CN102181950A - Preparation method of super-bright and showy special polyester fully-drawn mixed fiber filament for fabric tape - Google Patents
Preparation method of super-bright and showy special polyester fully-drawn mixed fiber filament for fabric tape Download PDFInfo
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- CN102181950A CN102181950A CN2011100774051A CN201110077405A CN102181950A CN 102181950 A CN102181950 A CN 102181950A CN 2011100774051 A CN2011100774051 A CN 2011100774051A CN 201110077405 A CN201110077405 A CN 201110077405A CN 102181950 A CN102181950 A CN 102181950A
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Abstract
The invention discloses a preparation method of a super-bright and showy special polyester fully-drawn mixed fiber filament for a fabric tape, which comprises the following steps of: (1) pre-crystallizing materials, wherein the materials are super-bright PET slices, and the dried hot air is concretely used for pre-crystallizing; (2) feeding the materials in a screw way: feeding the dried PET slices into a screw extruder by electromagnetic vibration; (3) filtering: filtering the mixture extruded by the extruder under the condition that the continuous production of spinning filaments and the constant pressure of the screw extruder are ensured; and (4) spinning: enabling the mixture taken out of the filter to enter a spinning component with a mixed spinneret orifice of a trilobal orifice and a circular orifice, spouting through a spinneret plate of the mixed spinneret orifice of the spinning component, and then, drawing, sizing and winding for molding. The super-bright and showy special polyester fully-drawn mixed fiber filament for the fabric tape, which is prepared by the preparation method disclosed by the invention, has higher brightness, soft fabric feeling and bright and showy color after dyeing, the performance of the mixed fiber filament is very similar to the performance of polyamide, and the mixed fiber filament is an ideal substitute of a polyamide fabric tape filament.
Description
Technical field
The invention belongs to the fiber production technical field, the full drawing-off of the gorgeous ribbon special polyester of particularly a kind of PET superbright mixes the preparation method of fine long filament.
Background technology
It is last word in the market that the full drawing-off of the gorgeous ribbon special polyester of PET superbright mixes fine long filament, on ribbon silk market, belong to high-end product, but there is following defective in it: 1) its brightness and pliability are difficult to take into account simultaneously, high its pliability of long filament of brightness is not enough, and its brightness of long filament that pliability is good is darker; 2) elongation at break is low, and feel is not good.
Summary of the invention
The object of the present invention is to provide the full drawing-off of the gorgeous ribbon special polyester of a kind of PET superbright to mix the preparation method of fine long filament.
Realize that the technology of the present invention solution is: the full drawing-off of the gorgeous ribbon special polyester of a kind of PET superbright mixes the preparation method of fine long filament, may further comprise the steps:
Step 1, material is carried out pre-crystallization, described material PET section; The concrete heated drying air that adopts is carried out pre-crystallization;
Step 2, the feeding of material screw; The PET section that drying is good is sent in the screw extruder with electric and magnetic oscillation;
Step 3, filtration are filtered the fused mass after the extruder extruding, guarantee the constant of continuous production spinning and screw extruder pressure when filtering;
Step 4, spinning, fused mass after coming out from filter enters spinning manifold, spray from mixing spinneret hole by spinning manifold, carry out drawing-off, typing, coiling and molding afterwards, wherein said spinnerets is provided with the spinneret orifice that is shaped as triangle, circle, and the preceding strand of reeling is introduced into the dual network nozzle and adds network.
The quantitative proportion of described triangle spinneret orifice and circular spinneret orifice is 8-30: 1.
When step 1 was carried out pre-crystallization with material, the temperature of pre-crystallization was 168~178 ℃, and the temperature of heated drying air is 170~178 ℃, and air dew point is smaller or equal to-60 ℃, and material moisture is 30ppm, and be 5~8 hours drying time.
The screen pack that filters filter device therefor when step 3 is filtered is 25 microns.
The spinneret orifice that step 4 is sprayed silk is special-shaped spinneret orifice of three unique leaves and round spinneret orifice mixed type spinnerets, described filament spinning component is 30/120/150/400/250/400 purpose screen pack, temperature during spinning is 288~298 ℃, spinning speed is 4300~4500 meters/minute, the wind speed of cooling quench is 0.4~0.6m/s, wind-warm syndrome is 23~25 ℃, and relative humidity is 70~80%.
Spinning manifold in the step 4 adopts the slow cooling heater.
According to technique scheme, product of the present invention has the following advantages:
1) color and luster brilliance is gorgeous: this project adopts the spinning manifold that has the slow cooling heating, special-shaped spinneret orifice shape spinnerets of three unique leaves and circular hole production, and finished product strand cross sectional shape major part is an equilateral triangle, and brightness is higher, and dyeing back bright in color is gorgeous.
2) soft exquisiteness: most of fibre section is an equilateral triangle in this combined yarn, and the sub-fraction fibre section is circular, soft, fine and smooth, smooth.
3) elongation at break is higher: when we develop this product, adopted comparatively advanced equipment having the spinning manifold production of slow cooling heater, take unique process for high speed spin-drawing one-step method to finish, has higher elongation at break, its elongation at break reaches 36% ± 2, and common long filament only is 26% ± 4
Exempt from starching when 4) weaving: adopt during production to add pre-network and then drawing-off and HEAT SETTING earlier, strand enters the dual network nozzle and adds network before coiling, and the network degree is more, reaches 16-20/m, conventional long filament only be 8-12 individual/m.
The present invention compared with prior art, the mixed fine long filament of being made by PET of the full drawing-off of the gorgeous ribbon special polyester of superbright has some total character of polyester fiber, but the excellent ribbon silk of making at PET is simpler than the production of polyamide fibre ribbon silk, cost of material is lower, the finished silk price is low, performance is similar to polyamide fibre, after spinning through drawing-off, HEAT SETTING, add network one step and finish, make the fiber made not only have bright color but also have the feel of soft and smooth property.Concrete advantage is as follows: the silk brightness of 1) spinning is higher, and dyeing back bright in color is gorgeous, plays fabulous decoration function when making gift wrap; 2) fiber and goods thereof is soft, because elongation is bigger, soft comfortable when making product; 3) have good dyeability, can be used for common DISPERSE DYES and carry out boiling dyeing at normal pressure and need not carrier, dye to such an extent that fiber COLOR FASTNESS and oxygen resistence are strong; 4) have good chemical proofing, light resistance and heat resistance; 5) fiber never fades.
The specific embodiment
The full drawing-off of the gorgeous ribbon special polyester of a kind of PET superbright of invention mixes the preparation method of fine long filament, be PET section to be given entering in the screw extruder behind the crystallizing and drying melt extrude, carry out spinning through mixing the spinneret orifice spinning head, tow enters the GR1 predraft through the blowing cooling and stretches through GR1 and GR2, typing, winding head are reeled, and promptly obtain the gorgeous ribbon special polyester of PET superbright full-drawn yarn and mix long filament.Specifically may further comprise the steps:
Step 1, material is carried out pre-crystallization, described material is the PET section; The concrete heated drying air that adopts is carried out pre-crystallization; When material was carried out pre-crystallization, the temperature of pre-crystallization was 168~178 ℃, and the temperature temperature of heated drying air is 170~178 ℃, and air dew point is smaller or equal to-60 ℃, and material moisture is 30ppm, and be 5~8 hours drying time.
The feeding of step 2, material screw: with the PET heated-air drying of cutting into slices, afterwards with the PET section by in the electric and magnetic oscillation feeding screw extruder; Described material is PET (polyethylene terephthalate) section.
Step 3, filtration are filtered the fused mass after the extruder extruding, guarantee the constant of continuous production spinning and screw extruder pressure when filtering; The screen pack of filter device therefor is 25 microns during filtration.
Step 4, spinning, the fused mass after coming out from filter enters filament spinning component, by the mixing spinneret hole ejection of trefoil hole and circular port, carries out small scale drawing-off, typing, coiling and molding afterwards, and strand is introduced into the dual network nozzle and adds network before reeling.
Spinneret orifice is special-shaped spinneret orifice of three leaves and circular spinneret orifice mixed type spinnerets, described filament spinning component is 30/120/150/400/250/400 purpose screen pack, temperature during spinning is 290~298 ℃, spinning speed is 4300~4500 meters/minute, the wind speed of cooling quench is 0.6~0.8m/s, wind-warm syndrome is 23~25 ℃, and relative humidity is 70~80%.
The ribbon silk that the present invention produces mixes the alternative chinlon filament of fine long filament and is applicable to all kinds of packing adornments etc.Below in conjunction with embodiment the present invention is done further detailed description:
Embodiment 1
The gorgeous ribbon special polyester of a kind of PET superbright full-drawn yarn mixes the preparation method of fine long filament, may further comprise the steps:
Step 1, material is carried out pre-crystallization, described material PET section; The concrete heated drying air that adopts is carried out pre-crystallization; When material was carried out pre-crystallization, pre-crystallization temperature was 168 ℃, and the temperature of heated drying air is 170 ℃, and air dew point is-60 ℃, and material moisture is 30ppm, and be 8 hours drying time.
Step 2, the feeding of material screw: at first with the PET heated-air drying, afterwards that drying is good PET section is by in the electric and magnetic oscillation feeding screw extruder; When the material screw was fed, described material was PET (polyethylene terephthalate) section.
Step 3, filtration are filtered the fused mass after the extruder extruding, guarantee the constant of continuous production spinning and screw extruder pressure when filtering; The screen pack of filter device therefor is 25 microns during filtration.
Step 4, spinning, fused mass after coming out from filter enters filament spinning component, mixing spinneret hole ejection by trefoil hole and circular port, wherein the quantitative proportion of triangle spinneret orifice and circular spinning nozzle is 8: 1, carry out the GR1 predraft afterwards and stretch typing, winding head winding shaping again through GR1 and GR2.The spinneret orifice that sprays silk is the special-shaped spinneret orifice of three leaves and two kinds of mix aperture of circular port, described filament spinning component is 30/120/150/400/250/400 purpose screen pack, temperature during spinning is 294 ℃, spinning speed is 4300 meters/minute, the wind speed of cooling quench is 0.6m/s, wind-warm syndrome is 25 ℃, and relative humidity is 70%.
Embodiment 2
The gorgeous ribbon special polyester of a kind of PET superbright full-drawn yarn fiber preparation method may further comprise the steps:
Step 1, material is carried out pre-crystallization, described material is the PET section; The concrete heated drying air that adopts is carried out pre-crystallization; When material was carried out pre-crystallization, pre-crystallization temperature was 172 ℃, and the temperature of heated drying air is 172 ℃, and air dew point is-56 ℃, and material moisture is 30ppm, and be 6 hours drying time.
The feeding of step 2, material screw: with the PET heated-air drying of cutting into slices, afterwards that drying is good PET section is by in the electric and magnetic oscillation feeding screw extruder; When the material screw was fed, described material was PET (polyethylene terephthalate) section.
Step 3, filtration are filtered the fused mass after the extruder extruding, guarantee the constant of continuous production spinning and screw extruder pressure when filtering; The screen pack of filter device therefor is 25 microns during filtration.
Step 4, spinning, fused mass after coming out from filter enters filament spinning component, mixing spinneret hole ejection by trefoil hole and circular port, wherein the quantitative proportion of triangle spinneret orifice and circular spinning nozzle is 30: 1, carry out the GR1 predraft afterwards and stretch typing, winding head winding shaping again through GR1 and GR2.The spinneret orifice that sprays silk is the special-shaped spinneret orifice of three leaves and two kinds of mix aperture of circular port, described filament spinning component is 30/120/150/400/250/400 purpose screen pack, temperature during spinning is 296 ℃, spinning speed is 4400 meters/minute, the wind speed of cooling quench is 0.7m/s, wind-warm syndrome is 26 ℃, and relative humidity is 80%.
Embodiment 3
The gorgeous ribbon special polyester of a kind of PET superbright full-drawn yarn fiber preparation method may further comprise the steps:
Step 1, material is carried out pre-crystallization, described material is the PET section; The concrete heated drying air that adopts is carried out pre-crystallization; When material was carried out pre-crystallization, pre-crystallization temperature was 174 ℃, and the temperature of heated drying air is 174 ℃, and air dew point is-60 ℃, and material moisture is 5 hours for 30ppm drying time.
The feeding of step 2, material screw: with the PET heated-air drying of cutting into slices, afterwards that drying is good PET section is by in the electric and magnetic oscillation feeding screw extruder; When the material screw was fed, described material was PET (polyethylene terephthalate) section.
Step 3, filtration are filtered the fused mass after the extruder extruding, guarantee the constant of continuous production spinning and screw extruder pressure when filtering; The screen pack of filter device therefor is 25 microns during filtration.
Step 4, spinning, fused mass after coming out from filter enters filament spinning component, mixing spinneret hole ejection by trefoil hole and circular port, wherein the quantitative proportion of triangle spinneret orifice and circular spinning nozzle is 20: 1, carry out the GR1 predraft afterwards and stretch typing, winding head winding shaping again through GR1 and GR2.The spinneret orifice that sprays silk is the special-shaped spinneret orifice of three leaves and two kinds of mix aperture of circular port, described filament spinning component is 30/120/150/400/250/400 purpose screen pack, temperature during spinning is 296 ℃, spinning speed is 4500 meters/minute, the wind speed of cooling quench is 0.8m/s, wind-warm syndrome is 24 ℃, and relative humidity is 75%.
Claims (6)
1. the full drawing-off of the gorgeous ribbon special polyester of superbright mixes the preparation method of fine long filament, it is characterized in that, may further comprise the steps:
Step 1, material is carried out pre-crystallization, described material PET section; The concrete heated drying air that adopts is carried out pre-crystallization;
Step 2, the feeding of material screw; The PET section that drying is good is sent in the screw extruder with electric and magnetic oscillation;
Step 3, filtration are filtered the fused mass after the extruder extruding, guarantee the constant of continuous production spinning and screw extruder pressure when filtering;
Step 4, spinning, fused mass after coming out from filter enters spinning manifold, spray from mixing spinneret hole by spinning manifold, carry out drawing-off, typing, coiling and molding afterwards, wherein said spinnerets is provided with the spinneret orifice that is shaped as triangle, circle, and the preceding strand of reeling is introduced into the dual network nozzle and adds network.
2. the full drawing-off of the gorgeous ribbon special polyester of superbright according to claim 1 mixes the preparation method of fine long filament, it is characterized in that the quantitative proportion of described triangle spinneret orifice and circular spinneret orifice is 8-30: 1.
3. the full drawing-off of the gorgeous ribbon special polyester of superbright according to claim 1 and 2 mixes the preparation method of fine long filament, it is characterized in that, when step 1 is carried out pre-crystallization with material, the temperature of pre-crystallization is 168~178 ℃, the temperature of heated drying air is 170~178 ℃, air dew point is smaller or equal to-60 ℃, and material moisture is 30ppm, and be 5~8 hours drying time.
4. the full drawing-off of the gorgeous ribbon special polyester of superbright according to claim 1 and 2 mixes the preparation method of fine long filament, it is characterized in that, the screen pack that filters filter device therefor when step 3 is filtered is 25 microns.
5. the full drawing-off of the gorgeous ribbon special polyester of superbright according to claim 1 and 2 mixes the preparation method of fine long filament, it is characterized in that, the spinneret orifice that step 4 is sprayed silk is special-shaped spinneret orifice of three unique leaves and round spinneret orifice mixed type spinnerets, described filament spinning component is 30/120/150/400/250/400 purpose screen pack, temperature during spinning is 288~298 ℃, spinning speed is 4300~4500 meters/minute, the wind speed of cooling quench is 0.4~0.6m/s, wind-warm syndrome is 23~25 ℃, and relative humidity is 70~80%.
6. the full drawing-off of the gorgeous ribbon special polyester of superbright according to claim 1 and 2 mixes the preparation method of fine long filament, it is characterized in that, the spinning manifold in the step 4 adopts the slow cooling heater.
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Citations (10)
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JPH02251610A (en) * | 1989-03-27 | 1990-10-09 | Unitika Ltd | Production of polyester yarn |
CN1403638A (en) * | 2001-09-13 | 2003-03-19 | 中国石化上海石油化工股份有限公司 | Hot-pipe spinning process of producing composite Dacron filament with special shape and different shrinkage |
CN1403639A (en) * | 2001-09-13 | 2003-03-19 | 中国石化上海石油化工股份有限公司 | Production process of composite Dacron filament with special shape, different fiber and different shrinkage |
CN1403634A (en) * | 2001-09-13 | 2003-03-19 | 中国石化上海石油化工股份有限公司 | Production process of composite Dacron filament with special shape and different shrinkage |
CN1403636A (en) * | 2001-09-13 | 2003-03-19 | 中国石化上海石油化工股份有限公司 | Production process of composite Dacron filament with special shape, different fiber and different shrinkage |
CN1936126A (en) * | 2006-09-28 | 2007-03-28 | 陈泉锋 | Production method for spinning polyester preoriented yarn by reusing polyester bottle chip |
CN1970854A (en) * | 2005-11-22 | 2007-05-30 | 东丽纤维研究所(中国)有限公司 | Water-absorbent rapid-dry impermeable profile mixed fiber terylen filament and method for producing same |
CN101050552A (en) * | 2007-04-10 | 2007-10-10 | 江苏三鑫化纤有限公司 | Single stage drawing method for terylene continuous yarn filament in use for meshbelt, and preparation |
CN101638813A (en) * | 2009-08-25 | 2010-02-03 | 江苏菲霖纤维科技有限公司 | Producing method for spinning heterogeneous colored terylene preoriented continuous yarn by recycled polyester bottle sheet materials |
CN101760794A (en) * | 2009-12-11 | 2010-06-30 | 仪征市星海化纤有限公司 | Preparation method of cationic heat-absorbing and perspiration superfine fibres |
-
2011
- 2011-03-30 CN CN2011100774051A patent/CN102181950A/en active Pending
Patent Citations (10)
Publication number | Priority date | Publication date | Assignee | Title |
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JPH02251610A (en) * | 1989-03-27 | 1990-10-09 | Unitika Ltd | Production of polyester yarn |
CN1403638A (en) * | 2001-09-13 | 2003-03-19 | 中国石化上海石油化工股份有限公司 | Hot-pipe spinning process of producing composite Dacron filament with special shape and different shrinkage |
CN1403639A (en) * | 2001-09-13 | 2003-03-19 | 中国石化上海石油化工股份有限公司 | Production process of composite Dacron filament with special shape, different fiber and different shrinkage |
CN1403634A (en) * | 2001-09-13 | 2003-03-19 | 中国石化上海石油化工股份有限公司 | Production process of composite Dacron filament with special shape and different shrinkage |
CN1403636A (en) * | 2001-09-13 | 2003-03-19 | 中国石化上海石油化工股份有限公司 | Production process of composite Dacron filament with special shape, different fiber and different shrinkage |
CN1970854A (en) * | 2005-11-22 | 2007-05-30 | 东丽纤维研究所(中国)有限公司 | Water-absorbent rapid-dry impermeable profile mixed fiber terylen filament and method for producing same |
CN1936126A (en) * | 2006-09-28 | 2007-03-28 | 陈泉锋 | Production method for spinning polyester preoriented yarn by reusing polyester bottle chip |
CN101050552A (en) * | 2007-04-10 | 2007-10-10 | 江苏三鑫化纤有限公司 | Single stage drawing method for terylene continuous yarn filament in use for meshbelt, and preparation |
CN101638813A (en) * | 2009-08-25 | 2010-02-03 | 江苏菲霖纤维科技有限公司 | Producing method for spinning heterogeneous colored terylene preoriented continuous yarn by recycled polyester bottle sheet materials |
CN101760794A (en) * | 2009-12-11 | 2010-06-30 | 仪征市星海化纤有限公司 | Preparation method of cationic heat-absorbing and perspiration superfine fibres |
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Application publication date: 20110914 |