 ml, sloughs the impurity such as mineral substance in the raw bone meal, and the pH value that the raw bone meal behind acid soak is washed with water to washing water is 6; Raw bone meal after the washing is that 70 ℃, pH value are through 5 hours extracting glues under the yellow soda ash alkali lye of 14,4000 ml in temperature; The extracting glue with the acid neutralization, is regulated pH value to 5.5, and neutralizer is 60 ℃ in temperature and carries out the secondary coarse filtration with vacuum filter and flame filter press down; To filtrate and under temperature is 60 ℃, carry out the filter of secondary essence with membrane filtration and IX filtration, smart filtrating packed to such an extent that candy special use gelatin 140 restrains with the ordinary method concentrate drying.Its product index such as table 1.
Table 1:
The intensity of congealing | 281g |
Viscosity | 3.90mpa.s |
Transmitance | 450 nm 86%,? 620nm? 97%. |
Embodiment 2: a kind of raw bone meal prepares the method for the special-purpose gelatin of candy fast; 1000 gram animal bone are worn into 160 purpose bone meal; In temperature is that 15 ℃, pH value are to soak 6 hours in the phosphoric acid solution of 2.5,6000 ml, sloughs the impurity such as mineral substance in the raw bone meal, and the pH value that the raw bone meal behind acid soak is washed with water to washing water is 4; Raw bone meal after the washing is that 40 ℃, pH value are through 18 hours extracting glues under the sodium hydrogencarbonate alkali lye of 8,10000 ml in temperature; The extracting glue with the acid neutralization, is regulated pH value to 6.5, and neutralizer is 40 ℃ in temperature and carries out the secondary coarse filtration with vacuum filter and flame filter press down; To filtrate and under temperature is 40 ℃, carry out the filter of secondary essence with membrane filtration and IX filtration, smart filtrating packed to such an extent that candy special use gelatin 150 restrains with the ordinary method concentrate drying.Its product index such as table 2.
Table 2:
The intensity of congealing | 270g |
Viscosity | 3.70mpa.s |
Transmitance | 450nm? 87%, 620nm? 98%. |
Embodiment 3: a kind of raw bone meal prepares the method for the special-purpose gelatin of candy fast; 1000 gram animal bone are worn into 120 purpose bone meal; In temperature is that 20 ℃, pH value are to soak 8 hours in the hydrochloric acid soln of 2,4000 ml, sloughs the impurity such as mineral substance in the raw bone meal, and the pH value that the raw bone meal behind acid soak is washed with water to washing water is 5; Raw bone meal after the washing is that 50 ℃, pH value are through 15 hours extracting glues under the compound alkali lye of Pottasium Hydroxide and calcium hydroxide of 10,8000 ml in temperature; The extracting glue with the acid neutralization, is regulated pH value to 6, and neutralizer is 45 ℃ in temperature and carries out the secondary coarse filtration with vacuum filter and flame filter press down; To filtrate and under temperature is 42 ℃, carry out the filter of secondary essence with membrane filtration and IX filtration, smart filtrating packed to such an extent that candy special use gelatin 135 restrains with the ordinary method concentrate drying.Its product index such as table 3.
Table 3:
The intensity of congealing | 280g |
Viscosity | 4.20mpa.s |
Transmitance | 450nm? 88%, 620nm? 98%. |
Embodiment 4: a kind of raw bone meal prepares the method for the special-purpose gelatin of candy fast; 1000 gram animal bone are worn into 100 purpose bone meal; In temperature is that 18 ℃, pH value are to soak 10 hours in the glacial acetic acid solution of 2.5,3000 ml; Slough the impurity such as mineral substance in the raw bone meal; The pH value that raw bone meal behind acid soak is washed with water to washing water is 5.5, the raw bone meal after the washing temperature be 60 ℃, pH value be under the compound alkali lye of sodium hydroxide and sodium hydrogencarbonate of 10.5,7000 ml through 13 hours extracting glues, with the extracting glue with the acid neutralization; Regulate pH value to 5.5; Neutralizer is 55 ℃ in temperature and carries out the secondary coarse filtration with vacuum filter and flame filter press down, will filtrate and under temperature is 50 ℃, carry out the filter of secondary essence with membrane filtration and IX filtration, and smart filtrating packed to such an extent that candy special use gelatin 150 restrains with the ordinary method concentrate drying.Its product index such as table 4.
Table 4
The intensity of congealing | 310g |
Viscosity | 4.25mpa.s |
Transmitance | 450nm? 87%, 620nm? 97%. |
Embodiment 5: a kind of raw bone meal prepares the method for the special-purpose gelatin of candy fast; 1000 gram animal bone are worn into 80 purpose bone meal; In temperature is that 18 ℃, pH value are to soak 9 hours in the phosphoric acid solution of 2.0,3500 ml, sloughs the impurity such as mineral substance in the raw bone meal, and the pH value that the raw bone meal behind acid soak is washed with water to washing water is 5.5; Raw bone meal after the washing is that 55 ℃, pH value are through 8 hours extracting glues under the compound alkali lye of Pottasium Hydroxide and calcium hydroxide of 9,6500 ml in temperature; The extracting glue with the acid neutralization, is regulated pH value to 5.5, and neutralizer is 50 ℃ in temperature and carries out the secondary coarse filtration with vacuum filter and flame filter press down; To filtrate and under temperature is 48 ℃, carry out the filter of secondary essence with membrane filtration and IX filtration, smart filtrating packed to such an extent that candy special use gelatin 148 restrains with the ordinary method concentrate drying.Its product index such as table 5.
Like table 5:
The intensity of congealing | 295g |
Viscosity | 4.16mpa.s |
Transmitance | 450nm? 88%, 620nm? 98%. |
Obviously, the above embodiment of the present invention only is to give an example for what clearly the present invention is described and is done, and is not to be the qualification to embodiment of the present invention.For the those of ordinary skill in affiliated field, on the basis of above-mentioned explanation, can also make other multi-form variation or change, can't give exhaustive to all embodiments here.Everyly belong to the row that conspicuous variation that technical scheme of the present invention extends out or change still are in protection scope of the present invention.
Claims (5)
1. a raw bone meal prepares the method for the special-purpose gelatin of candy fast; The technical scheme that the present invention takes is: a kind of raw bone meal prepares the method for the special-purpose gelatin of candy fast, it is characterized in that it and is made up of following operation: animal bone abrasive dust → pickling removal of impurities → washing → extracting glue → neutralization → coarse filtration → essence filter → concentrate drying packing; Wherein: the processing condition of abrasive dust operation are: animal bone is ground to form 40~160 purpose raw bone meals; The processing condition of pickling removal of impurities operation are: will grind good raw bone meal and in temperature is 15 ℃~25 ℃ acid solution, soak 6~12 hours; Slough the impurity such as mineral substance in the raw bone meal; The pH value of acid solution is 1~2.5, and the mass volume ratio of raw bone meal and acid solution is 1g:2~6ml; The processing condition of washing step are: the raw bone meal behind acid soak is used water washing, to the PH=4 that washes water~6; The processing condition of extracting glue operation are: the raw bone meal after will washing in temperature be under 40 ℃~70 ℃ the alkali lye through 5~18 hours extracting glues, the pH value of alkali lye is 8~14, the mass volume ratio of raw bone meal and alkali lye is 1g:4~10ml; In with the processing condition of operation be: the extracting glue is regulated pH value to 5.5~6.5 with acid; The processing condition of coarse filtration operation are: the extracting glue of becoming reconciled in inciting somebody to action with filter filters under 40 ℃~60 ℃ temperature, and gelatin solution is separated with solid residue; The processing condition of smart filter operation are: with the smart filter under 40 ℃~60 ℃ temperature of the gelatin solution after the coarse filtration; The processing condition of concentrate drying packaging process are: essence filtrating is packed with the ordinary method concentrate drying.
2. a kind of raw bone meal according to claim 1 prepares the method for the special-purpose gelatin of candy fast, it is characterized in that described acid solution is hydrochloric acid solution or nitric acid or phosphoric acid liquid or Glacial acetic acid min. 99.5 liquid.
3. a kind of raw bone meal according to claim 1 prepares the method for the special-purpose gelatin of candy fast, it is characterized in that described alkali lye is the complex liquid of two kinds of alkali lye of Pottasium Hydroxide alkali lye or sodium hydroxide lye or yellow soda ash alkali lye or sodium hydrogencarbonate alkali lye or calcium hydroxide alkali lye or above-mentioned alkali lye.
4. a kind of raw bone meal according to claim 1 prepares the method for the special-purpose gelatin of candy fast, it is characterized in that described coarse filtration is to adopt vacuum filtration and Plate Filtration cascade filtration.
5. a kind of raw bone meal according to claim 1 prepares the method for the special-purpose gelatin of candy fast, it is characterized in that described smart filter is to adopt membrane filtration and IX to filter cascade filtration.
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Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103122219A (en) * | 2011-11-17 | 2013-05-29 | 中国科学院理化技术研究所 | Method for preparing gelatin by taking bone as raw material |
CN103571342A (en) * | 2013-10-29 | 2014-02-12 | 张苗 | Method of preparing animal bone glue by virtue of solvent method |
CN103627329A (en) * | 2013-11-21 | 2014-03-12 | 安徽丰原发酵技术工程研究有限公司 | Method for extracting gelatin from tailings |
CN103740283A (en) * | 2013-12-24 | 2014-04-23 | 安徽省淮河制胶有限公司 | Preparation method for producing industrial gum via animal bones |
CN108203567A (en) * | 2016-12-20 | 2018-06-26 | 湖南尔康明胶有限公司 | The technique that a kind of acid system prepares pharmagel |
CN109554120A (en) * | 2018-11-29 | 2019-04-02 | 沾化恒鑫工业科技有限公司 | A kind of method of alkaline process production cattle hide gelatin |
CN116515402A (en) * | 2023-06-12 | 2023-08-01 | 成都经典明胶有限公司 | Clarification method of gelatin |
Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN87103821A (en) * | 1987-05-25 | 1988-12-07 | 宋洪潮 | The alkali washing process of gelatin manufacture and equipment |
WO1994021739A1 (en) * | 1993-03-19 | 1994-09-29 | Ellco Food Ab | Method for producing gelatin |
CN1318607A (en) * | 2000-04-19 | 2001-10-24 | 包头东宝乐凯明胶有限公司 | Technological process of producing bone gelatine for color photography |
JP2003206448A (en) * | 2002-01-15 | 2003-07-22 | Nitta Gelatin Inc | Method of producing gelatin |
EP1499202A1 (en) * | 2002-04-22 | 2005-01-26 | Danexport A/S | Method for producing gelatin |
CN101942276A (en) * | 2010-08-23 | 2011-01-12 | 浙江吉达生物科技有限公司 | Process for preparing fish product gelatin |
CN102181234A (en) * | 2011-03-16 | 2011-09-14 | 罗赛洛(温州)明胶有限公司 | Process for producing high-viscosity cowhide alkaline gelatin by batch and alkaline (BATALK) method |
-
2011
- 2011-11-13 CN CN 201110357287 patent/CN102433075B/en active Active
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN87103821A (en) * | 1987-05-25 | 1988-12-07 | 宋洪潮 | The alkali washing process of gelatin manufacture and equipment |
WO1994021739A1 (en) * | 1993-03-19 | 1994-09-29 | Ellco Food Ab | Method for producing gelatin |
CN1318607A (en) * | 2000-04-19 | 2001-10-24 | 包头东宝乐凯明胶有限公司 | Technological process of producing bone gelatine for color photography |
JP2003206448A (en) * | 2002-01-15 | 2003-07-22 | Nitta Gelatin Inc | Method of producing gelatin |
EP1499202A1 (en) * | 2002-04-22 | 2005-01-26 | Danexport A/S | Method for producing gelatin |
CN101942276A (en) * | 2010-08-23 | 2011-01-12 | 浙江吉达生物科技有限公司 | Process for preparing fish product gelatin |
CN102181234A (en) * | 2011-03-16 | 2011-09-14 | 罗赛洛(温州)明胶有限公司 | Process for producing high-viscosity cowhide alkaline gelatin by batch and alkaline (BATALK) method |
Non-Patent Citations (1)
Title |
---|
姚龙坤: "关于酸法猪皮明胶的生产", 《明胶科学与技术》 * |
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103122219A (en) * | 2011-11-17 | 2013-05-29 | 中国科学院理化技术研究所 | Method for preparing gelatin by taking bone as raw material |
CN103571342A (en) * | 2013-10-29 | 2014-02-12 | 张苗 | Method of preparing animal bone glue by virtue of solvent method |
CN103627329A (en) * | 2013-11-21 | 2014-03-12 | 安徽丰原发酵技术工程研究有限公司 | Method for extracting gelatin from tailings |
CN103627329B (en) * | 2013-11-21 | 2015-12-30 | 安徽丰原发酵技术工程研究有限公司 | A kind of method extracting gelatin from tailing |
CN103740283A (en) * | 2013-12-24 | 2014-04-23 | 安徽省淮河制胶有限公司 | Preparation method for producing industrial gum via animal bones |
CN108203567A (en) * | 2016-12-20 | 2018-06-26 | 湖南尔康明胶有限公司 | The technique that a kind of acid system prepares pharmagel |
CN109554120A (en) * | 2018-11-29 | 2019-04-02 | 沾化恒鑫工业科技有限公司 | A kind of method of alkaline process production cattle hide gelatin |
CN109554120B (en) * | 2018-11-29 | 2021-02-26 | 山东恒鑫生物科技有限公司 | Method for producing oxhide gelatin by alkaline process |
CN116515402A (en) * | 2023-06-12 | 2023-08-01 | 成都经典明胶有限公司 | Clarification method of gelatin |
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Effective date of registration: 20171128 Address after: 751100 Jin Ji industrial park, Wuzhong City, the Ningxia Hui Autonomous Region (Guan Ma Lake) Patentee after: NINGXIA XINHAOYUAN BIOLOGICAL POLYTRON TECHNOLOGIES INC. Address before: The victory road 810001 Qinghai city of Xining province Xing Sheng Xiang No. 8 fidelity Park Building No. 3 room 1103 Co-patentee before: Mou Zhongchen Patentee before: Dai Yimin |