CN102225358A - Ore dressing method of vanadium titanium magnetite - Google Patents
Ore dressing method of vanadium titanium magnetite Download PDFInfo
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- CN102225358A CN102225358A CN2011101503080A CN201110150308A CN102225358A CN 102225358 A CN102225358 A CN 102225358A CN 2011101503080 A CN2011101503080 A CN 2011101503080A CN 201110150308 A CN201110150308 A CN 201110150308A CN 102225358 A CN102225358 A CN 102225358A
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Abstract
The invention discloses an ore dressing method of a vanadium titanium magnetite and belongs to the field of magnetic separation of vanadium titanium magnetite. The invention provides an ore dressing method of a vanadium titanium magnetite. The method has low costs and simple operations, and comprises the following processing steps of: a. crushing and screening vanadium titanium magnetic iron ore, carrying out fine grinding to have a granularity no more than 3mm, then carrying out magnetic separation under a field intensity of 3000-5000 Oe to obtain a rough concentrate and a mine tailing; b. grinding the rough concentrate to 80 mesh and carrying out magnetic separation by a magnet separator with a field intensity of 1000-1500 Oe; c. then carrying out magnetic separation by a magnet separator with a field intensity of 800-1000 Oe to obtain a qualified iron ore concentrate and a mine tailing. According to the invention, after coarse grain tailings discarding, low-grade raw ore vanadium titanium magnetite, which needs no repeated grinding, can reach concentrate grade with TFe equal to 59% and recovery rate reaching about 80%. In the technology, repeated grinding and grading are not needed after coarse grain tailings discarding, therefore magnetic separation costs are lowered substantially.
Description
Technical field
The present invention relates to a kind of physics method beneficiation method, belong to vanadium titano-magnetite magnetic separation field.
Background technology
Vanadium titano-magnetite reserves in the world are very abundant, and the reserves of China come out at the top, and Sichuan Panxi Diqu and area, Chengde reserves reach 10,000,000,000 tons.Vanadium titano-magnetite is a kind of mineral intergrowth of multielement, and its composition is with place of production difference difference to some extent, in general, and main iron content (oxide form with iron in the ore deposit exists) 30-34wt% in the ore deposit, V
2O
50.3-1wt%, TiO
28-14wt%; The ore that exploitation is come out obtains iron (vanadium) concentrate through broken and ore dressing, as the raw material of iron and steel smelting; Select the mine tailing of iron to be used to reclaim concentrated ilmenite, as the raw material that extracts titanium products.
At present, selecting from the nature vanadium titano-magnetite all must be through grind grading into the ore-dressing technique of stove iron ore, usually adopting two sections rank mill rank choosings (is limit edging choosing, regrinding and reconcentration) selects iron, adopt spiral electric separation+method for floating to select titanium or bulk flotation method to select titanium or spiral+shaking table method to select titanium selecting the mine tailing behind the iron.Mill rank, two sections rank choosing method selects iron, and first section ore grinding to-200 orders (0.074mm) granularity is 45%, is 1800-2500Oe (oersted) magnetic separation in field intensity; Second section ore grinding to-200 granularity is 80%, is the 1300-1800Oe magnetic separation in field intensity.Its shortcoming is that the rate of recovery of iron ore concentrate and ilmenite concentrate is not high, and cost is higher, is mainly used in the screening of the high-grade vanadium titano-magnetite of TFe (full iron) more than or equal to 30%.
At above-mentioned defective, Chinese patent CN 101564707B discloses a kind of low grade vanadium titanomagnetite (vanadium titano-magnetite of TFe content between 15-25) and higher screening technique of iron ore concentrate quality of being applicable to, promptly adopt mill rank, three sections rank to select technology to carry out magnetic separation, wherein, one stages of magnetic separation: ore is slightly broken to be pulverized to granularity≤15mm, grading system gets-200 order granularities and reaches 30% ore pulp, is magnetic separation under the 3000-4000Oe in field intensity; Two stages of magnetic separation: a stages of magnetic separation concentrate carries out the pulverizing second time after taking off magnetic, and grading system gets-200 order granularities and reaches 55% ore pulp, is magnetic separation under the 1800-2200Oe in field intensity; Three stages of magnetic separation: pulverize for the third time after two stages of magnetic separation concentrate take off magnetic, grading system gets-200 order granularities and reaches 80% ore pulp, is that magnetic separation obtains iron ore concentrate (TFe is 57%) and magnetic tailing under the 1200-1800Oe in field intensity.
As seen, the ore-dressing technique of selecting from the nature vanadium titano-magnetite in the prior art into the stove iron ore all must at first will be milled to the ore deposit-200 orders (0.074mm), and follow-up also the need through two to three overground classifications sorts with magnetic separator then or cyclone sorts, its complex procedures, cost is higher.
Summary of the invention
The present invention is directed to above-mentioned defective, provide that a kind of cost is low, the beneficiation method of the simple vanadium titano-magnetite of operation.
Technical scheme of the present invention is:
The invention provides a kind of beneficiation method of vanadium titano-magnetite, its processing step is:
A is finely ground to granularity＜3mm with v-ti magnetite ore crushing and screening, and back magnetic separation under field intensity 3000-5000Oe obtains rough concentrate and mine tailing;
B is milled to-80 orders with above-mentioned rough concentrate, carries out magnetic separation with the magnetic separator of field intensity 1000-1500Oe;
C is the magnetic separator magnetic separation of 800-1000Oe again with field intensity, gets qualified iron ore concentrate and mine tailing.
Preferably, above-mentioned v-ti magnetite ore is crushed to granularity≤15mm earlier and is finely ground to granularity≤3mm again.
Preferably, adopt ball milling or rod milling to be finely ground to granularity≤3mm in the said method.
Preferably, field intensity is 4000Oe in a step.
Preferably, field intensity is 1200Oe in the b step.
Preferably, field intensity is 1000Oe in the c step.
Beneficial effect of the present invention: through being 59% not needing repeatedly just can to reach concentrate grade TFe through magnetic separation under the overground situation behind the discarding coarse tailing, the rate of recovery reaches about 80% to the vanadium titano-magnetite of head grade about 25% in the present invention.This technology need not be milled to the ore deposit-200 orders (0.074mm) earlier, but does not need through repeatedly overground the magnetic separation cost to be reduced greatly after adopting discarding coarse tailing; And titanium not overground (rough concentrate is milled to-80 orders, guarantees that then titanium is not overground) provides good platform for follow-up ore-dressing technique reclaims beneficiating ingredient.
Description of drawings
Fig. 1 is the process chart of vanadium titano-magnetite ore dressing method of the present invention.
The specific embodiment
The invention provides a kind of beneficiation method of vanadium titano-magnetite, its processing step is:
A is finely ground to granularity≤3mm with v-ti magnetite ore crushing and screening, and back magnetic separation under field intensity 3000-5000Oe (oersted) obtains rough concentrate and mine tailing; B is milled to-80 orders with above-mentioned rough concentrate, carries out magnetic separation with the magnetic separator of field intensity 1000-1500Oe, is the magnetic separator magnetic separation of 800-1000Oe again with field intensity, qualified iron ore concentrate and mine tailing.
Raw material before becoming ore pulp must be selected suitable granularity, this vanadium titano-magnetite need adopt jaw crusher slightly broken, through thin breaking in the gyratory crusher ore grain size is reached-15mm again, then through the ball mill fine grinding make granularity reach-be the magnetic separator magnetic separation of 3000-5000Oe directly behind the 3mm with magnetic field intensity, obtain rough concentrate and mine tailing (mine tailing TFe＜3%, TiO
2＜1%), rough concentrate enters next section operation, thereby reaches the requirement of discarding coarse tailing, reduces overground cost; Rough concentrate is finely ground to 80 orders through ore mill again and enters subsequent handling and reach required qualified concentrate containing (TFe is 59%), and the rate of recovery reaches about 80%.
Embodiment
Getting TFe is 24.54%, TiO
2Content is 100 kilograms of 9.5% vanadium titano-magnetites, ore reduction, screening, the ore grain size≤15mm behind the finished breaking; Ore after the fragmentation enters ball mill, is finely ground to granularity≤3mm, carries out magnetic separation with the magnetic separator of field intensity 4000Oe, and magnetic separation gets 85.28 kilograms of rough concentrates and mine tailing; Rough concentrate ball milling after the magnetic separation is to-80 orders, carries out magnetic separation with the magnetic separator of field intensity 1200Oe, and the magnetic separator with 1000Oe sorts again; The TFe that finally obtains 34.5 kilograms is 59.25% iron ore concentrate; Mine tailing enters next step utilization of selecting titanium.
Adopt beneficiation method of the present invention, select field intensity 3000-5000Oe in a step for use, select field intensity 1000-1500Oe in the b step for use, select field intensity 800-1000Oe in the c step for use; By can getting qualified iron ore concentrate and mine tailing after the above-mentioned steps magnetic separation, and the TFe content of gained iron ore concentrate can reach about 59%, and the rate of recovery can reach about 81%.
For the vanadium titano-magnetite (TFe content is between 15-25) of same grade, use traditional beneficiation method (multistage overground ore dressing), the TFe content after the ore dressing is about 54%, the rate of recovery of TFe is about 65%; And use beneficiation method of the present invention, and the TFe content after the ore dressing can reach about 59%, and the rate of recovery can reach about 81%; As seen, beneficiation method of the present invention has reached the advanced level of this type ore-dressing technique at present to the rate of recovery and the raising TFe grade of TFe.And this beneficiation method has vanadium titano-magnetite sorted according to the character of ore and can reach discarding coarse tailing, and titanium is not overground, has energy-saving and cost-reducing advantage.
Claims (6)
1. the beneficiation method of a vanadium titano-magnetite, processing step is:
A is finely ground to granularity≤3mm with v-ti magnetite ore crushing and screening, and back magnetic separation under field intensity 3000-5000Oe obtains rough concentrate and mine tailing;
B is milled to-80 orders with above-mentioned rough concentrate, carries out magnetic separation with the magnetic separator of field intensity 1000-1500Oe;
C is the magnetic separator magnetic separation of 800-1000Oe again with field intensity, gets qualified iron ore concentrate and mine tailing.
2. the beneficiation method of vanadium titano-magnetite according to claim 1 is characterized in that, in a step, the v-ti magnetite ore is crushed to granularity≤15mm fine grinding more earlier.
3. according to the beneficiation method of claim 1 or 2 described vanadium titano-magnetites, it is characterized in that field intensity is 4000Oe in a step.
4. according to the beneficiation method of each described vanadium titano-magnetite of claim 1-3, it is characterized in that field intensity is 1200Oe in the b step.
5. according to the beneficiation method of each described vanadium titano-magnetite of claim 1-4, it is characterized in that field intensity is 1000Oe in the c step.
6. according to the beneficiation method of each described vanadium titano-magnetite of claim 1-5, it is characterized in that ball milling or rod milling are adopted in fine grinding.
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Cited By (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102580843A (en) * | 2012-02-22 | 2012-07-18 | 攀钢集团矿业有限公司 | Mineral separation method for vanadium-titanium magnetite ores |
| CN102641782A (en) * | 2012-05-23 | 2012-08-22 | 太原钢铁(集团)有限公司 | Beneficiation method |
| CN103111363A (en) * | 2012-12-26 | 2013-05-22 | 东北大学 | Deep reduction comprehensive utilization method of iron ore containing rare earths |
| CN103120984A (en) * | 2011-11-19 | 2013-05-29 | 赵中林 | Method of iron concentrate powder magnetic separation in dry mode |
| CN103157551A (en) * | 2013-04-01 | 2013-06-19 | 山东乾舜矿冶科技股份有限公司 | Comprehensive recovery process of intense-weathering poor vanadium titano-magnetite |
| CN103736574A (en) * | 2014-01-21 | 2014-04-23 | 米易元通铁钛有限责任公司 | Vanadium titano-magnetite screening method |
| CN103816980A (en) * | 2014-02-28 | 2014-05-28 | 四川安宁铁钛股份有限公司 | Closed circuit grinding grading technology |
| CN103949339A (en) * | 2014-05-12 | 2014-07-30 | 长沙矿冶研究院有限责任公司 | Method for recycling iron and titanium in vanadium titano-magnetite |
| CN105107616A (en) * | 2015-09-22 | 2015-12-02 | 赣州金环磁选设备有限公司 | Low-cost high-recovery environment-friendly mineral separation method of low-grade vanadium titano-magnetite |
| CN105478232A (en) * | 2015-11-24 | 2016-04-13 | 广州有色金属研究院 | Mineral processing method for enriching vanadium pentoxide from graphite vanadium ore |
| CN109174398A (en) * | 2018-08-02 | 2019-01-11 | 汤铁 | A kind of comprehensive utilization process of vanadium titano-magnetite |
| CN109675708A (en) * | 2018-12-14 | 2019-04-26 | 四川龙蟒矿冶有限责任公司 | A kind of Pre-sorting technique of vanadium titano-magnetite |
| CN109939815A (en) * | 2019-03-29 | 2019-06-28 | 中冶北方（大连）工程技术有限公司 | Two product ore-dressing technique of vanadium titano-magnetite |
| CN111545341A (en) * | 2020-04-29 | 2020-08-18 | 广东邦普循环科技有限公司 | Process for removing chromium from laterite-nickel ore |
| CN112371304A (en) * | 2020-10-22 | 2021-02-19 | 攀钢集团攀枝花钢铁研究院有限公司 | Method and system for sand setting and tailing discarding of vanadium titano-magnetite |
| CN112387409A (en) * | 2020-10-22 | 2021-02-23 | 攀钢集团攀枝花钢铁研究院有限公司 | Grinding-assisting method and system for vanadium titano-magnetite |
| CN114682367A (en) * | 2022-04-01 | 2022-07-01 | 攀钢集团攀枝花钢铁研究院有限公司 | Grinding and selecting method of vanadium titano-magnetite |
| CN114713362A (en) * | 2022-04-21 | 2022-07-08 | 攀枝花学院 | Vanadium titano-magnetite titanium-selecting flotation collecting agent and vanadium titano-magnetite titanium-selecting process |
| CN114733631A (en) * | 2022-03-31 | 2022-07-12 | 龙佰武定钛业有限公司 | Method and system for quickly crushing, grinding and grading high-titanium slag |
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Cited By (24)
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|---|---|---|---|---|
| CN103120984A (en) * | 2011-11-19 | 2013-05-29 | 赵中林 | Method of iron concentrate powder magnetic separation in dry mode |
| CN102580843A (en) * | 2012-02-22 | 2012-07-18 | 攀钢集团矿业有限公司 | Mineral separation method for vanadium-titanium magnetite ores |
| CN102641782A (en) * | 2012-05-23 | 2012-08-22 | 太原钢铁(集团)有限公司 | Beneficiation method |
| CN103111363A (en) * | 2012-12-26 | 2013-05-22 | 东北大学 | Deep reduction comprehensive utilization method of iron ore containing rare earths |
| CN103157551A (en) * | 2013-04-01 | 2013-06-19 | 山东乾舜矿冶科技股份有限公司 | Comprehensive recovery process of intense-weathering poor vanadium titano-magnetite |
| CN103157551B (en) * | 2013-04-01 | 2014-11-19 | 山东乾舜矿冶科技股份有限公司 | Comprehensive recovery process of intense-weathering poor vanadium titano-magnetite |
| CN103736574A (en) * | 2014-01-21 | 2014-04-23 | 米易元通铁钛有限责任公司 | Vanadium titano-magnetite screening method |
| CN103736574B (en) * | 2014-01-21 | 2015-11-18 | 米易元通铁钛有限责任公司 | Vanadium titano-magnetite screen method |
| CN103816980A (en) * | 2014-02-28 | 2014-05-28 | 四川安宁铁钛股份有限公司 | Closed circuit grinding grading technology |
| CN103949339A (en) * | 2014-05-12 | 2014-07-30 | 长沙矿冶研究院有限责任公司 | Method for recycling iron and titanium in vanadium titano-magnetite |
| CN105107616A (en) * | 2015-09-22 | 2015-12-02 | 赣州金环磁选设备有限公司 | Low-cost high-recovery environment-friendly mineral separation method of low-grade vanadium titano-magnetite |
| CN105478232A (en) * | 2015-11-24 | 2016-04-13 | 广州有色金属研究院 | Mineral processing method for enriching vanadium pentoxide from graphite vanadium ore |
| CN109174398A (en) * | 2018-08-02 | 2019-01-11 | 汤铁 | A kind of comprehensive utilization process of vanadium titano-magnetite |
| CN109675708A (en) * | 2018-12-14 | 2019-04-26 | 四川龙蟒矿冶有限责任公司 | A kind of Pre-sorting technique of vanadium titano-magnetite |
| CN109939815A (en) * | 2019-03-29 | 2019-06-28 | 中冶北方（大连）工程技术有限公司 | Two product ore-dressing technique of vanadium titano-magnetite |
| CN109939815B (en) * | 2019-03-29 | 2020-10-16 | 中冶北方（大连）工程技术有限公司 | Mineral separation process for two products of vanadium titano-magnetite |
| CN111545341A (en) * | 2020-04-29 | 2020-08-18 | 广东邦普循环科技有限公司 | Process for removing chromium from laterite-nickel ore |
| CN112371304A (en) * | 2020-10-22 | 2021-02-19 | 攀钢集团攀枝花钢铁研究院有限公司 | Method and system for sand setting and tailing discarding of vanadium titano-magnetite |
| CN112387409A (en) * | 2020-10-22 | 2021-02-23 | 攀钢集团攀枝花钢铁研究院有限公司 | Grinding-assisting method and system for vanadium titano-magnetite |
| CN114733631A (en) * | 2022-03-31 | 2022-07-12 | 龙佰武定钛业有限公司 | Method and system for quickly crushing, grinding and grading high-titanium slag |
| CN114682367A (en) * | 2022-04-01 | 2022-07-01 | 攀钢集团攀枝花钢铁研究院有限公司 | Grinding and selecting method of vanadium titano-magnetite |
| CN114682367B (en) * | 2022-04-01 | 2023-10-27 | 攀钢集团攀枝花钢铁研究院有限公司 | Grinding and selecting method of vanadium titano-magnetite |
| CN114713362A (en) * | 2022-04-21 | 2022-07-08 | 攀枝花学院 | Vanadium titano-magnetite titanium-selecting flotation collecting agent and vanadium titano-magnetite titanium-selecting process |
| CN114713362B (en) * | 2022-04-21 | 2024-03-15 | 攀枝花学院 | Vanadium titano-magnetite titanium-separating flotation collector and vanadium titano-magnetite titanium-separating process |
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