CN102433048A - Chlorinated rubber finish and preparation method thereof - Google Patents
Chlorinated rubber finish and preparation method thereof Download PDFInfo
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- CN102433048A CN102433048A CN2011100807286A CN201110080728A CN102433048A CN 102433048 A CN102433048 A CN 102433048A CN 2011100807286 A CN2011100807286 A CN 2011100807286A CN 201110080728 A CN201110080728 A CN 201110080728A CN 102433048 A CN102433048 A CN 102433048A
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Abstract
The invention discloses a chlorinated rubber finish and a preparation method thereof The chlorinated rubber finish provided in the invention comprises the following components, by weight, 10-30 parts of titanium dioxide, 10-30 parts of xylene, 10-20 parts of chlorinated paraffin, 10-20 parts of chlorinated rubber, 6-12 parts of a change promoting agent, and 2-8 parts of a coupling agent. The chlorinated rubber adopted in the invention, which contains no organic solvents, has the advantages of environmental protection, non-toxicity, and good safety. The water resistance, the endurance, the weatherability, the corrosion resistance and the decoration of the chlorinated rubber finish are improved through improving the ratio of the change promoting agent: the coupling agent: other components, and the adhesion between the layers of the chlorinated rubber finish is excellent, so the layers of the finish are miscible in one, thereby there is no need to remove the firm old finish when the old chlorinated rubber finish is afresh maintained and coated, and the maintenance is convenient.
Description
Technical field
The present invention relates to the paint field, be specifically related to a kind of chlorinated rubber finish paint and preparation method thereof.
Background technology
Finish paint is one deck of smearing at last in the construction wall finishing as the final coating of application, and the whole structure that the finishing back is demonstrated all is to embody through this one deck.Therefore material therefor there is higher requirement; Not only good colourity and brightness to be arranged; More require to have good anti-pollution, ageing-resistant, protection against the tide; Mildew resistance is good, also to have free from environmental pollution, safety non-toxic, no fire hazard, easy construction, dried coating film fast, protect light and protect characteristics such as look good, good permeability.Have and decorate and defencive function,, the resistivity in the face of severe environment need be arranged also like color, gloss, texture etc.
Sell the various finish paints that use in the market, most of performances are comparatively single, can not satisfy the diversified demand of people, especially to being applied in the finish paint in industrial refitting field.Also there is organic problem of solvent residue in existing finish paint, so not only brings environmental hazard, also can influence the healthy of people.
Summary of the invention
The purpose of this invention is to provide a kind of chlorinated rubber finish paint.
Chlorinated rubber finish paint provided by the invention, it comprises the material of following weight proportion: white titanium pigment 10-30 part, YLENE 10-30 part, clorafin 10-20 part, chlorinated rubber 10-20 part, short change agent 6-12 part, coupling agent 2-8 part.
Above-mentioned chlorinated rubber finish paint preferably includes the material of following weight proportion: 20 parts of white titanium pigments, 20 parts of YLENE, 15 parts of clorafins, 15 parts of chlorinated rubbers, short 9 parts of agent, 5 parts of the coupling agents of becoming.
Above-mentioned short change agent can be the 6900-20X polyamide wax.
Preferably, said coupling agent is positive titanic acid ester.
Another object of the present invention is to provide a kind of preparation method of above-mentioned chlorinated rubber finish paint.It mainly may further comprise the steps:
1) takes by weighing white titanium pigment, YLENE, clorafin, chlorinated rubber, short agent and the coupling agent of becoming;
2) each component that takes by weighing in the step 1) is mixed stirring, obtain above-mentioned chlorinated rubber finish paint.
Preferably, among the above-mentioned preparation method, the weight proportion of said each component is: white titanium pigment 10-30 part, YLENE 10-30 part, clorafin 10-20 part, chlorinated rubber 10-20 part, short change agent 6-12 part, coupling agent 2-8 part.
The more excellent weight proportion of above-mentioned each component is: 20 parts of white titanium pigments, 20 parts of YLENE, 15 parts of clorafins, 15 parts of chlorinated rubbers, short 9 parts of agent, 5 parts of the coupling agents of becoming.
Preferably, said short change agent is the 6900-20X polyamide wax.
Preferably, said coupling agent is positive titanic acid ester.
The present invention can be prepared into versicolor chlorinated rubber finish paint.
The present invention can carry out surface treatment in use, is specially preceding road lacquer and answers complete drying, eliminates greasy dirts all on the paint film and foreign material.The present invention can adopt Airless spraying, aerial spraying, roller coating and/or brushing.Wherein roller coating can be used when application can not reach desired thickness with brushing.When roller coating and brushing, amount of dilution can be 0-3% (in paint weight).The present invention can once be sprayed and reach dry film 140 μ m when being adopted hydraulic spraying, does not need repeatedly to spray.
The application road number of chlorinated rubber finish paint of the present invention is preferably the 1-2 road, can decide as the case may be.
Chlorinated rubber finish paint provided by the invention has the following advantages:
(1) the chlorinated rubber organic solvent-free that uses, thereby environment-protecting asepsis;
(2) paint film of the present invention's formation is low to the infiltration of water vapour and oxygen, and the present invention has good water tolerance, preservative property and ornamental;
(3) it is fast to have a dryness, than the fast several times of the dryness of alkyd paint;
(4) have excellent low-temperature construction performance, can under-20 ℃-50 ℃ environment, construct;
(5) dissolve each other and be one between paint film layer and the layer, excellent ply adhesion is arranged, when on the old paint film of chlorinated rubber, keeping in repair again, needn't remove firm old paint film, keep in repair very convenient;
(6) have good weathering resistance and weather resistance.
Purposes of the present invention is extremely extensive, is applicable to the protection on various land steelwork such as boats and ships waterline, shell, superstructure and power plant, Iron And Steel Plant, harbour steelwork, chemical plant, bridge, freight container, hydraulic steel gate, factory building, petroleum storage tank outer wall, dry gas holder surface and the usefulness of making to decorate finish paint.
Embodiment
In order to make the object of the invention, technical scheme and advantage clearer,, the present invention is further elaborated below in conjunction with embodiment.Should be appreciated that specific embodiment described herein only in order to explanation the present invention, and be not used in qualification the present invention.
The raw material that uses among the present invention mainly contains white titanium pigment, YLENE, clorafin, chlorinated rubber, short agent and the coupling agent of becoming, wherein:
Clorafin is available from Shanghai electrochemical factory; Chlorinated rubber is available from chemical plant, Fenghua, Zhejiang.The short agent employing 6900-20X polyamide wax that becomes is available from Di Sibalong company.
Embodiment 1.
Press following weight proportion (weight part):
After above-mentioned each component that takes by weighing mixed stirring, it was qualified to be dispersed to fineness through sand mill, obtains chlorinated rubber finish paint of the present invention.
Before adopting the present invention to carry out application, carry out surface treatment earlier, surface treatment is behind preceding road lacquer complete drying, eliminates greasy dirts all on the paint film and foreign material.The chlorinated rubber finish paint for preparing with method of the present invention then carries out Airless spraying, before japanning, is rust-proofing primer with aluminium powder chlorinated rubber rust-inhibiting paint earlier, is that the middle layer lacquer carries out the lacquer processing of preceding road with chlorinated rubber iron oxide red thick rust-inhibiting paint.The amount of dilution of Airless spraying is 0-5% (in a paint weight), dilutes with 101 thinners well known in the art, and the thickness that forms dry film is 70-140 μ m; The bore of nozzle is 0.4-0.5mm; Spray too that power is 15-20Mpa, application 1-2 road can be decided as the case may be.
Be not more than 85% in relative humidity, the ground temperature is higher than under the condition of above 3 ℃ of dew point, treats the steel surface that being coated with of coating finish be equipped with preceding road lacquer with the chlorinated rubber finish paint of this method preparation and carries out Airless spraying, and the result is as shown in table 1.
Table 1. chlorinated rubber finish paint Airless spraying result
| Sample | Volume solid % | Build μ m | Wet-film thickness μ m | Consumption g/m2 |
| 1 | 44±3 | 69.5 | 157 | 221 |
| 2 | 42±3 | 70 | 167 | 235 |
| 3 | 42±3 | 40 | 94 | 120 |
| 4 | 42±3 | 71 | 168 | 237 |
| 5 | 40±3 | 40 | 100 | 127 |
| 6 | 42±3 | 70 | 165 | 234 |
| 7 | 42±3 | 70 | 167 | 233 |
| 8 | 42±3 | 70 | 167 | 234 |
| 9 | 40±3 | 40 | 100 | 127 |
Wherein, the volume solid is pressed GB/T9272 eqv ISO3233:1998 regulation mensuration.31 ℃ of flash-points.
Above-mentioned chlorinated rubber finish paint is measured time of drying under 25 ℃ of conditions, refer to do≤2h, does solid work≤12h.
5 ℃, 20 ℃ and 30 ℃ of overcoating pitch times of measuring the chlorinated rubber finish paint of present embodiment preparation down, experimental result is as shown in table 2 below respectively.
Table 2. overcoating pitch time
Through observation, but the knowledge capital invention has excellent water tolerance, weather resistance, non-corrosibility, weathering resistance and ornamental, and dryness is fast, safety and environmental protection.
Embodiment 2.
Press following weight proportion (weight part):
After above-mentioned each component that takes by weighing mixed stirring, sand milling to fineness was qualified, obtains chlorinated rubber finish paint of the present invention.
Before adopting the present invention to carry out application, carry out surface treatment earlier, surface treatment is behind preceding road lacquer complete drying, eliminates greasy dirts all on the paint film and foreign material.Chlorinated rubber finish paint with method preparation of the present invention carries out aerial spraying then.Before japanning, be rust-proofing primer with the epoxy zinc-rich rust-inhibiting paint earlier, be the middle layer lacquer carries out the lacquer processing of preceding road with the epoxy micaceous iron oxide rustproof paint.The amount of dilution of aerial spraying is 0-10% (in a paint weight), dilutes with 101 thinners well known in the art, and the bore of nozzle is 2.0-3.0mm, and air pressure is 0.3-0.4Mpa, application 1-2 road.
Be not more than 85% in relative humidity, the ground temperature is higher than under the condition of above 3 ℃ of dew point, treats the steel surface that being coated with of coating finish be equipped with preceding road lacquer with the chlorinated rubber finish paint of present embodiment preparation and carries out Airless spraying, and structure is as shown in table 3.
Table 3. chlorinated rubber finish paint Airless spraying result
| Sample | Volume solid % | Build μ m | Wet-film thickness μ m | Consumption g/m 2 |
| 1 | 44±3 | 70 | 159 | 223 |
| 2 | 42±3 | 70 | 167 | 235 |
| 3 | 42±3 | 40 | 94 | 120 |
| 4 | 42±3 | 71 | 169 | 238 |
| 5 | 40±3 | 40 | 100 | 127 |
| 6 | 42±3 | 70 | 165 | 234 |
| 7 | 42±3 | 70 | 165 | 232 |
| 8 | 42±3 | 70 | 167 | 234 |
| 9 | 40±3 | 40 | 101 | 128 |
Wherein, the volume solid is pressed GB/T9272 eqv ISO3233:1998 regulation mensuration.31 ℃ of flash-points.
Above-mentioned chlorinated rubber finish paint is measured time of drying under 25 ℃ of conditions, refer to do≤2h, does solid work≤12h.
5 ℃, 20 ℃ and 30 ℃ of overcoating pitch times of measuring the chlorinated rubber finish paint of present embodiment preparation down, experimental result is as shown in table 4 below respectively.
Table 4. overcoating pitch time
Through observation, but the knowledge capital invention has excellent water tolerance, weather resistance, non-corrosibility, weathering resistance and ornamental, and dryness is fast, safety and environmental protection.
Embodiment 3
Press following weight proportion (weight part):
After above-mentioned each component that takes by weighing mixed stirring, sand milling to fineness was qualified, obtains chlorinated rubber finish paint of the present invention.
Before adopting the present invention to carry out application, carry out surface treatment earlier, surface treatment is behind preceding road lacquer complete drying, eliminates greasy dirts all on the paint film and foreign material.The chlorinated rubber finish paint for preparing with method of the present invention then carries out Airless spraying, before japanning, is rust-proofing primer with aluminium powder chlorinated rubber rust-inhibiting paint earlier, is that the middle layer lacquer carries out the lacquer processing of preceding road with chlorinated rubber iron oxide red thick rust-inhibiting paint.The amount of dilution of Airless spraying is 0-5% (in a paint weight), dilutes with 101 thinners well known in the art, and the thickness of formation dry film is 70-140 μ m, and the bore of nozzle is 0.4-0.5mm, sprays too that power is 15-20Mpa, application 1-2 road.
Be not more than 85% in relative humidity, the ground temperature is higher than under the condition of above 3 ℃ of dew point, treats the steel surface that being coated with of coating finish be equipped with preceding road lacquer with the chlorinated rubber finish paint of present embodiment preparation and carries out Airless spraying, and structure is as shown in table 5.
Table 5. chlorinated rubber finish paint Airless spraying result
| Sample | Volume solid % | Build μ m | Wet-film thickness μ m | Consumption g/m 2 |
| 1 | 44±3 | 70 | 158 | 222 |
| 2 | 42±3 | 70 | 168 | 236 |
| 3 | 42±3 | 40 | 95 | 121 |
| 4 | 42±3 | 70 | 167 | 234 |
| 5 | 42±3 | 40 | 95 | 121 |
| 6 | 42±3 | 70 | 167 | 234 |
| 7 | 42±3 | 70 | 167 | 234 |
| 8 | 42±3 | 70 | 167 | 234 |
| 9 | 40±3 | 40 | 100 | 127 |
Wherein, the volume solid is pressed GB/T9272 eqv ISO3233:1998 regulation mensuration.31 ℃ of flash-points.
Above-mentioned chlorinated rubber finish paint is measured time of drying under 25 ℃ of conditions, refer to do≤2h, does solid work≤12h.
5 ℃, 20 ℃ and 30 ℃ of overcoating pitch times of measuring the chlorinated rubber finish paint of present embodiment preparation down, experimental result is as shown in table 6 below respectively.
Table 6. overcoating pitch time
Through observation, but the knowledge capital invention has excellent water tolerance, weather resistance, non-corrosibility, weathering resistance and ornamental, and dryness is fast, safety and environmental protection.
The present invention can once be sprayed and reach dry film 140 μ m when being adopted hydraulic spraying.Do not need repeatedly to spray.
The above is merely preferred embodiment of the present invention, is not to be used for limiting practical range of the present invention; If do not break away from the spirit and scope of the present invention, the present invention is made amendment or is equal to replacement, all should be encompassed in the middle of the protection domain of claim of the present invention.
Claims (9)
1. a chlorinated rubber finish paint is characterized in that, comprises the component of following weight proportion: white titanium pigment 10-30 part, YLENE 10-30 part, clorafin 10-20 part, chlorinated rubber 10-20 part, short change agent 6-12 part, coupling agent 2-8 part.
2. chlorinated rubber finish paint as claimed in claim 1 is characterized in that, said chlorinated rubber finish paint comprises the material of following weight proportion: 20 parts of white titanium pigments, 20 parts of YLENE, 15 parts of clorafins, 15 parts of chlorinated rubbers, short 9 parts of agent, 5 parts of the coupling agents of becoming.
3. according to claim 1 or claim 2 chlorinated rubber finish paint is characterized in that said short change agent is the 6900-20X polyamide wax.
4. chlorinated rubber finish paint as claimed in claim 3 is characterized in that, said coupling agent is positive titanic acid ester.
5. the preparation method of the described chlorinated rubber finish paint of claim 1 is characterized in that, said preparation method may further comprise the steps:
1) takes by weighing white titanium pigment, YLENE, clorafin, chlorinated rubber, short agent and the coupling agent of becoming;
2) each component that takes by weighing in the step 1) is mixed stirring, obtain the said chlorinated rubber finish paint of claim 1.
6. preparation method as claimed in claim 5 is characterized in that, the weight proportion of said each component is: white titanium pigment 10-30 part, YLENE 10-30 part, clorafin 10-20 part, chlorinated rubber 10-20 part, short change agent 6-12 part, coupling agent 2-8 part.
7. preparation method as claimed in claim 5 is characterized in that, the weight proportion of said each component is: 20 parts of white titanium pigments, 20 parts of YLENE, 15 parts of clorafins, 15 parts of chlorinated rubbers, short 9 parts of agent, 5 parts of the coupling agents of becoming.
8. like each described preparation method among the claim 5-7, it is characterized in that said short change agent is the 6900-20X polyamide wax.
9. preparation method as claimed in claim 8 is characterized in that, said coupling agent is positive titanic acid ester.
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| CN2011100807286A CN102433048A (en) | 2011-03-31 | 2011-03-31 | Chlorinated rubber finish and preparation method thereof |
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| CN2011100807286A CN102433048A (en) | 2011-03-31 | 2011-03-31 | Chlorinated rubber finish and preparation method thereof |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102898900A (en) * | 2012-09-28 | 2013-01-30 | 启东市华亚工业配套有限公司 | Rubber paint |
| CN104046110A (en) * | 2014-06-19 | 2014-09-17 | 吴江华诚复合材料科技有限公司 | Acid-alkali-resistant chlorinated rubber architectural coating |
| CN104194445A (en) * | 2014-09-19 | 2014-12-10 | 苏州洛特兰新材料科技有限公司 | Chlorinated rubber exterior wall coating |
| CN104212249A (en) * | 2014-09-24 | 2014-12-17 | 句容市给力包装制品厂 | Waterproof coating |
| CN105885651A (en) * | 2014-12-01 | 2016-08-24 | 黄传波 | Chlorinated rubber anticorrosive coating |
| CN105907200A (en) * | 2016-06-24 | 2016-08-31 | 无锡伊佩克科技有限公司 | Anti-rust primer for steel and preparation method thereof |
| CN107141894A (en) * | 2017-06-01 | 2017-09-08 | 冯智勇 | A kind of chlorinated rubber protective paint |
| CN111389693A (en) * | 2020-04-02 | 2020-07-10 | 安徽金誉材料股份有限公司 | Production process of hydrophilic aluminum foil for air conditioner |
| CN112094540A (en) * | 2020-09-25 | 2020-12-18 | 中昊北方涂料工业研究设计院有限公司 | Special rubber protective primer |
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| GB696087A (en) * | 1950-03-06 | 1953-08-26 | Ideal Chemical Products Inc | Improvements in or relating to coating composition |
| CN101024741A (en) * | 2007-02-09 | 2007-08-29 | 重庆大学 | Anti-corrosion anti-dirt method or biological anti-dirt and conductive anti-dirt combination |
| CN101155647A (en) * | 2005-04-05 | 2008-04-02 | 中国涂料株式会社 | Tie coat for organopolysiloxane antifouling coat, composite coats, and ships and underwater structures covered with the composite coats |
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- 2011-03-31 CN CN2011100807286A patent/CN102433048A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB696087A (en) * | 1950-03-06 | 1953-08-26 | Ideal Chemical Products Inc | Improvements in or relating to coating composition |
| CN101155647A (en) * | 2005-04-05 | 2008-04-02 | 中国涂料株式会社 | Tie coat for organopolysiloxane antifouling coat, composite coats, and ships and underwater structures covered with the composite coats |
| CN101024741A (en) * | 2007-02-09 | 2007-08-29 | 重庆大学 | Anti-corrosion anti-dirt method or biological anti-dirt and conductive anti-dirt combination |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102898900A (en) * | 2012-09-28 | 2013-01-30 | 启东市华亚工业配套有限公司 | Rubber paint |
| CN104046110A (en) * | 2014-06-19 | 2014-09-17 | 吴江华诚复合材料科技有限公司 | Acid-alkali-resistant chlorinated rubber architectural coating |
| CN104194445A (en) * | 2014-09-19 | 2014-12-10 | 苏州洛特兰新材料科技有限公司 | Chlorinated rubber exterior wall coating |
| CN104212249A (en) * | 2014-09-24 | 2014-12-17 | 句容市给力包装制品厂 | Waterproof coating |
| CN105885651A (en) * | 2014-12-01 | 2016-08-24 | 黄传波 | Chlorinated rubber anticorrosive coating |
| CN105907200A (en) * | 2016-06-24 | 2016-08-31 | 无锡伊佩克科技有限公司 | Anti-rust primer for steel and preparation method thereof |
| CN107141894A (en) * | 2017-06-01 | 2017-09-08 | 冯智勇 | A kind of chlorinated rubber protective paint |
| CN111389693A (en) * | 2020-04-02 | 2020-07-10 | 安徽金誉材料股份有限公司 | Production process of hydrophilic aluminum foil for air conditioner |
| CN112094540A (en) * | 2020-09-25 | 2020-12-18 | 中昊北方涂料工业研究设计院有限公司 | Special rubber protective primer |
| CN112094540B (en) * | 2020-09-25 | 2022-03-15 | 中昊北方涂料工业研究设计院有限公司 | Special rubber protective primer |
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Application publication date: 20120502 |