CN102182254B - Manufacturing process of inorganic fireproof coiled material and inorganic fireproof coiled material - Google Patents

Manufacturing process of inorganic fireproof coiled material and inorganic fireproof coiled material Download PDF

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Publication number
CN102182254B
CN102182254B CN 201110021386 CN201110021386A CN102182254B CN 102182254 B CN102182254 B CN 102182254B CN 201110021386 CN201110021386 CN 201110021386 CN 201110021386 A CN201110021386 A CN 201110021386A CN 102182254 B CN102182254 B CN 102182254B
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China
Prior art keywords
inorganic
coiled material
fire
manufacture craft
material manufacture
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Expired - Fee Related
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CN 201110021386
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Chinese (zh)
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CN102182254A (en
Inventor
李月英
杨升辉
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Nantong Haoyige Textile Co ltd
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BEIJING SOLID BUILDING ENGINEERING Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/02Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
    • C04B28/04Portland cements

Abstract

The invention discloses a manufacturing process of an inorganic fireproof coiled material and the inorganic fireproof coiled material, and the manufacturing process comprises the following steps: (a) preparing raw materials; (b) putting 1.3-2.5kg of coagulation accelerator, 7-10.5kg of flame retardant, 0.7-1.2kg of modified cellulose ether, 175-200kg of cement, 350kg of calcium carbonate powder, 300kg of 70-140-mesh first-level sand, 1.5-2.0kg of 6mm polypropylene fiber and 2.0-2.5kg of organic silicon waterproof agent in the step (a) into a stirring machine for stirring, and then performing 150-mesh filtration; (c) putting 150-200kg of acrylic acid emulsion and 0.5-0.8kg of liquid defoamer in the step (a) into a reaction kettle, starting to stir, performing mixing, and then performing the 70-mesh filtration; (d) mixing liquid which is well filtered in the step (c) with powder which is well filtered in the step (b) to get inorganic slurry; (e) spray-coating the inorganic slurry; and (f) performing the drying process. The inorganic fireproof coiled material comprises an upper inorganic slurry layer, a lower inorganic slurry layer and a non-woven fabric layer positioned between the upper inorganic slurry layer and the lower inorganic slurry layer, the fire resistance grade is high, and the adhesive force with other products is strong.

Description

Inorganic fire coiled material manufacture craft and inorganic fire coiled material
Technical field
The inorganic fire coiled material that the present invention relates to a kind of inorganic fire coiled material manufacture craft and utilize inorganic fire coiled material manufacture craft to make.
Background technology
The fire resistance rating of insulation material of the prior art is low, pyrotechnics firecracker just can it be ignited (like CCTV's big fire); And water resistance is poor, and weatherability is poor.In addition, insulation material of the prior art and other products to attach adhesion ratio relatively poor, be difficult for attaching the higher fire proofing material of sticking one deck fire resistance rating above that to improve the fire resistance rating of insulation material.
Summary of the invention
To the deficiency that exists in the prior art; The object of the present invention is to provide and a kind ofly make the fire resistance rating height, attach the strong inorganic fire coiled material manufacture craft of viscous force, and a kind of inorganic fire coiled material that utilizes said inorganic fire coiled material manufacture craft to make is provided with other products; Inorganic fire coiled material of the present invention can attach sticking together well with insulation material and improve the fire resistance rating of insulation material.
Technical scheme of the present invention is achieved in that inorganic fire coiled material manufacture craft, comprises the steps:
(a) raw material is prepared: acrylic emulsion 150-200kg, coagulant 1.3-2.5kg, liquid antifoaming agent 0.5-0.8kg; Fire retardant 7-10.5kg, modified cellulose ethers 0.7-1.2kg, cement 175-200kg; Dicalcium powder 350kg; 70-140 purpose one-level sand 300kg, 6mm polypropylene fibre 1.5-2.0kg, waterproofing agent of organosilicon 2.0-2.5kg;
(b) the coagulant 1.3-2.5kg in the step (a), fire retardant 7-10.5kg, modified cellulose ethers 0.7-1.2kg, cement 175-200kg, dicalcium powder 350kg, 70-140 order one-level sand 300kg, 6mm polypropylene fibre 1.5-2.0kg and waterproofing agent of organosilicon 2.0-2.5kg are dropped into the mixer the inside and stir, carry out 150 orders then and filter;
(c) acrylic emulsion 150-200kg in the step (a) and liquid antifoaming agent 0.5-0.8kg are dropped in the agitated reactor, start to stir and mix, carry out 70 orders then and filter;
(d) filtering good liquid in the step (c), pour into and start mixer in the container, slowly add filtering good powder in the step (b) again, mix and stir inorganic slurry;
(e) inorganic slurry spraying: the smooth paving of nonwoven on coil production line head platform, is opened spraying paste system automatically, inorganic slurry is uniformly sprayed on two sides of nonwoven; (f) stoving process: open rolling layer pressure type drying system simultaneously, get the inorganic fire coiled material after the oven dry.
Above-mentioned inorganic fire coiled material manufacture craft, said cement is 42.5 cement.
Above-mentioned inorganic fire coiled material manufacture craft, said coagulant is: the early strong low temperature coagulant of magnesite.
Above-mentioned inorganic fire coiled material manufacture craft, said liquid antifoaming agent is: silicone defoaming agent.
Above-mentioned inorganic fire coiled material manufacture craft, said fire retardant be manganese dioxide, ammonium phosphate, antimony oxide, organophosphorus ester, phosphite ester, chloride phosphate, contain halocarbon, contain halogenohydrin, Halogen ester or Halogen ether.
Bake out temperature is 75-85 ℃ in the above-mentioned inorganic fire coiled material manufacture craft, said step (f); Drying time is 10 minutes.
Above-mentioned inorganic fire coiled material manufacture craft, said acrylic emulsion solid content 60 ± 1%, pH are 7-9, viscosity is 1000-2000cps.
The inorganic fire coiled material of the making of above-mentioned inorganic fire coiled material manufacture craft, comprise the inorganic slurry layer, down the inorganic slurry layer and on said inorganic slurry layer and said nonwoven layer between the inorganic slurry layer down.
Above-mentioned inorganic fire coiled material manufacture craft, said silicone defoaming agent are that silicone grease, emulsifying agent, waterproofing agent, thickening agent and water form through machinery emulsification.
The invention has the beneficial effects as follows: the inorganic fire coiled material fire resistance rating of utilizing inorganic fire coiled material manufacture craft of the present invention to make is high; Fire resistance rating can reach the A1 level; And to attach viscous force strong with other products, good waterproof performance, and pliability is very good; Do not contain harmful compositions such as asbestos fibre, sheerly environment-friendly products.Can be used for the insulating board for building composite coating, be used for improving timber intensity and fire-protection rating; Inorganic fire coiled material of the present invention can make the insulation material combustibility compound with it increase to B1 by B2.
Description of drawings
Fig. 1 is the structural representation of inorganic fire coiled material of the present invention.
Among the figure: the last inorganic slurry layer of 1-, inorganic slurry layer under the 2-, 3-nonwoven layer.
The specific embodiment
In conjunction with accompanying drawing the present invention is done further explanation:
As shown in Figure 1, inorganic fire coiled material manufacture craft comprises the steps:
(a) raw material is prepared: acrylic emulsion 150-200kg, coagulant 1.3-2.5kg, liquid antifoaming agent 0.5-0.8kg; Fire retardant 7-10.5kg, modified cellulose ethers 0.7-1.2kg, cement 175-200kg; Dicalcium powder 350kg; 70-140 purpose one-level sand 300kg, 6mm polypropylene fibre 1.5-2.0kg, waterproofing agent of organosilicon 2.0-2.5kg;
(b) the coagulant 1.3-2.5kg in the step (a), fire retardant 7-10.5kg, modified cellulose ethers 0.7-1.2kg, cement 175-200kg, dicalcium powder 350kg, 70-140 order one-level sand 300kg, 6mm polypropylene fibre 1.5-2.0kg and waterproofing agent of organosilicon 2.0-2.5kg are dropped into the mixer the inside and stir, carry out 150 orders then and filter;
(c) acrylic emulsion 150-200kg in the step (a) and liquid antifoaming agent 0.5-0.8kg are dropped in the agitated reactor, start to stir and mix, carry out 70 orders then and filter;
(d) filtering good liquid in the step (c), pour into and start mixer in the container, slowly add filtering good powder in the step (b) again, mix and stir inorganic slurry;
(e) inorganic slurry spraying: the smooth paving of nonwoven on coil production line head platform, is opened spraying paste system automatically, inorganic slurry is uniformly sprayed on two sides of nonwoven;
(f) stoving process: open rolling layer pressure type drying system simultaneously, get the inorganic fire coiled material after the oven dry.
Said cement is 42.5 cement; Said coagulant is the early strong low temperature coagulant of magnesite; Said liquid antifoaming agent is a silicone defoaming agent; Said fire retardant is manganese dioxide, ammonium phosphate, antimony oxide, organophosphorus ester, phosphite ester, chloride phosphate, contain halocarbon, contain halogenohydrin, Halogen ester or Halogen ether; Bake out temperature is 75-85 ℃ in the said step (f), and drying time is 10 minutes; Said acrylic emulsion solid content 60 ± 1%, pH are 7-9, and viscosity is 1000-2000cps; Said silicone defoaming agent is that silicone grease, emulsifying agent, waterproofing agent, thickening agent and water form through machinery emulsification.
The inorganic fire coiled material that the inorganic fire coiled material manufacture craft of present embodiment is produced comprise inorganic slurry layer 1, down inorganic slurry layer 2 and on said inorganic slurry layer 1 and said nonwoven layer 3 between the inorganic slurry layer 2 down; The inorganic fire coiled material fire-protection rating of present embodiment reaches the A1 level, and to attach viscous force strong and pliability is very good with other products, and fire protecting performance is good, does not contain harmful compositions such as asbestos fibre, sheerly environment-friendly products.Can be used for the insulating board for building composite coating, be used for improving timber intensity and fire-protection rating; The inorganic fire coiled material of present embodiment can make the insulation material combustibility compound with it increase to B1 by B2.

Claims (8)

1. inorganic fire coiled material manufacture craft is characterized in that, comprises the steps:
(a) raw material is prepared: acrylic emulsion 150-200kg, coagulant 1.3-2.5kg, liquid antifoaming agent 0.5-0.8kg; Fire retardant 7-10.5kg, modified cellulose ethers 0.7-1.2kg, cement 175-200kg; Dicalcium powder 350kg; 70-140 purpose one-level sand 300kg, 6mm polypropylene fibre 1.5-2.0kg, waterproofing agent of organosilicon 2.0-2.5kg;
(b) the coagulant 1.3-2.5kg in the step (a), fire retardant 7-10.5kg, modified cellulose ethers 0.7-1.2kg, cement 175-200kg, dicalcium powder 350kg, 70-140 order one-level sand 300kg, 6mm polypropylene fibre 1.5-2.0kg and waterproofing agent of organosilicon 2.0-2.5kg are dropped into the mixer the inside and stir, carry out 150 orders then and filter;
(c) acrylic emulsion 150-200kg in the step (a) and liquid antifoaming agent 0.5-0.8kg are dropped in the agitated reactor, start to stir and mix, carry out 70 orders then and filter;
(d) filtering good liquid in the step (c), pour into and start mixer in the container, slowly add filtering good powder in the step (b) again, mix and stir inorganic slurry;
(e) inorganic slurry spraying: the smooth paving of nonwoven on coil production line head platform, is opened spraying paste system automatically, inorganic slurry is uniformly sprayed on two sides of nonwoven;
(f) stoving process: open rolling layer pressure type drying system simultaneously, get the inorganic fire coiled material after the oven dry.
2. inorganic fire coiled material manufacture craft according to claim 1 is characterized in that said cement is 42.5 cement.
3. inorganic fire coiled material manufacture craft according to claim 1 is characterized in that, said coagulant is the early strong low temperature coagulant of magnesite.
4. inorganic fire coiled material manufacture craft according to claim 1 is characterized in that said liquid antifoaming agent is a silicone defoaming agent.
5. inorganic fire coiled material manufacture craft according to claim 1 is characterized in that, said fire retardant is manganese dioxide, ammonium phosphate, antimony oxide, organophosphorus ester, phosphite ester, chloride phosphate, contain halocarbon, contain halogenohydrin, Halogen ester or Halogen ether.
6. inorganic fire coiled material manufacture craft according to claim 1 is characterized in that, bake out temperature is 75-85 ℃ in the said step (f); Drying time is 10 minutes.
7. according to the arbitrary described inorganic fire coiled material manufacture craft of claim 1-6, it is characterized in that said acrylic emulsion solid content 60 ± 1%, pH are 7-9, viscosity is 1000-2000cps.
8. the inorganic fire coiled material made of the arbitrary said inorganic fire coiled material manufacture craft of claim 1-7; It is characterized in that, comprise inorganic slurry layer (1), following inorganic slurry layer (2) and be positioned at said inorganic slurry layer (1) and the said nonwoven layer (3) between the inorganic slurry layer (2) down of going up.
CN 201110021386 2011-01-19 2011-01-19 Manufacturing process of inorganic fireproof coiled material and inorganic fireproof coiled material Expired - Fee Related CN102182254B (en)

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Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103159438B (en) * 2013-03-29 2015-03-18 上海克络蒂材料科技发展有限公司 Low-viscosity flexible polymer cement and fiber reinforcement fireproof coiled material
CN103951893B (en) * 2014-05-15 2016-09-21 精碳伟业(北京)科技有限公司 Fireproof coiled materials on steel structure and preparation method thereof
CN105952079B (en) * 2016-06-01 2018-09-28 深圳迈辽技术转移中心有限公司 A kind of ecologic coating coiled material and preparation method thereof for directly pasting interior wall
CN110215629B (en) * 2019-06-20 2021-03-26 山东鲁阳节能材料股份有限公司 Fireproof heat absorption blanket and preparation method thereof
CN111779183A (en) * 2020-08-10 2020-10-16 中盛节能科技有限公司 Cement-based back lining with heat reflection capacity and manufacturing method thereof
CN113530117A (en) * 2021-08-12 2021-10-22 北京赛博思工程技术研究院 Mineral core fireproof refrigeration organic heat insulation composite board

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4320439A1 (en) * 1992-06-22 1993-12-23 Yhtyneet Paperitehtaat Oy Valk Insulating material for building - comprises mineral fibre layer to which top surface of holed plastic is connected
CN101219903A (en) * 2007-12-05 2008-07-16 北京瑞泰高温材料科技股份有限公司 Advanced silica refractory and manufacturing technique thereof
CN101407687A (en) * 2008-06-05 2009-04-15 北京冶建新技术公司 Quick-drying type composite water-proof paint and preparation thereof
CN201350711Y (en) * 2009-02-11 2009-11-25 厉朝岳 Compound flexible fireproofing coiled material
CN101769021A (en) * 2009-12-29 2010-07-07 高永利 Inflaming retarding flame-repellent foam core compound light partition wall

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4320439A1 (en) * 1992-06-22 1993-12-23 Yhtyneet Paperitehtaat Oy Valk Insulating material for building - comprises mineral fibre layer to which top surface of holed plastic is connected
CN101219903A (en) * 2007-12-05 2008-07-16 北京瑞泰高温材料科技股份有限公司 Advanced silica refractory and manufacturing technique thereof
CN101407687A (en) * 2008-06-05 2009-04-15 北京冶建新技术公司 Quick-drying type composite water-proof paint and preparation thereof
CN201350711Y (en) * 2009-02-11 2009-11-25 厉朝岳 Compound flexible fireproofing coiled material
CN101769021A (en) * 2009-12-29 2010-07-07 高永利 Inflaming retarding flame-repellent foam core compound light partition wall

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Effective date of registration: 20201111

Address after: 226000 No.165, South Renmin Road, Yudong Town, Haimen City, Nantong City, Jiangsu Province

Patentee after: HAIMEN BIWEI INTELLECTUAL PROPERTY SERVICE Co.,Ltd.

Address before: 101109 Beijing city town Huoxian Tongzhou District Huang Pu Cun East factory

Patentee before: BEIJING SOLID BUILDING ENGINEERING Co.,Ltd.

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Effective date of registration: 20220309

Address after: 226000 No.7, Xinuo Road, Yudong Town, Haimen District, Haimen City, Nantong City, Jiangsu Province

Patentee after: Nantong haoyige Textile Co.,Ltd.

Address before: No.165, Renmin South Road, Yudong Town, Haimen City, Nantong City, Jiangsu Province, 226000

Patentee before: HAIMEN BIWEI INTELLECTUAL PROPERTY SERVICE Co.,Ltd.

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Granted publication date: 20120523

Termination date: 20220119