CN102329152A - Complete polishing glaze archaizing brick overglaze and preparation method thereof - Google Patents
Complete polishing glaze archaizing brick overglaze and preparation method thereof Download PDFInfo
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- CN102329152A CN102329152A CN201110168602A CN201110168602A CN102329152A CN 102329152 A CN102329152 A CN 102329152A CN 201110168602 A CN201110168602 A CN 201110168602A CN 201110168602 A CN201110168602 A CN 201110168602A CN 102329152 A CN102329152 A CN 102329152A
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Abstract
The invention relates to a complete polishing glaze archaizing brick overglaze and a preparation method thereof. The complete polishing glaze archaizing brick overglaze is prepared from the following raw materials by weight percent: 4-8% of albite, 9-12% of potassium feldspar, 12-15% of calcite, 4-6% of barium carbonate, 6-10% of alumina, 12-15% of burnt talcum, 2-4% of zinc oxide, 2-5% of quartz powder, 9-13% of kaolin, 5-9% of wollastonite and the balance of impurities. The preparation method comprises the following steps: carrying out ball milling in a ratio of weighed raw material to ballstone to ethylene glycol to squeegee oil of 1: (1.8-2): 0.25: 0.3, and simultaneously controlling the fineness degree as follows: the screenings of 325-mesh sieve is 0.3-0.4%; printing on ground glaze and fancy glaze layers through 100-mesh silk screen by using a continuous printing process; and finally, firing through a liquefied gas raceway kiln firing system. According to the invention, the purposes of improving the stability of the process and the quality of the product, reducing glaze material loss in production process, reducing cost and simultaneously avoiding the generation of a screen sticking problem in production are achieved.
Description
Technical field
The present invention relates to a kind of full throwing glaze brick cover-coat enamel modelled after an antique and preparation method thereof.
Background technology
Full throwing glaze is a kind of a kind of special formulation glaze that can carry out polishing process at glaze; It is last one glaze that imposes on brick modelled after an antique; Be generally transparent cover-coat enamel or transparent convex fancy glaze at present, the full throwing glazed brick that imposes on full throwing glaze integrates polished tile and brick advantage modelled after an antique, and it is smooth bright clean as the polished tile that glaze is looked like; Rich patterns as its glaze pattern of while such as the brick modelled after an antique, color is thick and heavy or gorgeous.Its glaze characteristics are transparent do not hide beneath cover-coat enamel and Ge Dao fancy glazes; Very thin one deck of a jettisoning transparent when throwing glaze, and the full throwing of transparent convex fancy glaze do glaze is a spotlight, the protruding granular glaze that its protruding glaze becomes to be interrupted in the brick face through screen printing; Burn till and throw glaze again, effect is peculiar especially.The full glaze brick modelled after an antique of throwing reflects well to have characteristic on market, be a megatrend of ceramic industry.
Complete to throw glaze be under glazed, belongs to ornamental brick, it be after having executed ground-coat enamel with regard to stamp, execute the cover-coat enamel of layer of transparent again, fire afterwards the whole cover-coat enamel part of skimming, keep a part of cover coat, printed layer, ground-coat enamel.The full glaze brick modelled after an antique of throwing belongs to once-firing, polishes at glaze, belongs to last procedure.
Say from the angle of technology, throw the glaze production technique entirely and mainly contain two kinds at present:
The technology that some enterprises of a kind of original production sytull adopt, employing be the technology of massed glaze behind the first stamp, the transparent on surface is thicker, so stereoscopic sensation is stronger, the transparency is better, and polishing easily; In addition, because its glaze is thicker, therefore throw easily, but cost is higher relatively.
Another kind is a kind of technology that the original enterprise that produces brick modelled after an antique adopts, and promptly no matter is decorative pattern or the frit on surface glaze under, all stamps, and this technology naturalness is high, cost is low, but is easy to during the throwing glaze show-through.In addition, also there are some technical difficult points in this kind method, like the too thick great amount of bubbles that then when firing, produces easily of glaze, makes product throw the antifouling ability in back, loss of gloss.And glaze layer book too, then ornamental brick always has distortion, is prone to during polishing produce leak throw or local grinning effect.Therefore, during production in enormous quantities, product quality cannot say for sure to demonstrate,prove, and premium grads is difficult to stablize, and therefore, the deficiency that the present invention is directed to this kind method is improved.
Summary of the invention
The objective of the invention is to overcome above-mentioned shortcoming; A kind of full throwing glaze brick cover-coat enamel modelled after an antique and preparation method thereof is provided; The stability that has realized improving technology with quality product, reduce glaze loss in the production process, reduce cost, sticking net and come the quality to be difficult to stable problem in the time of avoiding producing simultaneously because of glaze bed thickness strip.
For addressing the above problem, the present invention realizes through following technical scheme:
Full throwing glaze of the present invention brick cover-coat enamel modelled after an antique, it is mainly formed by the feedstock production of following mass percent:
Albite 4-8%, potassium felspar sand 9-12%, calcite 12-15%, barium carbonate 4-6%, aluminum oxide 6-10%, burning talcum 12-15%, zinc oxide 2-4%, silica powder 2-5%, kaolin 9-13%, wollastonite 5-9%, all the other are impurity.
The chemical ingredients of described full throwing glaze brick cover-coat enamel modelled after an antique is formed content:
SiO
2: Al 60%,
2O
3: 8%, CaO:5%, MgO:10%, K
2O+Na
2O:8%, ZnO:2%, BaO:3%, loss on ignition IL:4%.
Take by weighing raw material according to described prescription; By raw material: ballstone: terepthaloyl moietie: stamp-pad ink=1: 1.8-2: carry out ball milling at 0.25: 0.3; Controlling fineness simultaneously is: 325 mesh sieves tail over 0.3-0.4%; Be printed onto on ground-coat enamel, the fancy glaze layer through the continuous typography of 100 order silk screens, fire through liquefied gas rolling tunnel kiln calcining system at last.
The continuous typography of described silk screen is the continuous typography of silk screen at least 2 roads, the continuous typography of preferred 3 road silk screens.
Described cover-coat enamel is fired through liquefied gas rolling tunnel kiln calcining system, and concrete firing temperature band is: 800 ℃ of minimum temperatures, 1220 ℃ of top temperatures.
Described firing temperature band is preferably: 872 ℃ of minimum temperatures, 1096 ℃ of top temperatures.
Full throwing glaze of the present invention brick cover-coat enamel modelled after an antique and preparation method thereof through regulating the chemical ingredients of prescription, is rationally controlled the usage quantity of system component, has improved the stability and the quality product of technology, and formulation cost is reduced; In glaze making processes, add terepthaloyl moietie and stamp-pad ink in proportion and replace that water, methyl are regulated cover-coat enamel viscosity, flowability, the generation of sticking net problem when having avoided producing; Adopt twice at least, the continuous typography of the silk screen in preferred three roads is through 100 order silk screens; Be printed onto the full glaze cover-coat enamel of throwing on ground-coat enamel, the fancy glaze layer; Reduce glaze loss in the production process, reduce cost, can also avoid because glaze bed thickness strip comes quality to be difficult to stable problem.
Embodiment
Below in conjunction with embodiment the present invention is done further explain.
Full throwing glaze of the present invention brick cover-coat enamel modelled after an antique, it mainly is prepared from albite, potassium felspar sand, calcite, barium carbonate, aluminum oxide, burning talcum, zinc oxide, silica powder, kaolin, wollastonite.
Table 1 is for constituting the full embodiment that throws the Different Weight degree of each component of glaze brick cover-coat enamel modelled after an antique:
Table 2: the chemical component table (weight percent) of throwing glaze brick cover-coat enamel modelled after an antique entirely
| Chemical ingredients | SiO 2 | Al 2O 3 | CaO | MgO | K 2O+Na 2O | ZnO | BaO | Loss on ignition |
| Per-cent (%) | 60 | 8 | 5 | 10 | 8 | 2 | 3 | 4 |
Take by weighing raw material according to described prescription; By raw material: ballstone: terepthaloyl moietie: stamp-pad ink=1: 1.8-2: carry out ball milling at 0.25: 0.3; Controlling fineness simultaneously is: 325 mesh sieves tail over 0.3-0.4%, are printed onto on ground-coat enamel, the fancy glaze layer through the continuous typography of 100 order silk screens; Fire through liquefied gas rolling tunnel kiln calcining system at last.3 tons of ball mill ball milling times are 18-20 hour, and 1.5 tons of ball mill ball milling times are 12-15 hour.
The continuous typography of described silk screen is the continuous typography of silk screen at least 2 roads, the continuous typography of preferred 3 road silk screens.The continuous typography of silk screen mainly refers to carries out at least twice silk screen printing continuously.
Described cover-coat enamel is fired through liquefied gas rolling tunnel kiln calcining system, and concrete firing temperature band is: 800 ℃ of minimum temperatures, 1220 ℃ of top temperatures.
Described firing temperature band is preferably: 872 ℃ of minimum temperatures, 1096 ℃ of top temperatures.
In sum, being merely in the preferable enforcement of the present invention, is not that the present invention is done any pro forma restriction; The those of ordinary skill of all industry all can be by the above and embodiment of the present invention swimmingly; But all professional and technical personnel of being familiar with are not in breaking away from technical scheme scope of the present invention, and the above technology contents that is disclosed capable of using and a little change of making is modified and the equivalent variations that develops is equivalent embodiment of the present invention; Simultaneously, all foundations essence technology of the present invention all still belongs within the protection domain of technical scheme of the present invention change, modification and the differentiation of any equivalent variations that above embodiment did.
Claims (6)
1. throw glaze brick cover-coat enamel modelled after an antique entirely for one kind, it is characterized in that:
It is mainly formed by the feedstock production of following mass percent:
Albite 4-8%, potassium felspar sand 9-12%, calcite 12-15%, barium carbonate 4-6%, aluminum oxide 6-10%, burning talcum 12-15%, zinc oxide 2-4%, silica powder 2-5%, kaolin 9-13%, wollastonite 5-9%, all the other are impurity.
2. full throwing glaze according to claim 1 brick cover-coat enamel modelled after an antique is characterized in that:
The chemical ingredients of described full throwing glaze brick cover-coat enamel modelled after an antique is formed content:
SiO
2: Al 60%,
2O
3: 8%, CaO:5%, MgO:10%, K
2O+Na
2O:8%, ZnO:2%, BaO:3%, loss on ignition IL:4%.
3. full preparation method who throws glaze brick cover-coat enamel modelled after an antique is characterized in that:
Prescription according to claim 1 takes by weighing raw material; By raw material: ballstone: terepthaloyl moietie: stamp-pad ink=1: 1.8-2: carry out ball milling at 0.25: 0.3; Controlling fineness simultaneously is: 325 mesh sieves tail over 0.3-0.4%; Be printed onto on ground-coat enamel, the fancy glaze layer through the continuous typography of 100 order silk screens, fire through liquefied gas rolling tunnel kiln calcining system at last.
4. according to the preparation method of full throwing glaze according to claim 3 brick cover-coat enamel modelled after an antique, it is characterized in that:
The continuous typography of described silk screen is the continuous typography of silk screen at least 2 roads, the continuous typography of preferred 3 road silk screens.
5. the preparation method of full throwing glaze according to claim 3 brick cover-coat enamel modelled after an antique is characterized in that:
Described cover-coat enamel is fired through liquefied gas rolling tunnel kiln calcining system, and concrete firing temperature band is: 800 ℃ of minimum temperatures, 1220 ℃ of top temperatures.
6. the preparation method of full throwing glaze according to claim 5 brick cover-coat enamel modelled after an antique is characterized in that:
Described firing temperature band is preferably: 872 ℃ of minimum temperatures, 1096 ℃ of top temperatures.
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| CN201110168602A CN102329152A (en) | 2011-06-21 | 2011-06-21 | Complete polishing glaze archaizing brick overglaze and preparation method thereof |
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Cited By (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103804027A (en) * | 2014-02-28 | 2014-05-21 | 湖南泰鑫瓷业有限公司 | Glazed with natural drape texture and manufacturing method thereof |
| CN103833419A (en) * | 2014-01-02 | 2014-06-04 | 惠达卫浴股份有限公司 | Purple bronze glaze with metallic luster and preparation method thereof |
| CN104072205A (en) * | 2014-07-11 | 2014-10-01 | 江苏拜富科技有限公司 | Full polish ceramic product and preparation method thereof |
| CN105924233A (en) * | 2016-04-29 | 2016-09-07 | 山东狮子王陶瓷科技有限公司 | Peeling-glaze marble tile and preparation method thereof |
| CN105948501A (en) * | 2016-04-29 | 2016-09-21 | 山东狮子王陶瓷科技有限公司 | Negative oxygen ion diamond super-spar ecological ceramic tile and preparation method thereof |
| CN106145680A (en) * | 2016-08-18 | 2016-11-23 | 温书强 | A kind of pottery jade glaze |
| CN106966598A (en) * | 2017-04-15 | 2017-07-21 | 景德镇陶瓷大学 | A kind of low temperature high-hardness, wearable throws glaze and preparation method thereof entirely |
| CN107963813A (en) * | 2017-12-18 | 2018-04-27 | 广东永航新材料实业股份有限公司 | A kind of preparation method of the candy glaze being tuned into by raw glaze and candy glaze Ceramic Tiles |
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| CN108178513A (en) * | 2017-12-05 | 2018-06-19 | 湖南陶润会文化传播有限公司 | Unglazed gorgeous colour response glaze and preparation method thereof |
| CN108996908A (en) * | 2018-10-23 | 2018-12-14 | 佛山市陶莹新型材料有限公司 | A kind of printing polishing glaze and preparation method thereof and the application method in tile product |
| CN109456048A (en) * | 2018-12-06 | 2019-03-12 | 佛山市玉矶材料科技有限公司 | A kind of metal tile and preparation method thereof |
| CN109761648A (en) * | 2019-03-19 | 2019-05-17 | 重庆唯美陶瓷有限公司 | It is a kind of to throw glaze Ceramic Tiles and preparation method thereof entirely |
| CN110255902A (en) * | 2019-05-27 | 2019-09-20 | 湖北杭瑞陶瓷有限责任公司 | A kind of overglaze being rapidly fired to suitable for glazed tile, glazed tile and preparation method thereof |
| CN110683766A (en) * | 2019-11-22 | 2020-01-14 | 重庆唯美陶瓷有限公司 | Full-polished glaze and preparation method thereof, black ink-jet ceramic tile and manufacturing method thereof |
| CN110818258A (en) * | 2019-12-10 | 2020-02-21 | 湖南德兴瓷业有限公司 | Underglaze color rheological reaction glaze and preparation method thereof |
| CN110978221A (en) * | 2019-11-20 | 2020-04-10 | 江西和美陶瓷有限公司 | Preparation process for solving polishing yellow edge problem of gray glazed brick |
| CN112062468A (en) * | 2020-08-26 | 2020-12-11 | 广东嘉联企业陶瓷有限公司 | Texture glaze layer applied to surface of rock plate and preparation method thereof |
| CN112079568A (en) * | 2020-09-02 | 2020-12-15 | 广东嘉联企业陶瓷有限公司 | Color development glaze layer applied to surface of rock plate and preparation method thereof |
| CN112592059A (en) * | 2020-12-28 | 2021-04-02 | 肇庆乐华陶瓷洁具有限公司 | High-transparency anti-fouling full-glazed glaze and preparation method of glazed brick using same |
| CN112919807A (en) * | 2021-01-25 | 2021-06-08 | 青岛硕远硅胶科技有限公司 | Glaze making method for improving smoothness of glaze surface |
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| CN103833419A (en) * | 2014-01-02 | 2014-06-04 | 惠达卫浴股份有限公司 | Purple bronze glaze with metallic luster and preparation method thereof |
| CN103833419B (en) * | 2014-01-02 | 2015-01-14 | 惠达卫浴股份有限公司 | Purple bronze glaze with metallic luster and preparation method thereof |
| CN103804027A (en) * | 2014-02-28 | 2014-05-21 | 湖南泰鑫瓷业有限公司 | Glazed with natural drape texture and manufacturing method thereof |
| CN104072205A (en) * | 2014-07-11 | 2014-10-01 | 江苏拜富科技有限公司 | Full polish ceramic product and preparation method thereof |
| CN104072205B (en) * | 2014-07-11 | 2015-11-25 | 江苏拜富科技有限公司 | A kind of full throwing glaze ceramic and preparation method thereof |
| CN105924233A (en) * | 2016-04-29 | 2016-09-07 | 山东狮子王陶瓷科技有限公司 | Peeling-glaze marble tile and preparation method thereof |
| CN105948501A (en) * | 2016-04-29 | 2016-09-21 | 山东狮子王陶瓷科技有限公司 | Negative oxygen ion diamond super-spar ecological ceramic tile and preparation method thereof |
| CN106145680A (en) * | 2016-08-18 | 2016-11-23 | 温书强 | A kind of pottery jade glaze |
| CN106966598A (en) * | 2017-04-15 | 2017-07-21 | 景德镇陶瓷大学 | A kind of low temperature high-hardness, wearable throws glaze and preparation method thereof entirely |
| CN106966598B (en) * | 2017-04-15 | 2019-10-08 | 景德镇陶瓷大学 | A kind of low temperature high-hardness, wearable throws glaze and preparation method thereof entirely |
| CN108178513A (en) * | 2017-12-05 | 2018-06-19 | 湖南陶润会文化传播有限公司 | Unglazed gorgeous colour response glaze and preparation method thereof |
| CN107963813A (en) * | 2017-12-18 | 2018-04-27 | 广东永航新材料实业股份有限公司 | A kind of preparation method of the candy glaze being tuned into by raw glaze and candy glaze Ceramic Tiles |
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| CN108996908A (en) * | 2018-10-23 | 2018-12-14 | 佛山市陶莹新型材料有限公司 | A kind of printing polishing glaze and preparation method thereof and the application method in tile product |
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| CN110978221A (en) * | 2019-11-20 | 2020-04-10 | 江西和美陶瓷有限公司 | Preparation process for solving polishing yellow edge problem of gray glazed brick |
| CN110978221B (en) * | 2019-11-20 | 2021-08-31 | 江西和美陶瓷有限公司 | Preparation process for solving polishing yellow edge problem of gray glazed brick |
| CN110683766A (en) * | 2019-11-22 | 2020-01-14 | 重庆唯美陶瓷有限公司 | Full-polished glaze and preparation method thereof, black ink-jet ceramic tile and manufacturing method thereof |
| CN110683766B (en) * | 2019-11-22 | 2022-02-08 | 重庆唯美陶瓷有限公司 | Full-polished glaze and preparation method thereof, black ink-jet ceramic tile and manufacturing method thereof |
| CN110818258A (en) * | 2019-12-10 | 2020-02-21 | 湖南德兴瓷业有限公司 | Underglaze color rheological reaction glaze and preparation method thereof |
| CN112062468A (en) * | 2020-08-26 | 2020-12-11 | 广东嘉联企业陶瓷有限公司 | Texture glaze layer applied to surface of rock plate and preparation method thereof |
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| CN112592059A (en) * | 2020-12-28 | 2021-04-02 | 肇庆乐华陶瓷洁具有限公司 | High-transparency anti-fouling full-glazed glaze and preparation method of glazed brick using same |
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Application publication date: 20120125 |