CN102250522A - Double-component metal effect paint for one-step spraying and preparation method thereof - Google Patents
Double-component metal effect paint for one-step spraying and preparation method thereof Download PDFInfo
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Abstract
The invention relates to double-component metal effect paint for one-step spraying and a preparation method thereof. The metal effect paint comprises the following components: (1) component A which comprises the following components in parts by weight: 7-10 parts of metallic pigment, 40-70.6 parts of resin, 10.4-40.9 parts of solvent, 10.4-42.6 parts of cellulose acetate butyrate with the concentration of 20%, 1.0-6.2 parts of wax, 0.03-0.5 part of dispersant, 0.03-0.1 part of flatting agent and 0.3-0.1 part of de-foaming agent; (2) component B which comprises the following components in parts by weight: 40-95 parts of curing agent resin and 10-60 parts of solvent; (3) component C which comprises the following components in parts by weight: 100 parts of solvent b; and the component A, the component B and the component C are mixed in the weight ratio of 4-8 to 1 to 4-8 for usage. Compared with the prior art, the double-component metal effect paint provided by the invention is simple and convenient, and can improve the array of the metallic pigment and avoid sagging and floating and other phenomena.
Description
Technical field
The present invention relates to a kind of coating, especially relate to two component metal effect lacquers of disposable spray finishing and preparation method thereof.
Background technology
Spraying coating process at most metal effect lacquer is 2~3 times sprayings, reach better covering power, but on the production line of streamline operration in order to save room and time, enhance productivity, it is good and avoid the sagging and the metal effect of the effect of growing dim to coat with lacquer to be issued to spraying opacifying power in the situation that does not change technology, yet there are no relevant report.
Traditional disposable spray finishing technology, if reach the effect of the opacifying power that is coated with for a time, just be easy to generate some disadvantages as: sagging, grow dim, metallic pigment arrange bad etc.
Summary of the invention
Purpose of the present invention be exactly provide in order to overcome the defective that above-mentioned prior art exists a kind of easy, can improve metallic pigment and arrange, avoid two component metal effects lacquers of sagging and the disposable spray finishing that grows dim and preparation method thereof.
Purpose of the present invention can be achieved through the following technical solutions: the two component metal effect lacquers of disposable spray finishing is characterized in that this metal effect enamel-cover is drawn together following component:
(1) A component comprises following component and weight part content: metallic pigment 7~10, resin 40~70.6, solvent 10.4~40.9,20% cellulose acetate butyrate 10.4~42.6, wax 1.0~6.2, dispersion agent 0.03~0.5, flow agent 0.03~0.1, defoamer 0.3~0.1;
(2) B component comprises following component and weight part content: curing agent resin 40~95, solvent 10~60;
(3) C component comprises following component and weight part content: solvent b100;
Described A component, B component and C component are 4~8 with weight ratio: 1: 4~8 mix the back uses.
Metallic pigment are zinc powder, aluminium powder, Stainless Steel Powder or nickel powder in the described A component.
Resin is acrylic resin, fluorocarbon resin, aminoresin or vibrin in the described A component.
Solvent is N-BUTYL ACETATE, dimethylbenzene, ethylene glycol ether acetate or 100# solvent oil in the described A component.
20% cellulose acetate butyrate is that to be dissolved in the N-BUTYL ACETATE massfraction be 20% cellulose acetate butyrate in the described A component.
Wax is polyethylene wax or polyamide wax in the described A component; Dispersion agent is BYK-170, BYK-107A or BYK-220S etc.; Flow agent is TEGO FLOW-425, BYK-333 or BYK-306; Defoamer is BYK-070, BYK-055, BYK-011 or BYK-530.
Curing agent resin is Bayer N75 in the described B component; Solvent a is N-BUTYL ACETATE or dimethylbenzene.
Solvent b is N-BUTYL ACETATE or dimethylbenzene in the described C component.
The preparation method of the two component metal effect lacquers of disposable spray finishing is characterized in that this method may further comprise the steps:
(1) preparation of A component
(a) add dispersion agent and partial solvent by the prescription requirement in metallic pigment, stirring makes mixture a;
(b) by prescription requirements resin, wax, 20% cellulose acetate butyrate, remaining solvent, flow agent, mixing, the maintenance temperature is 30~50 ℃, under 800~1200 rev/mins stirring velocity, stirs and obtains mixture b in 20~30 minutes;
(c) mixture a and mixture b are mixed, under 800~900 rev/mins stirring velocity, stirred 20~30 minutes, obtain mixture c, viscosity is adjusted to 150~260 seconds scopes with being coated with 4 glasss of detections;
(d) filter, promptly get component A;
(2) preparation of B component
(I) by the prescription requirement curing agent resin is added among the solvent a, add stirrer and disperseed 20~30 minutes, make mixture d;
(II) filter, make B component;
(3) preparation of C component
Solvent b stirring after 10~15 minutes, is filtered and promptly got component C;
(4) be used for one time and spray the preparation that the two-pack metal effect coats with lacquer
With A component, B component and C component is 4~8: 1: 4~8 mixing by weight, promptly gets product.
The detection of described degree of cleaning is to scrape the paperboard blade coating with the wet film preparing device of 100 μ m, scrapes that no obvious particle gets final product on the paperboard.
Compared with prior art, the present invention has the following advantages:
(1) can effectively improve the production efficiency of streamline operration;
(2) effectively improve the arrangement of metallic pigment, the phenomenon that has reduced sagging and grown dim.
Embodiment
The present invention is described in detail below in conjunction with specific embodiment.
The spraying swath that the imitation streamline operration is used, air pressure, see the arrangement of its pigment powder and sagging and the situation of growing dim with the metal effect lacquer that goes out a spraying of lacquer amount; The effect of being improved can be found by observing.
Embodiment 1
Component A
(a) earlier metallic pigment are added in the keg by the prescription requirement, add dispersion agent and partial solvent, and stir, stirring gets final product;
(b) by the prescription requirement resin, wax, 20%CAB, remaining solvent, flow agent, defoamer are added in the vat, 800~1200 rev/mins, stirred 20~30 minutes, maintain the temperature at 30~50 ℃;
(c) sampling (b) detects degree of cleaning, is scraping the paperboard blade coating with the wet film preparing device of 100 μ m, scrapes no obvious particle on the paperboard;
(d) 800~900 commentaries on classics in (a) adding (b) were stirred 20~30 minutes;
(e) sampling (d) detects degree of cleaning, does not have obvious particle, viscosity with being coated with 4 glasss of detections, is adjusted to 150~260 seconds scopes;
(f) filter weighing and bagging.
Embodiment 2
Component A
(a) earlier metallic pigment are added in the keg by the requirement of assembly side, add dispersion agent and partial solvent, and stir, stirring gets final product;
(b) by the requirement of component prescription resin, wax, 20%CAB, remaining solvent, flow agent, defoamer are added in the vat, 800~1200 rev/mins, stirred 20~30 minutes, maintain the temperature at 30~50 ℃;
(c) sampling (b) detects degree of cleaning, is scraping the paperboard blade coating with the wet film preparing device of 100 μ m, scrapes no obvious particle on the paperboard;
(d) (a) added (b) middle stirring 20~30 minutes;
(e) sampling (d) detects degree of cleaning, does not have obvious particle, viscosity with being coated with 4 glasss of detections, is adjusted to 150~260 seconds scopes;
(f) filter weighing and bagging.
Embodiment 3
Component A
(a) earlier metallic pigment are added in the keg by the prescription requirement, add dispersion agent and partial solvent, and stir, stirring gets final product;
(b) by the prescription requirement resin, wax, 20%CAB, remaining solvent, flow agent, photostabilizer are added in the vat, 800~1200 rev/mins, stirred 20~30 minutes, maintain the temperature at 30~50 ℃;
(c) sampling (b) detects degree of cleaning, is scraping the paperboard blade coating with the wet film preparing device of 100 μ m, scrapes no obvious particle on the paperboard;
(d) (a) added (b) middle stirring 20~30 minutes;
(e) sampling (d) detects degree of cleaning, does not have obvious particle, viscosity with being coated with 4 glasss of detections, is adjusted to 150~260 seconds scopes;
(f) filter weighing and bagging.
Component B
Component C
Embodiment 4
A kind of method for preparing the two component metal effect lacquers of disposable spray finishing, this method comprises following processing step:
Component A:
(a) earlier metallic pigment zinc powder 70kg is added in the keg by the prescription requirement, add 0.3kg dispersant B YK-170 and 50kg solvent butyl acetate, and stir, stirring obtains mixture a;
(b) by the prescription requirement 370kg resin ELEMENTLS-2060A, 336kg resin ELEMENTLS-2060B, 25kg polyethylene wax, 37kg polyamide wax, 426kg being dissolved in the N-BUTYL ACETATE massfraction is 20% cellulose acetate butyrate Eastman CAB381-2, remaining solvent: in 20kg dimethylbenzene, 34kg vinyl acetic monomer, 0.3kg flow agent TEGO FLOW-425,1kg defoamer BYK-070, the adding vat, 1000 rev/mins, stirred 20 minutes, maintain the temperature at 30 ℃, obtain mixture b;
(c) sampling mixture b detects degree of cleaning, is scraping the paperboard blade coating with the wet film preparing device of 100 μ m, scrapes that no obvious particle gets final product on the paperboard;
(d) stirring 20 minutes among the mixture a adding mixture b, obtain mixture d;
(e) sampling mixture d detects degree of cleaning, does not have obvious particle, and viscosity is adopted the conventional 4 glasss of detection methods that are coated with, and is adjusted to 150 seconds;
(f) filter, obtain component A.
Component B:
(I) by prescription 70kg curing agent resin Bayer N75 is put into suitable cylinder, add the 30kg N-BUTYL ACETATE then, on dispersion machine, disperseed 20 minutes again, obtain mixture c;
(II) sampling mixture c detects degree of cleaning, does not have obvious particle, and is qualified;
(III) filter, obtain B component.
Component C:
(i) by prescription solvent butyl acetate 100kg is all added in the suitable cylinder, stirred 10 minutes;
(ii) filter weighing and bagging.
When this programme uses component A, B component and component C are sprayed by weight 4: 1: 4 mixed.
Embodiment 5
A kind of method for preparing the two component metal effect lacquers of disposable spray finishing, this method comprises following processing step:
Component A:
(a) earlier metallic pigment aluminium powder 100kg is added in the keg by the prescription requirement, add 5kg dispersant B YK-170 and 100kg solvent butyl acetate, and stir, stirring obtains mixture a;
(b) by prescription requirements 690~706kg ELEMENTLS-2060A and ELEMENTLS-2060B, 5kg polyethylene wax, 5kg polyamide wax, 104kg being dissolved in the N-BUTYL ACETATE massfraction is in 20% cellulose acetate butyrate Eastman CAB 381-2, remaining solvent 159kg dimethylbenzene, 150kg vinyl acetic monomer, 1kg flow agent TEGO FLOW 425,3kg defoamer-070, the adding vat, 1200 rev/mins, stirred 30 minutes, maintain the temperature at 50 ℃, obtain mixture b;
(c) sampling mixture b detects degree of cleaning, is scraping the paperboard blade coating with the wet film preparing device of 100 μ m, scrapes that no obvious particle gets final product on the paperboard;
(d) stirring 30 minutes among the mixture a adding mixture b, obtain mixture d;
(e) sampling mixture d detects degree of cleaning, does not have obvious particle, viscosity with being coated with 4 glasss of detections, is adjusted to 260 seconds;
(f) filter, obtain component A.
Component B:
(I) by prescription 95kg curing agent resin Bayer N75 is put into suitable cylinder, add 10kg dimethylbenzene then, on dispersion machine, disperseed 30 minutes again, obtain mixture c;
(II) sampling mixture c detects degree of cleaning, does not have obvious particle, and is qualified;
(III) filter, obtain B component.
Component C:
(i) by prescription solvent xylene 100kg is all added in the suitable cylinder, stirred 15 minutes;
(ii) filter weighing and bagging.
When this programme uses component A, B component and component C are sprayed by weight 8: 1: 4 mixed.
Embodiment 6
A kind of method for preparing the two component metal effect lacquers of disposable spray finishing, this method comprises following processing step:
Component A:
(a) earlier metallic pigment nickel powder 80~90kg is added in the keg by the prescription requirement, add 0.8~0.9kg dispersant B YK-170 and 54~80kg solvent xylene, and stir, stirring obtains mixture a;
(b) by prescription requirements 536~576kg ELEMENTLS-2060A and ELEMENTLS-2060B, 17~18kg polyethylene wax, 198~202kg being dissolved in the N-BUTYL ACETATE massfraction is in 20% cellulose acetate butyrate Eastman CAB 531-1, remaining 100~120kg solvent xylene, 0.6~0.8kg flow agent TEGOFLOW-425, the 2.5~2.8kg defoamer BYK-070 adding vat, 900~1000 rev/mins, stirred 25~28 minutes, maintain the temperature at 40~45 ℃, obtain mixture b;
(c) sampling mixture b detects degree of cleaning, is scraping the paperboard blade coating with the wet film preparing device of 100 μ m, scrapes that no obvious particle gets final product on the paperboard;
(d) stirring 25~28 minutes among the mixture a adding mixture b, obtain mixture d;
(e) sampling mixture d detects degree of cleaning, does not have obvious particle, viscosity with being coated with 4 glasss of detections, is adjusted to 200~220 seconds scopes;
(f) filter, obtain component A.
Component B:
(I) by prescription 40kg curing agent resin Bayer N75 is put into suitable cylinder, add the 60kg N-BUTYL ACETATE then, on dispersion machine, disperseed again 25~28 minutes, obtain mixture c;
(II) sampling mixture c detects degree of cleaning, does not have obvious particle, and is qualified;
(III) filter, obtain B component.
Component C:
(i) by prescription solvent butyl acetate 100kg is all added in the suitable cylinder, stirred 12~13 minutes;
(ii) filter weighing and bagging.
When this programme uses component A, B component and component C are sprayed by weight 6: 1: 6 mixed.
Claims (10)
1. the two component metal effects of disposable spray finishing coat with lacquer, and it is characterized in that this metal effect enamel-cover is drawn together following component:
(1) A component comprises following component and weight part content: metallic pigment 7~10, resin 40~70.6, solvent 10.4~40.9,20% cellulose acetate butyrate 10.4~42.6, wax 1.0~6.2, dispersion agent 0.03~0.5, flow agent 0.03~0.1, defoamer 0.3~0.1;
(2) B component comprises following component and weight part content: curing agent resin 40~95, solvent 10~60;
(3) C component comprises following component and weight part content: solvent b100;
Described A component, B component and C component are 4~8 with weight ratio: 1: 4~8 mix the back uses.
2. the two component metal effect lacquers of disposable spray finishing according to claim 1 is characterized in that metallic pigment are zinc powder, aluminium powder, Stainless Steel Powder or nickel powder in the described A component.
3. the two component metal effect lacquers of disposable spray finishing according to claim 1 is characterized in that resin is acrylic resin, fluorocarbon resin, aminoresin or vibrin in the described A component.
4. the two component metal effect lacquers of disposable spray finishing according to claim 1 is characterized in that solvent is N-BUTYL ACETATE, dimethylbenzene, ethylene glycol ether acetate or 100# solvent oil in the described A component.
5. the two component metal effects lacquers of disposable spray finishing according to claim 1 is characterized in that, 20% cellulose acetate butyrate is that to be dissolved in the N-BUTYL ACETATE massfraction be 20% cellulose acetate butyrate in the described A component.
6. the two component metal effect lacquers of disposable spray finishing according to claim 1 is characterized in that wax is polyethylene wax or polyamide wax in the described A component; Dispersion agent is BYK-170, BYK-107A or BYK-220S etc.; Flow agent is TEGO FLOW-425, BYK-333 or BYK-306; Defoamer is BYK-070, BYK-055, BYK-011 or BYK-530.
7. the two component metal effect lacquers of disposable spray finishing according to claim 1 is characterized in that curing agent resin is Bayer N75 in the described B component; Solvent a is N-BUTYL ACETATE or dimethylbenzene.
8. the two component metal effect lacquers of disposable spray finishing according to claim 1 is characterized in that solvent b is N-BUTYL ACETATE or dimethylbenzene in the described C component.
9. the preparation method of the two component metal effects lacquers of a disposable spray finishing as claimed in claim 1 is characterized in that this method may further comprise the steps:
(1) preparation of A component
(a) add dispersion agent and partial solvent by the prescription requirement in metallic pigment, stirring makes mixture a;
(b) by prescription requirements resin, wax, 20% cellulose acetate butyrate, remaining solvent, flow agent, mixing, the maintenance temperature is 30~50 ℃, under 800~1200 rev/mins stirring velocity, stirs and obtains mixture b in 20~30 minutes;
(c) mixture a and mixture b are mixed, under 800~900 rev/mins stirring velocity, stirred 20~30 minutes, obtain mixture c, viscosity is adjusted to 150~260 seconds scopes with being coated with 4 glasss of detections;
(d) filter, promptly get component A;
(2) preparation of B component
(I) by the prescription requirement curing agent resin is added among the solvent a, add stirrer and disperseed 20~30 minutes, make mixture d;
(II) filter, make B component;
(3) preparation of C component
Solvent b stirring after 10~15 minutes, is filtered and promptly got component C;
(4) be used for one time and spray the preparation that the two-pack metal effect coats with lacquer
With A component, B component and C component is 4~8: 1: 4~8 mixing by weight, promptly gets product.
10. the preparation method of the two component metal effects lacquers of disposable spray finishing according to claim 9 is characterized in that the detection of described degree of cleaning is to scrape the paperboard blade coating with the wet film preparing device of 100 μ m, scrapes that no obvious particle gets final product on the paperboard.
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CN102492355A (en) * | 2011-12-21 | 2012-06-13 | 天津灯塔涂料工业发展有限公司 | Bi-component enamel paint resistant to high-temperature baking of special medium and preparation method thereof |
CN103497605A (en) * | 2013-09-27 | 2014-01-08 | 东来涂料技术(上海)有限公司 | Oily acrylic acid metallic paint with high storage stability and preparation method thereof |
CN103834247A (en) * | 2012-11-22 | 2014-06-04 | 汉达精密电子(昆山)有限公司 | Aluminium powder paint, spraying method of aluminium powder paint and product sprayed by the method |
CN103992713A (en) * | 2014-04-28 | 2014-08-20 | 浙江钱锦气雾剂制品有限公司 | Blue white zinc self-spraying healant |
CN104140708A (en) * | 2014-07-28 | 2014-11-12 | 黄能威 | Rainbow agent |
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CN1511901A (en) * | 2002-12-27 | 2004-07-14 | 深圳市海川实业股份有限公司 | High performance metal filling building decorative paint |
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CN102492355A (en) * | 2011-12-21 | 2012-06-13 | 天津灯塔涂料工业发展有限公司 | Bi-component enamel paint resistant to high-temperature baking of special medium and preparation method thereof |
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CN103509412B (en) * | 2012-06-21 | 2017-04-12 | 关西涂料株式会社 | Brightness coating composition |
CN103834247A (en) * | 2012-11-22 | 2014-06-04 | 汉达精密电子(昆山)有限公司 | Aluminium powder paint, spraying method of aluminium powder paint and product sprayed by the method |
CN103497605A (en) * | 2013-09-27 | 2014-01-08 | 东来涂料技术(上海)有限公司 | Oily acrylic acid metallic paint with high storage stability and preparation method thereof |
CN103497605B (en) * | 2013-09-27 | 2016-03-23 | 东来涂料技术(上海)有限公司 | Oiliness metal acrylate paint that a kind of stability in storage is strong and preparation method thereof |
CN103992713A (en) * | 2014-04-28 | 2014-08-20 | 浙江钱锦气雾剂制品有限公司 | Blue white zinc self-spraying healant |
CN103992713B (en) * | 2014-04-28 | 2019-01-11 | 浙江品创知识产权服务有限公司 | A kind of indigo plant white zine self-spray type healant |
CN104140708A (en) * | 2014-07-28 | 2014-11-12 | 黄能威 | Rainbow agent |
CN104140708B (en) * | 2014-07-28 | 2016-07-27 | 黄能威 | A kind of rainbow agent |
CN110028879A (en) * | 2019-04-02 | 2019-07-19 | 福建三昊科技有限公司 | A kind of reflective membrane, encapsulating material and preparation method |
CN110183904A (en) * | 2019-06-13 | 2019-08-30 | 广东顺德洋紫薇化工有限公司 | Fire-retardant ink and preparation method thereof and inflaming retarding membrane |
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Address after: 201807 No. 1221 Xin He Lu, Jiading Industrial Zone, Jiading District, Shanghai. Patentee after: Dong Lai coating technology (Shanghai) Limited by Share Ltd Address before: 201807 No. 1221 Xin He Lu, North Jiading Industrial Zone, Jiading District, Shanghai. Patentee before: Eastern paint technology (Shanghai) Co., Ltd. |