CN102418060A - Processing method for TC4 titanium alloy large-sized bar - Google Patents
Processing method for TC4 titanium alloy large-sized bar Download PDFInfo
- Publication number
- CN102418060A CN102418060A CN2011104117523A CN201110411752A CN102418060A CN 102418060 A CN102418060 A CN 102418060A CN 2011104117523 A CN2011104117523 A CN 2011104117523A CN 201110411752 A CN201110411752 A CN 201110411752A CN 102418060 A CN102418060 A CN 102418060A
- Authority
- CN
- China
- Prior art keywords
- forging
- fire
- less
- titanium alloy
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Forging (AREA)
Abstract
The invention discloses a processing method for a TC4 titanium alloy large-sized bar. The method comprises the following steps of: cogging and forging TC4 titanium alloy ingots for 2 to 3 heating times to obtain forging billets; 2, upsetting the forging billets repeatedly and performing drawing-out forging for 2 to 3 heating times; 3, upsetting the forging billets subjected to forging repeatedly and performing drawing-out forging for 3 to 5 heating times; and 4, performing chamfering round forging on the forging billets subjected to forging for 2 heating times to obtain the TC4 titanium alloy large-sized bar with the diameter of 200 to 400 mm and length of not less than 2,500 mm. The TC4 titanium alloy bar processed by the method has uniform and fine grains, few internal defects and high safety and accords with the domestic advanced level of the like products. In the processed TC4 titanium alloy bar, the room-temperature tensile strength is 920 to 960 MPa; the yield strength is 830 to 870 MPa; the elongation percentage is not less than 12 percent; the contraction ratio of the cross section is not less than 36 percent; flaw detection clutter reflects small signals; and the flaw detection level is high.
Description
Technical field
The invention belongs to the titanium alloy rod bar preparing technical field, be specifically related to a kind of working method of TC4 titanium alloy large size bar.
Background technology
Advantages such as titanium alloy has the specific tenacity height, resistance to corrosion is strong, high-temperature behavior is good, processability is good are the important materials that use in fields such as Aeronautics and Astronautics, weapons.Aircraft industry is the main application fields of titanium alloy, and TC4 is the maximum alloy designations of consumption, accounts for about 70% of titanium alloy ultimate production, is mainly used in the structural part of aircraft.Along with the development of aircraft industry, for safe reliability, prolongs life, the raising structure benefit that improves aircraft, the development trend of airplane design is to reduce welding; Load spare adopts heavy froging and large-scale integral forging, for satisfying development, the production of heavy froging and large-scale integral forging, needs to use high quality, large-size titanium alloy bar; Yet, at home in the above bar production method of TC4 titanium alloy Φ 100mm, for guaranteeing tissue, performance unanimity and meeting the requirements; Need below transformation temperature, carry out upsetting pull repeatedly forges; And the forged realization of upsetting pull is confined to axially owing to receive the restriction of upsetting pull forging method, make small deformation district and distortion dead band be organized in lesser temps the time all can not obtain effective refinement all the time; And homogeneity of structure is relatively poor; Thereby make that cycle length, the bar substance of the above bar production of domestic TC4 titanium alloy Φ 100mm are less, the quality product consistence is poor, and the UT rank is low.The diameter of rod of suitability for industrialized production and application is Φ 220mm to the maximum at present; Single Zhi Changdu only has about 1.5 meters; Be difficult to satisfy the demand in fields such as domestic and international Aeronautics and Astronautics, boat,, but still be confined to little blank upsetting pull technology repeatedly though domestic many units have carried out the development of the above scale rod bar of Φ 200mm; Bar length or substance are difficult to improve, and tissue, UT and quality conformance etc. require still to exist big gap.
Summary of the invention
Technical problem to be solved by this invention is the deficiency to above-mentioned prior art, provides a kind of method simple, does not need the large-tonnage forging equipment, can on the press of less tonnage, realize the working method of the TC4 titanium alloy large size bar of suitability for industrialized production.Adopting the TC4 titanium alloy rod bar room temperature tensile intensity of the inventive method processing is 920MPa～960MPa, and ys is 830MPa～870MPa, and unit elongation is not less than 12%, and relative reduction in area is not less than 36%, and the flaw detection clutter echo signal is less, and the flaw detection rank is high.
For solving the problems of the technologies described above, the technical scheme that the present invention adopts is: a kind of working method of TC4 titanium alloy large size bar is characterized in that this method may further comprise the steps:
Step 1, the TC4 titan alloy casting ingot that diameter is not less than 700mm are that 2～3 fire are forged in cogging under 1150 ℃～1200 ℃ the condition in temperature; Control every fire time forging ratio and be not less than 1.5; Total forging ratio is not less than 3, and every fire time final forging temperature all is not less than 900 ℃, obtains forging stock;
Step 2, be that 2～3 fire are forged in jumping-up and pulling repeatedly under 20 ℃～50 ℃ the condition more than the TC4 titan alloy casting ingot beta transformation point in temperature with forging stock described in the step 1; Controlling every fire time forging ratio is 1.5～1.8; Total forging ratio is not less than 3, and every fire time final forging temperature all is not less than 820 ℃;
Step 3, be that 3～5 fire are forged in jumping-up and pulling repeatedly under 20 ℃～30 ℃ the condition below the ingot casting beta transformation point in temperature with the forging stock after forging in the step 2; Control every fire time forging ratio and be not less than 1.5; The total forging ratio of two-phase region is not less than 6, and every fire time final forging temperature all is not less than 820 ℃;
Step 4, be round as a ball forging 2 fire of chamfered edge under 30 ℃～50 ℃ the condition below the ingot casting beta transformation point in temperature with the forging stock after forging in the step 3; Every fire time final forging temperature all is not less than 800 ℃; Obtaining diameter is 200mm～400mm, and length is not less than the TC4 titanium alloy rod bar of 2500mm.
The working method of above-mentioned a kind of TC4 titanium alloy large size bar is heated to the min of 1150 ℃～1200 ℃ and insulation (D/2+20) min～(D/2+40) with titan alloy casting ingot before every fire described in the step 1 time forges, and wherein D is the diameter of TC4 titan alloy casting ingot.
The working method of above-mentioned a kind of TC4 titanium alloy large size bar; Before every fire described in the step 2 time forges forging stock is heated to more than the TC4 titan alloy casting ingot beta transformation point min of 20 ℃～50 ℃ and insulation (L/2+20) min～(L/2+40), wherein L is the minimum length of side of the xsect of forging stock.
The working method of above-mentioned a kind of TC4 titanium alloy large size bar adopts the switching-over pier to pull out mode in jumping-up and the pulling forging process described in the step 3 repeatedly, and it is different that the pier that wherein commutates pulls out the direction that is meant each jumping-up and pulling.
The working method of above-mentioned a kind of TC4 titanium alloy large size bar; Before every fire described in the step 3 time forges with forging stock be heated to below the TC4 titan alloy casting ingot beta transformation point 20 ℃～30 ℃ and insulation (L '/2+20) min～(L '/2+40) min, wherein L ' is the minimum length of side of the xsect of forging stock.
Below the working method of above-mentioned a kind of TC4 titanium alloy large size bar, the forging stock water-cooled to 300 after will forging after every fire described in the step 3 time forges ℃.
The working method of above-mentioned a kind of TC4 titanium alloy large size bar, the round as a ball forged every fire of chamfered edge described in the step 4 time deflection is 25%～35%.
The present invention compared with prior art has the following advantages:
1, the inventive method is simple, does not need the large-tonnage forging equipment, can on the press of less tonnage, realize suitability for industrialized production.
2, the present invention can make that through three vacuum consumable electrode arc furnace meltings the ingot casting composition is more even, and segregation is little, and the ingot casting subsurface defect is few simultaneously, and at the bottom of excision rising head and the ingot, helps getting rid of in advance the influence of ingot casting melting defective to subsequent production.
3, the present invention adopts the mode that the high temperature upsetting pull+the switching-over upsetting pull combines, and can effectively eliminate or reduce the small deformation district and be out of shape the dead band to organizing conforming influence, helps improving the homogeneity of structure of blank.
4, adopt the big specification TC4 titanium alloy rod uniform crystal particles, tiny of the inventive method processing, subsurface defect is few, and is safe, and constant product quality property is good, helps high standard flaw detection requirement, meets the like product advanced international level.
5, adopting the TC4 titanium alloy rod bar room temperature tensile intensity of the inventive method processing is 920MPa～960MPa; Ys is 830MPa～870MPa, and unit elongation is not less than 12%, and relative reduction in area is not less than 36%; The flaw detection clutter echo signal is less, and the flaw detection rank is high.
Through embodiment, technical scheme of the present invention is done further detailed description below.
Embodiment
Embodiment 1
Present embodiment employing diameter is that the TC4 titan alloy casting ingot of Φ 700mm is that raw material processing diameter is the TC4 titanium alloy rod bar of Φ 250mm, and working method is specific as follows:
Step 1, to use the 2500T oil press be that 2 fire are forged in cogging under 1150 ℃ the condition in temperature with the TC4 titan alloy casting ingot of Φ 700mm, and the forging ratio of controlling every fire time is 1.5, and final forging temperature all is not less than 900 ℃, obtains the forging stock of 400mm * 400mm * 850mm; Before forging, said every fire time ingot casting is heated to 1150 ℃ and be incubated 390min with gas furnace;
Step 2, with the 2500T oil press with 400mm * 400mm described in the step 1 * 850mm forging stock temperature be more than the ingot casting beta transformation point under 20 ℃ the condition repeatedly jumping-up forge 2 fire with pulling; Control the inferior forging ratio of every fire and be 1.5, final forging temperature all is not less than 820 ℃; Before forging, said every fire time forging stock is heated to more than the ingot casting beta transformation point 20 ℃ and be incubated 240min with electric furnace;
Step 3, with the 2500T oil press with the 400mm * 400mm * 850mm forging stock after forging in the step 2 temperature be adopt under 30 ℃ the condition below the ingot casting beta transformation point switching-over pier pull out mode repeatedly jumping-up forge 3 fire with pulling; Each fire time forging ratio is 3, and every fire time final forging temperature all is not less than 820 ℃; Before said every fire time forges forging stock is heated to below the ingot casting beta transformation point 30 ℃ and be incubated 240min, below the forging stock water-cooled to 300 after will forging after every fire forges ℃; It is different that said switching-over pier pulls out the direction that is meant each jumping-up and pulling;
Step 4, be round as a ball forging 1 fire of chamfered edge under 30 ℃ the condition below the ingot casting beta transformation point in temperature with the forging stock after forging in the step 3; The forging deformation amount is 35%; Overhaul, be to forge 1 fire under 40 ℃ the condition below the ingot casting beta transformation point in temperature once more after the reconditioning, the forging deformation amount is 30%, and every fire time final forging temperature all is not less than 800 ℃; Obtaining diameter is 250mm, and length is the TC4 titanium alloy rod bar of 2500mm.
Embodiment 2
Present embodiment employing diameter is that the TC4 titan alloy casting ingot of Φ 700mm is that raw material processing diameter is the TC4 titanium alloy rod bar of Φ 200mm, and working method is specific as follows:
Step 1, to use the 2500T oil press be that 2 fire are forged in cogging under 1200 ℃ the condition in temperature as the TC4 titan alloy casting ingot of Φ 700mm with diameter; Control the inferior forging ratio of every fire and be 1.5; Final forging temperature all is not less than 900 ℃, obtains 380mm * 380mm * 760mm forging stock; Before said every fire time forges with gas furnace with ingot casting zone heating to 1200 ℃ and be incubated 370min;
Step 2, with the 2500T oil press with 380mm * 380mm described in the step 1 * 760mm forging stock temperature be more than the ingot casting beta transformation point under 30 ℃ the condition repeatedly jumping-up forge 3 fire with pulling; The inferior forging ratio of each fire is followed successively by 1.8,1.7 and 1.5, and final forging temperature all is not less than 820 ℃; Before forging, said every fire time forging stock is heated to more than the ingot casting beta transformation point 30 ℃ and be incubated 210min with electric furnace;
Step 3, with the 2500T oil press with the 380mm * 380mm * 760mm forging stock after forging in the step 2 temperature be adopt under 25 ℃ the condition below the ingot casting beta transformation point switching-over pier pull out mode repeatedly jumping-up forge 4 fire with pulling; Each fire time forging ratio is followed successively by 3,3,3 and 1.6, and every fire time final forging temperature all is not less than 820 ℃; Before said every fire time forges forging stock is heated to below the ingot casting beta transformation point 25 ℃ and be incubated 210min, below the forging stock water-cooled to 300 after will forging after every fire forges ℃; It is different that said switching-over pier pulls out the direction that is meant each jumping-up and pulling;
Step 4, be round as a ball forging 1 fire of chamfered edge under 40 ℃ the condition below the ingot casting beta transformation point in temperature with the forging stock after forging in the step 3; The forging deformation amount is 35%; Overhaul, be to forge 1 fire under 50 ℃ the condition below the ingot casting beta transformation point in temperature once more after the reconditioning, the forging deformation amount is 30%, and every fire time final forging temperature all is not less than 800 ℃; Obtaining diameter is 200mm, and length is the TC4 titanium alloy rod bar of 3000mm.
Embodiment 3
Present embodiment employing diameter is that the TC4 titan alloy casting ingot of Φ 800mm is that raw material processing diameter is the TC4 titanium alloy rod bar of Φ 400mm, and working method is specific as follows:
Step 1, to use the 3150T oil press be that 3 fire are forged in cogging under 1180 ℃ the condition in temperature with the TC4 titan alloy casting ingot of Φ 800mm; The inferior forging ratio of each fire is followed successively by 2.6,2.4 and 1.5; Final forging temperature all is not less than 900 ℃, obtains 580mm * 580mm * 1200mm forging stock; Before forging, said every fire time ingot casting is heated to 1180 ℃ and be incubated 430min with gas furnace;
Step 2, with the 3150T oil press with 580mm * 580mm described in the step 1 * 1200mm forging stock temperature be more than the ingot casting beta transformation point under 50 ℃ the condition repeatedly jumping-up forge 3 fire with pulling; The inferior forging ratio of each fire is followed successively by 1.8,1.7 and 1.5, and final forging temperature all is not less than 820 ℃; Before forging, said every fire time forging stock is heated to more than the ingot casting beta transformation point 50 ℃ and be incubated 320min with electric furnace;
Step 3, with the 3150T oil press with the 580mm * 580mm * 1200mm forging stock after forging in the step 2 temperature be adopt under 20 ℃ the condition below the ingot casting beta transformation point switching-over pier pull out mode repeatedly jumping-up forge 5 fire with pulling; Each fire time forging ratio is followed successively by 1.8,1.6,1.8,1.6 and 1.5, and every fire time final forging temperature all is not less than 820 ℃; Before said every fire time forges forging stock is heated to below the ingot casting beta transformation point 20 ℃ and be incubated 320min, below the forging stock water-cooled to 300 after will forging after every fire forges ℃; It is different that said switching-over pier pulls out the direction that is meant each jumping-up and pulling;
Step 4, be round as a ball forging 1 fire of chamfered edge under 30 ℃ the condition below the ingot casting beta transformation point in temperature with the forging stock after forging in the step 3; The forging deformation amount is 35%; Overhaul, be to forge 1 fire under 30 ℃ the condition below the ingot casting beta transformation point in temperature once more after the reconditioning, the forging deformation amount is 25%, and every fire time final forging temperature all is not less than 800 ℃; Obtaining diameter is 400mm, and length is the TC4 titanium alloy rod bar of 3000mm.
The present invention carries out conventional thermal treatment and machining to the TC4 titanium alloy rod bar of embodiment 1 to embodiment 3 processing, then the bar after the machining is carried out Performance Detection, and the result sees the following form:
The performance test results of the bar of table 1 embodiment 1 to embodiment 3 processing
Can find out that from table 1 adopting the TC4 titanium alloy large size bar room temperature tensile intensity of the inventive method processing is 920MPa～960MPa, ys is 830MPa～870MPa, and unit elongation is not less than 12%, and relative reduction in area is not less than 36%.
The present invention observes the macrostructure of the TC4 titanium alloy rod bar of embodiment 1 to embodiment 3 processing, and the horizontal macrostructure of bar is even, does not see abnormal structures such as coarse-grain, is organized as fuzzy uniformly brilliant; And the mirco structure of many places different positionss such as central position, bar transverse section, 1/4R position, 1/2R position, 3/4R position and limit location analyzed contrast, the result shows that to adopt the bar homogeneity of structure of method processing of the present invention better.
With 5,000,000 probes, full sound path carries out UT to the TC4 titanium alloy rod bar of embodiment 1 to embodiment 3 processing in the present invention, and all through Φ 2.0mm flat-bottom hole, the clutter level be-9db～-6db, the clutter echo signal of detecting a flaw is less, the rank of detecting a flaw height.
The above; It only is preferred embodiment of the present invention; Be not that the present invention is done any restriction, every according to inventing technical spirit to any simple modification, change and equivalent structure variation that above embodiment did, all still belong in the protection domain of technical scheme of the present invention.
Claims (7)
1. the working method of a TC4 titanium alloy large size bar is characterized in that, this method may further comprise the steps:
Step 1, the TC4 titan alloy casting ingot that diameter is not less than 700mm are that 2～3 fire are forged in cogging under 1150 ℃～1200 ℃ the condition in temperature; Control every fire time forging ratio and be not less than 1.5; Total forging ratio is not less than 3, and every fire time final forging temperature all is not less than 900 ℃, obtains forging stock;
Step 2, be that 2～3 fire are forged in jumping-up and pulling repeatedly under 20 ℃～50 ℃ the condition more than the TC4 titan alloy casting ingot beta transformation point in temperature with forging stock described in the step 1; Controlling every fire time forging ratio is 1.5～1.8; Total forging ratio is not less than 3, and every fire time final forging temperature all is not less than 820 ℃;
Step 3, be that 3～5 fire are forged in jumping-up and pulling repeatedly under 20 ℃～30 ℃ the condition below the ingot casting beta transformation point in temperature with the forging stock after forging in the step 2; Control every fire time forging ratio and be not less than 1.5; The total forging ratio of two-phase region is not less than 6, and every fire time final forging temperature all is not less than 820 ℃;
Step 4, be round as a ball forging 2 fire of chamfered edge under 30 ℃～50 ℃ the condition below the ingot casting beta transformation point in temperature with the forging stock after forging in the step 3; Every fire time final forging temperature all is not less than 800 ℃; Obtaining diameter is 200mm～400mm, and length is not less than the TC4 titanium alloy rod bar of 2500mm.
2. the working method of a kind of TC4 titanium alloy large size bar according to claim 1; It is characterized in that; Before every fire described in the step 1 time forges titan alloy casting ingot is heated to the min of 1150 ℃～1200 ℃ and insulation (D/2+20) min～(D/2+40), wherein D is the diameter of TC4 titan alloy casting ingot.
3. the working method of a kind of TC4 titanium alloy large size bar according to claim 1; It is characterized in that; Before every fire described in the step 2 time forges forging stock is heated to more than the TC4 titan alloy casting ingot beta transformation point min of 20 ℃～50 ℃ and insulation (L/2+20) min～(L/2+40), wherein L is the length of side of the xsect of forging stock.
4. the working method of a kind of TC4 titanium alloy large size bar according to claim 1; It is characterized in that; Adopt the switching-over pier to pull out mode in jumping-up and the pulling forging process repeatedly described in the step 3, it is different that the pier that wherein commutates pulls out the direction that is meant each jumping-up and pulling.
5. the working method of a kind of TC4 titanium alloy large size bar according to claim 1; It is characterized in that; Before every fire described in the step 3 time forges with forging stock be heated to below the TC4 titan alloy casting ingot beta transformation point 20 ℃～30 ℃ and insulation (L '/2+20) min～(L '/2+40) min, wherein L ' is the length of side of the xsect of forging stock.
6. the working method of a kind of TC4 titanium alloy large size bar according to claim 1 is characterized in that, below the forging stock water-cooled to 300 after will forging after every fire described in the step 3 time forges ℃.
7. the working method of a kind of TC4 titanium alloy large size bar according to claim 1 is characterized in that, the round as a ball forged every fire of chamfered edge described in the step 4 time deflection is 25%～35%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011104117523A CN102418060A (en) | 2011-12-12 | 2011-12-12 | Processing method for TC4 titanium alloy large-sized bar |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011104117523A CN102418060A (en) | 2011-12-12 | 2011-12-12 | Processing method for TC4 titanium alloy large-sized bar |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN102418060A true CN102418060A (en) | 2012-04-18 |
Family
ID=45942703
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2011104117523A Pending CN102418060A (en) | 2011-12-12 | 2011-12-12 | Processing method for TC4 titanium alloy large-sized bar |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102418060A (en) |
Cited By (43)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102912270A (en) * | 2012-11-12 | 2013-02-06 | 西部钛业有限责任公司 | Hot-working process capable of improving cogging for titanium alloy cast ingot |
| CN102925650A (en) * | 2012-11-06 | 2013-02-13 | 西部钛业有限责任公司 | Method for manufacturing TA19 titanium alloy large-size bar |
| CN102922239A (en) * | 2012-11-13 | 2013-02-13 | 西部钛业有限责任公司 | Preparation method for TA5 titanium alloy bars with small specifications |
| CN102994922A (en) * | 2013-01-01 | 2013-03-27 | 西部钛业有限责任公司 | Preparation method of TA7 titanium alloy cake |
| CN103045906A (en) * | 2012-12-24 | 2013-04-17 | 洛阳双瑞精铸钛业有限公司 | Process method of producing high-grade TC4 alloy hot rolled plate with high material-obtaining rate and low cost |
| CN103510030A (en) * | 2013-09-23 | 2014-01-15 | 西北有色金属研究院 | Preparation method of TC21 titanium alloy large-specification bar |
| CN103938137A (en) * | 2014-04-08 | 2014-07-23 | 中国航空工业集团公司北京航空材料研究院 | Method for changing structure uniformity of large-specification titanium alloy bar |
| CN104070125A (en) * | 2014-03-11 | 2014-10-01 | 宁夏东方钽业股份有限公司 | Forging machining method of large-sized bar materials of TC4 (Ti-6Al-4V) titanium alloy |
| CN104722689A (en) * | 2015-03-16 | 2015-06-24 | 无锡市派克重型铸锻有限公司 | Large size aluminum alloy keelblook homogenization forging improving method |
| CN104762576A (en) * | 2015-04-24 | 2015-07-08 | 西北有色金属研究院 | Method for manufacturing TC18 titanium alloy whole basket-weave microstructure medium-specification ultra-long bars |
| CN104841830A (en) * | 2015-05-21 | 2015-08-19 | 西部超导材料科技股份有限公司 | Method for manufacturing TC4-DT titanium alloy large-size forged blanks |
| CN103586380B (en) * | 2013-11-08 | 2015-09-16 | 中国航空工业集团公司北京航空材料研究院 | A kind of ingot formation Forging Technology improving titanium alloy forging stock structural homogenity |
| CN104959506A (en) * | 2015-05-21 | 2015-10-07 | 西部超导材料科技股份有限公司 | Preparation method of hard-deformation non-burning titanium alloy boards |
| CN105063527A (en) * | 2015-07-28 | 2015-11-18 | 西部超导材料科技股份有限公司 | Preparation method of alpha titanium alloy forging stock |
| CN107282687A (en) * | 2017-05-22 | 2017-10-24 | 西部超导材料科技股份有限公司 | A kind of preparation method of Ti6Al4V titanium alloys fine grain bar |
| RU2644714C2 (en) * | 2015-12-22 | 2018-02-13 | Акционерное Общество "Чепецкий Механический Завод" (Ао Чмз) | Method for manufacturing rods of titanium based alloys |
| CN107760925A (en) * | 2017-11-10 | 2018-03-06 | 西北有色金属研究院 | A kind of preparation method of high-strength modified Ti 6Al 4V titanium alloy large size bars |
| CN108044007A (en) * | 2017-12-05 | 2018-05-18 | 西部超导材料科技股份有限公司 | A kind of forging method of high uniform Ti632211 titanium alloy plates |
| CN108097852A (en) * | 2017-12-18 | 2018-06-01 | 西安赛特思迈钛业有限公司 | A kind of forging method of TC4 titanium alloy large sizes bar |
| CN109226621A (en) * | 2018-10-24 | 2019-01-18 | 湖南金天钛业科技有限公司 | A kind of forging method of larger ratio of height to diameter titan alloy casting ingot |
| CN109252061A (en) * | 2018-09-30 | 2019-01-22 | 中国科学院金属研究所 | A kind of preparation method of high temperature, high thermal stability, high-fracture toughness titanium alloy rod bar |
| CN109439936A (en) * | 2018-12-19 | 2019-03-08 | 宝钛集团有限公司 | The preparation method of strong toughness titanium alloy super large-scale ring material in a kind of |
| CN109622833A (en) * | 2018-12-11 | 2019-04-16 | 陕西宏远航空锻造有限责任公司 | A kind of structural homogeneity control method of big thickness Ti-6Al-2Sn-4Zr-2Mo alloy forged piece |
| CN109946947A (en) * | 2019-05-08 | 2019-06-28 | 东莞得利钟表有限公司 | A kind of black titanium clock and watch gadget of high-strength corrosion-resistant and its manufacture craft |
| CN110592508A (en) * | 2019-09-12 | 2019-12-20 | 中国航发北京航空材料研究院 | Low-cost and high-performance titanium alloy short-process forging process |
| CN110722014A (en) * | 2019-10-21 | 2020-01-24 | 青岛理工大学 | Preparation method and application of Nb ingot blank and Nb rod |
| CN111057903A (en) * | 2019-12-09 | 2020-04-24 | 湖南湘投金天科技集团有限责任公司 | Large-size titanium alloy locking ring and preparation method thereof |
| CN111136473A (en) * | 2019-12-12 | 2020-05-12 | 西安圣泰金属材料有限公司 | Low-cost efficient preparation method of two-phase titanium alloy round bar |
| CN111286686A (en) * | 2020-04-09 | 2020-06-16 | 西部钛业有限责任公司 | Short-process preparation method of TC4 titanium alloy large-size bar with fine equiaxial structure |
| CN111390079A (en) * | 2020-03-13 | 2020-07-10 | 中铝沈阳有色金属加工有限公司 | Preparation method of ultra-large TC4 alloy cake |
| CN111889598A (en) * | 2020-08-07 | 2020-11-06 | 攀钢集团攀枝花钛材有限公司江油分公司 | TC4 titanium alloy forged material and preparation method thereof |
| CN112139413A (en) * | 2020-09-04 | 2020-12-29 | 中国航发北京航空材料研究院 | Forging method for improving texture and texture uniformity of TC18 titanium alloy large-size bar |
| CN112371886A (en) * | 2020-09-12 | 2021-02-19 | 武汉第二船舶设计研究所(中国船舶重工集团公司第七一九研究所) | Forging method of large-size titanium alloy bar blank for gas cylinder |
| CN112692096A (en) * | 2020-12-16 | 2021-04-23 | 西部钛业有限责任公司 | Preparation method of arc TC4 titanium alloy plate blank |
| CN112828222A (en) * | 2020-12-30 | 2021-05-25 | 西安西工大超晶科技发展有限责任公司 | Preparation method of multi-component titanium alloy forging |
| CN113182476A (en) * | 2021-04-28 | 2021-07-30 | 西部钛业有限责任公司 | Preparation method of high-strength TC11 titanium alloy forging |
| CN113579133A (en) * | 2020-04-30 | 2021-11-02 | 宝武特种冶金有限公司 | Free forging method for uniformly controlling titanium alloy structure |
| CN114309406A (en) * | 2020-09-29 | 2022-04-12 | 中国航发商用航空发动机有限责任公司 | Ti6242 titanium alloy disc and preparation method thereof |
| CN114433765A (en) * | 2022-02-08 | 2022-05-06 | 西部钛业有限责任公司 | Preparation method of high-toughness TA31 titanium alloy material |
| CN114769478A (en) * | 2021-11-16 | 2022-07-22 | 湖南金天钛业科技有限公司 | Forging method for improving axial structure uniformity of large titanium alloy bar |
| CN114850368A (en) * | 2022-06-14 | 2022-08-05 | 西部钛业有限责任公司 | Preparation method of ultra-large TC4 titanium alloy bar with high flaw detection requirement |
| CN115740306A (en) * | 2022-08-29 | 2023-03-07 | 西部超导材料科技股份有限公司 | Preparation method of Ti6Al4V titanium alloy bar |
| CN116240477A (en) * | 2023-03-02 | 2023-06-09 | 宝鸡市永盛泰钛业有限公司 | Technical method for low-cost titanium and titanium alloy forging products |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101157172A (en) * | 2007-10-19 | 2008-04-09 | 宝鸡市英耐特医用钛有限公司 | Method of preparing medical high-precision titanium and titanium alloy rod bar |
| CN101476096A (en) * | 2008-11-21 | 2009-07-08 | 宝鸡钛业股份有限公司 | Method for processing Ti-6Al-4V titanium alloy large size bar material |
| CN102230145A (en) * | 2011-06-20 | 2011-11-02 | 西部钛业有限责任公司 | Method for producing TC25 two-phase titanium alloy rod material with large specification |
-
2011
- 2011-12-12 CN CN2011104117523A patent/CN102418060A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101157172A (en) * | 2007-10-19 | 2008-04-09 | 宝鸡市英耐特医用钛有限公司 | Method of preparing medical high-precision titanium and titanium alloy rod bar |
| CN101476096A (en) * | 2008-11-21 | 2009-07-08 | 宝鸡钛业股份有限公司 | Method for processing Ti-6Al-4V titanium alloy large size bar material |
| CN102230145A (en) * | 2011-06-20 | 2011-11-02 | 西部钛业有限责任公司 | Method for producing TC25 two-phase titanium alloy rod material with large specification |
Non-Patent Citations (1)
| Title |
|---|
| 阎彩文等: "TC4钛合金异形锻件锻造工艺探索", 《钛工业进展》 * |
Cited By (60)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102925650A (en) * | 2012-11-06 | 2013-02-13 | 西部钛业有限责任公司 | Method for manufacturing TA19 titanium alloy large-size bar |
| CN102912270B (en) * | 2012-11-12 | 2014-05-07 | 西部钛业有限责任公司 | Hot-working process capable of improving cogging for titanium alloy cast ingot |
| CN102912270A (en) * | 2012-11-12 | 2013-02-06 | 西部钛业有限责任公司 | Hot-working process capable of improving cogging for titanium alloy cast ingot |
| CN102922239A (en) * | 2012-11-13 | 2013-02-13 | 西部钛业有限责任公司 | Preparation method for TA5 titanium alloy bars with small specifications |
| CN103045906A (en) * | 2012-12-24 | 2013-04-17 | 洛阳双瑞精铸钛业有限公司 | Process method of producing high-grade TC4 alloy hot rolled plate with high material-obtaining rate and low cost |
| CN102994922A (en) * | 2013-01-01 | 2013-03-27 | 西部钛业有限责任公司 | Preparation method of TA7 titanium alloy cake |
| CN102994922B (en) * | 2013-01-01 | 2014-09-17 | 西部钛业有限责任公司 | Preparation method of TA7 titanium alloy cake |
| CN103510030B (en) * | 2013-09-23 | 2015-08-05 | 西北有色金属研究院 | A kind of preparation method of TC21 titanium alloy large size bar |
| CN103510030A (en) * | 2013-09-23 | 2014-01-15 | 西北有色金属研究院 | Preparation method of TC21 titanium alloy large-specification bar |
| CN103586380B (en) * | 2013-11-08 | 2015-09-16 | 中国航空工业集团公司北京航空材料研究院 | A kind of ingot formation Forging Technology improving titanium alloy forging stock structural homogenity |
| CN104070125A (en) * | 2014-03-11 | 2014-10-01 | 宁夏东方钽业股份有限公司 | Forging machining method of large-sized bar materials of TC4 (Ti-6Al-4V) titanium alloy |
| CN104070125B (en) * | 2014-03-11 | 2016-08-17 | 宁夏东方钽业股份有限公司 | A kind of forging processing method of TC4 titanium alloy large size bar |
| CN103938137A (en) * | 2014-04-08 | 2014-07-23 | 中国航空工业集团公司北京航空材料研究院 | Method for changing structure uniformity of large-specification titanium alloy bar |
| CN103938137B (en) * | 2014-04-08 | 2016-01-06 | 中国航空工业集团公司北京航空材料研究院 | A kind of method changing titanium alloy large size bar homogeneity of structure |
| CN104722689A (en) * | 2015-03-16 | 2015-06-24 | 无锡市派克重型铸锻有限公司 | Large size aluminum alloy keelblook homogenization forging improving method |
| CN104762576A (en) * | 2015-04-24 | 2015-07-08 | 西北有色金属研究院 | Method for manufacturing TC18 titanium alloy whole basket-weave microstructure medium-specification ultra-long bars |
| CN104762576B (en) * | 2015-04-24 | 2016-10-12 | 西北有色金属研究院 | The preparation method of TC18 titanium alloy the whole network basket tissue medium format overlength bar |
| CN104841830A (en) * | 2015-05-21 | 2015-08-19 | 西部超导材料科技股份有限公司 | Method for manufacturing TC4-DT titanium alloy large-size forged blanks |
| CN104959506A (en) * | 2015-05-21 | 2015-10-07 | 西部超导材料科技股份有限公司 | Preparation method of hard-deformation non-burning titanium alloy boards |
| CN105063527A (en) * | 2015-07-28 | 2015-11-18 | 西部超导材料科技股份有限公司 | Preparation method of alpha titanium alloy forging stock |
| RU2644714C2 (en) * | 2015-12-22 | 2018-02-13 | Акционерное Общество "Чепецкий Механический Завод" (Ао Чмз) | Method for manufacturing rods of titanium based alloys |
| CN107282687A (en) * | 2017-05-22 | 2017-10-24 | 西部超导材料科技股份有限公司 | A kind of preparation method of Ti6Al4V titanium alloys fine grain bar |
| CN107282687B (en) * | 2017-05-22 | 2019-05-24 | 西部超导材料科技股份有限公司 | A kind of preparation method of Ti6Al4V titanium alloy fine grain bar |
| CN107760925A (en) * | 2017-11-10 | 2018-03-06 | 西北有色金属研究院 | A kind of preparation method of high-strength modified Ti 6Al 4V titanium alloy large size bars |
| CN107760925B (en) * | 2017-11-10 | 2018-12-18 | 西北有色金属研究院 | A kind of preparation method of high-strength modified Ti-6Al-4V titanium alloy large size bar |
| CN108044007A (en) * | 2017-12-05 | 2018-05-18 | 西部超导材料科技股份有限公司 | A kind of forging method of high uniform Ti632211 titanium alloy plates |
| CN108097852A (en) * | 2017-12-18 | 2018-06-01 | 西安赛特思迈钛业有限公司 | A kind of forging method of TC4 titanium alloy large sizes bar |
| CN109252061A (en) * | 2018-09-30 | 2019-01-22 | 中国科学院金属研究所 | A kind of preparation method of high temperature, high thermal stability, high-fracture toughness titanium alloy rod bar |
| CN109226621A (en) * | 2018-10-24 | 2019-01-18 | 湖南金天钛业科技有限公司 | A kind of forging method of larger ratio of height to diameter titan alloy casting ingot |
| CN109622833A (en) * | 2018-12-11 | 2019-04-16 | 陕西宏远航空锻造有限责任公司 | A kind of structural homogeneity control method of big thickness Ti-6Al-2Sn-4Zr-2Mo alloy forged piece |
| CN109439936A (en) * | 2018-12-19 | 2019-03-08 | 宝钛集团有限公司 | The preparation method of strong toughness titanium alloy super large-scale ring material in a kind of |
| CN109946947A (en) * | 2019-05-08 | 2019-06-28 | 东莞得利钟表有限公司 | A kind of black titanium clock and watch gadget of high-strength corrosion-resistant and its manufacture craft |
| CN110592508A (en) * | 2019-09-12 | 2019-12-20 | 中国航发北京航空材料研究院 | Low-cost and high-performance titanium alloy short-process forging process |
| CN110722014A (en) * | 2019-10-21 | 2020-01-24 | 青岛理工大学 | Preparation method and application of Nb ingot blank and Nb rod |
| CN111057903A (en) * | 2019-12-09 | 2020-04-24 | 湖南湘投金天科技集团有限责任公司 | Large-size titanium alloy locking ring and preparation method thereof |
| CN111136473A (en) * | 2019-12-12 | 2020-05-12 | 西安圣泰金属材料有限公司 | Low-cost efficient preparation method of two-phase titanium alloy round bar |
| CN111390079A (en) * | 2020-03-13 | 2020-07-10 | 中铝沈阳有色金属加工有限公司 | Preparation method of ultra-large TC4 alloy cake |
| CN111286686B (en) * | 2020-04-09 | 2021-09-10 | 西部钛业有限责任公司 | Short-process preparation method of TC4 titanium alloy large-size bar with fine equiaxial structure |
| CN111286686A (en) * | 2020-04-09 | 2020-06-16 | 西部钛业有限责任公司 | Short-process preparation method of TC4 titanium alloy large-size bar with fine equiaxial structure |
| CN113579133A (en) * | 2020-04-30 | 2021-11-02 | 宝武特种冶金有限公司 | Free forging method for uniformly controlling titanium alloy structure |
| CN111889598A (en) * | 2020-08-07 | 2020-11-06 | 攀钢集团攀枝花钛材有限公司江油分公司 | TC4 titanium alloy forged material and preparation method thereof |
| CN112139413A (en) * | 2020-09-04 | 2020-12-29 | 中国航发北京航空材料研究院 | Forging method for improving texture and texture uniformity of TC18 titanium alloy large-size bar |
| CN112371886B (en) * | 2020-09-12 | 2023-01-10 | 武汉第二船舶设计研究所(中国船舶重工集团公司第七一九研究所) | Forging method of large-size titanium alloy bar blank for gas cylinder |
| CN112371886A (en) * | 2020-09-12 | 2021-02-19 | 武汉第二船舶设计研究所(中国船舶重工集团公司第七一九研究所) | Forging method of large-size titanium alloy bar blank for gas cylinder |
| CN114309406A (en) * | 2020-09-29 | 2022-04-12 | 中国航发商用航空发动机有限责任公司 | Ti6242 titanium alloy disc and preparation method thereof |
| CN114309406B (en) * | 2020-09-29 | 2023-08-08 | 中国航发商用航空发动机有限责任公司 | Ti6242 titanium alloy disc and preparation method thereof |
| CN112692096A (en) * | 2020-12-16 | 2021-04-23 | 西部钛业有限责任公司 | Preparation method of arc TC4 titanium alloy plate blank |
| CN112692096B (en) * | 2020-12-16 | 2022-07-08 | 西部钛业有限责任公司 | Preparation method of arc TC4 titanium alloy plate blank |
| CN112828222A (en) * | 2020-12-30 | 2021-05-25 | 西安西工大超晶科技发展有限责任公司 | Preparation method of multi-component titanium alloy forging |
| CN113182476A (en) * | 2021-04-28 | 2021-07-30 | 西部钛业有限责任公司 | Preparation method of high-strength TC11 titanium alloy forging |
| CN113182476B (en) * | 2021-04-28 | 2023-10-13 | 西部钛业有限责任公司 | Preparation method of high-strength TC11 titanium alloy forging |
| CN114769478A (en) * | 2021-11-16 | 2022-07-22 | 湖南金天钛业科技有限公司 | Forging method for improving axial structure uniformity of large titanium alloy bar |
| CN114769478B (en) * | 2021-11-16 | 2023-08-18 | 湖南湘投金天钛业科技股份有限公司 | Forging method for improving uniformity of axial structure of titanium alloy large-sized bar |
| CN114433765B (en) * | 2022-02-08 | 2023-05-05 | 西部钛业有限责任公司 | Preparation method of high-strength and high-toughness TA31 titanium alloy material |
| CN114433765A (en) * | 2022-02-08 | 2022-05-06 | 西部钛业有限责任公司 | Preparation method of high-toughness TA31 titanium alloy material |
| CN114850368A (en) * | 2022-06-14 | 2022-08-05 | 西部钛业有限责任公司 | Preparation method of ultra-large TC4 titanium alloy bar with high flaw detection requirement |
| CN114850368B (en) * | 2022-06-14 | 2023-04-11 | 西部钛业有限责任公司 | Preparation method of ultra-large TC4 titanium alloy bar with high flaw detection requirement |
| CN115740306A (en) * | 2022-08-29 | 2023-03-07 | 西部超导材料科技股份有限公司 | Preparation method of Ti6Al4V titanium alloy bar |
| CN115740306B (en) * | 2022-08-29 | 2023-12-19 | 西部超导材料科技股份有限公司 | Preparation method of Ti6Al4V titanium alloy bar |
| CN116240477A (en) * | 2023-03-02 | 2023-06-09 | 宝鸡市永盛泰钛业有限公司 | Technical method for low-cost titanium and titanium alloy forging products |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102418060A (en) | Processing method for TC4 titanium alloy large-sized bar | |
| CN101476096B (en) | Method for processing Ti-6Al-4V titanium alloy large size bar material | |
| CN104070125B (en) | A kind of forging processing method of TC4 titanium alloy large size bar | |
| CN110935827B (en) | Forging method of large-specification fine-grain austenitic stainless steel SNCrW bar | |
| CN102513479A (en) | Production process for large-diameter fine isometric crystal tissue titanium alloy bar | |
| CN111304493B (en) | Superstrong high-plasticity titanium alloy and preparation method thereof | |
| CN103060733B (en) | Method for preparing large-size TC2 titanium alloy bars | |
| CN102000954A (en) | Method for manufacturing continuous pipe mill retained mandrel | |
| CN101456102A (en) | Alpha titanium alloy manual tungsten-electrode argon-shielded tungsten arc welding refined grain type welding wire and preparation method thereof | |
| CN105935733A (en) | Preparation method of large-size high-strength aluminum alloy forged cake | |
| CN112281032B (en) | Preparation method of aluminum alloy welding material | |
| CN105349829A (en) | Titanium alloy Ti80 seamless tube and preparation method thereof | |
| CN103143660A (en) | Preparation method of TC17 titanium alloy flat square section bar | |
| CN105441713A (en) | A titanium alloy seamless tube and a manufacturing method thereof | |
| CN102899580A (en) | Large cross section austenite stainless steel thick plate and manufacturing method thereof | |
| CN108796330A (en) | A kind of strong Mg-Gd-Y-Zr nanometers of isomery magnesium alloy preparation method of superelevation | |
| CN114055092B (en) | Method for manufacturing wind tunnel ultrahigh pressure pipe fitting by high nickel alloy structural steel | |
| CN110551928A (en) | Production method of 5654 aluminum alloy welding wire blank | |
| CN106222486A (en) | A kind of high intensity zirconium titanium ferro-aluminum vanadium alloy and preparation method thereof | |
| CN103993144A (en) | Method for production of H13 die steel by bloom continuous casting | |
| CN111020293B (en) | High-performance TA1 rod wire material and preparation method thereof | |
| CN103436733B (en) | A kind of mountain bike frame high fatigue property titanium alloy | |
| CN106498231A (en) | A kind of ocean engineering titanium alloy of yield strength higher than 1000MPa | |
| CN103898355B (en) | Ti-5Mo-5V-6Cr-3Al titanium alloy extruded tube and working method thereof | |
| Veeman et al. | Fabrication of functionally graded material via gas tungsten arc welding based wire feeding additive manufacturing: mechanical and microstructural characterization |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20120418 |