CN105839209A - Process for processing same-spinneret bi-color ultrafine composite polyester fibers - Google Patents
Process for processing same-spinneret bi-color ultrafine composite polyester fibers Download PDFInfo
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- CN105839209A CN105839209A CN201610355460.5A CN201610355460A CN105839209A CN 105839209 A CN105839209 A CN 105839209A CN 201610355460 A CN201610355460 A CN 201610355460A CN 105839209 A CN105839209 A CN 105839209A
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- Prior art keywords
- island
- colored
- sea
- polyester fiber
- double
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Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/28—Formation of filaments, threads, or the like while mixing different spinning solutions or melts during the spinning operation; Spinnerette packs therefor
- D01D5/30—Conjugate filaments; Spinnerette packs therefor
- D01D5/36—Matrix structure; Spinnerette packs therefor
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D10/00—Physical treatment of artificial filaments or the like during manufacture, i.e. during a continuous production process before the filaments have been collected
- D01D10/02—Heat treatment
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/04—Pigments
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/14—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyester as constituent
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Multicomponent Fibers (AREA)
Abstract
The invention relates to a process for processing same-spinneret bi-color ultrafine composite polyester fibers and belongs to the technical field of generation of continuous yarns. The process comprises the steps of taking alkali-soluble copolyester as a sea ingredientcomponent, taking PET-1 and PET-3 as island componentingredients, separately subjecting the sea componentingredient and the island ingredientcomponents to screw extruded melting, conveying and metering, enabling the melting to enter a conjugate spinning box body and a specially-designed three-ingredientcomponent spinning assembly, separately ejecting bi-color sea-island composite melting from the left and right sides of the same- spinneret, and carrying out a one-step-method spinning method, which comprises the steps of carrying out cooling, carrying out oiling, carrying out drawing, carrying out thermoforming and carrying out winding, thereby preparing bi-color sea-island polyester FDY (Fully Drawn Yarn). By applying the process to the a the processing of sea-island yarns, the process has the advantages of a short production flow, a good product quality, energy saving, environment-friendliness and the like.
Description
Technical field
The present invention relates to the processing technique of a kind of same plate double-colored superfine composite polyester fiber, belong to long filament generation technique
Field.
Background technology
Sea-island composite fiber, compared with general fibre, has minimum line density and high-specific surface area, is made into
Fabric has the characteristics such as high spreadability, soft, comfortable and easy to wear, tone is soft, be widely used in suede nap,
Imitative peach face, superfine fiber leather base fabric, highly dense waterproof fabric, high-performance cleaning cloth, high-performance suction strainer material
Deng production, become the product that added value is higher.Island superfine fiber has above-mentioned numerous premium properties and use
While Tu, there is also following deficiency: be 1. difficult to dye dark color: sea-island composite fiber, due to fiber finer, compares table
Area is big, and the colour developing efficiency of dyestuff is low, i.e. color rendering properties is poor.In order to obtain the same color degree of depth, superfine fibre contaminates
Color often wants several times higher than general fibre by amount of dye, obtains dark product surely even if so also differing, as deeply
Black, dark blue etc.；2. dyefastness is poor: the dyefastness of superfine fibre textile is typically poor than conventional fibre, bag
Include sun-proof, washable and fastness to sublimation.The main still fiber finer of its reason, specific surface area are big, therefore to select
The dyeing that color fastness is good, and the dye species that really can promote island-in-sea fabric color fastness at present is little.
Application number 201310146982.0 discloses " preparation method of a kind of atrous island polyester fully drawn yarn ",
By adding the original liquid coloring technology of black agglomerate, it is achieved that the production of atrous island superfine fiber.But mesh
During road application front and back, often by black island and white sea-island fibre network again plying, to produce, there is special color
Color effect and the fabric of style.This two step method plying the method for silk, need to through debatching, network combined, roll up again
Around process, there is the drawback such as technological process length, impaired, the cost increase of product quality.
Based on this, make the application.
Summary of the invention
For the deficiencies in the prior art, it is provided that the processing technique of a kind of double-colored polyester fiber of same plate, this technique is adopted
With composite spinning equipment and three component filament spinning components of particular design, spray double-colored island from same spinneret multiple
Close melt, cooled, oil, drawing-off, thermal finalization, the single step spining method of winding, prepare double-colored island
Polyester FDY (drafting silk).
For achieving the above object, the technical scheme that the application takes is as follows:
The processing technique of a kind of double-colored polyester fiber of same plate, using alkali soluble copolymer polyester (COPET) as common
Sea component, normal polyester (PET) melt is one of them island component, adds in normal polyester (PET)
The melt of a certain proportion of color grain is another island component, and wherein color grain is preferably pitch black master batch；Sea
Component and 2 island components melt respectively through screw extruding, carry, measure, and enter composite spinning casing and spy
Three component filament spinning components of different design, spray double-colored island respectively from the left and right sides of same spinneret compound molten
Body, cooled, oil, drawing-off, thermal finalization, winding, prepare double-colored island polyester fiber.
Main technical process and parameter include:
(1) Masterbatch raw material and dry pretreatment
Selection white carbon black active ingredient is 25%, the carbon black dispersion phase particle diameter master batch less than 300nm, utilizes continuously
Small-sized pad device, control hot blast temperature 120～130 DEG C, make master batch moisture content less than 80ppm.
(2) preparation of the double-colored sea-island FDY of composite spinning
The intrinsic viscosity central value of 1. sea component: COPET is 0.70dl/g, and dry section moisture content is less than 50
Ppm, screw rod each district temperature 260～280 DEG C.
2. the intrinsic viscosity central value of island component one: PET-3 is 0.685dl/g, and dry section moisture content is less than 50
Ppm, island is combined ratio 20～30:80～70.Screw rod each district temperature 270～290 DEG C.
3. the intrinsic viscosity central value of island component two: PET-1 is 0.685dl/g, and dry section moisture content is less than 50
ppm。
4. black Masterbatch adds 6～15wt% (relative to island components), island compound than 20～30:80～
70, screw rod each district temperature 270～290 DEG C.
5. spinning body temperature 270～295 DEG C, cross air blasting wind speed 0.4～0.6m/s；First hot-rolling speed
2000～2500m/min, temperature 70-90 DEG C；Second hot-rolling speed 4200～4500m/min, temperature
130-150℃；Oil applying rate 0.8～1.0%, prepares black island and the fiber number of white sea island filament and hole count scope
Being 50～150dtex/12～24f × 37i, total specification is the double-colored (black of 100～300dtex/24～48f × 37i
Sea-island FDY in vain).
The operation principle of the present invention and having the beneficial effect that:
(1) use composite spinning equipment and three component filament spinning components of particular design, spray from same spinneret
Go out double-colored island compounding flux, cooled, oil, drawing-off, thermal finalization, the single step spining method of winding,
Prepare double-colored island polyester fiber (FDY).One pack system need to be prepared respectively with general double-colored island superfine fiber
Or monochrome sea-island fibre, the two step method using network to pool capital the most again is different, and the technological process of production shortens, product
Quality advance, cost reduce.With this fiber can direct woven into fabric, after Alkali reduction, be not required to carry out again rear road
Dyeing, i.e. can get black and white double-colored island superfine fiber fabric.Eliminate poststaining operation simultaneously, be one more
Add environmental protection, the energy-conservation mode of production.
(2) melt using alkali soluble copolymer polyester (COPET) as common sea component, normal polyester (PET)
Body is one of them island component, and the melt being added with Masterbatch in normal polyester (PET) is another island component,
Use composite spinning equipment and three component filament spinning components of particular design, spray double-colored island from same spinneret
Compounding flux, cooled, oil, drawing-off, thermal finalization, the single step spining method of winding, prepare double-colored sea
Island polyester fiber (FDY).The fabric being made into this fiber, after Alkali reduction, is not required to carry out the dyeing of rear road again,
I.e. can get double-colored island superfine fiber fabric.Sea component is alkali soluble copolymer polyester, and island component is constituted by two kinds,
One is non-staining PET-3, and a kind of is the PET-1 of coloring, and the island component that two kinds of colors are different imparts fibre
Tieing up double-colored effect, melt is after the spinneret that spinneret orifice subregion is arranged, in the left and right sides of spinneret, simultaneously
Form the polyester fiber with dichromatism, thus realize the double-colored processing of plate.
Accompanying drawing explanation
Fig. 1 is the structural representation of three component filament spinning component spinnerets in the application；
Fig. 2 is the process chart of the application.
Wherein label: 1. spinneret；2. spinneret orifice；21. spinneret orifices one；22. spinneret orifices two.
Detailed description of the invention
The fiber of the application is made up of sea component and island component, and sea component is alkali soluble copolymer polyester COPET, island group
Dividing and be made up of two parts, a part is that another part is coloured for interpolation without adding conventional PET-3 (the most colourless)
After the conventional PET-1 (the most coloured) of master batch, PET-1 crystallized dry-1, send into screw rod together with Masterbatch
Extruder-1 melt extrudes sea component melt, in dosing pump-1 sends into three component filament spinning components, meanwhile,
COPET → crystallizing and drying-2 → screw extruder-2 → dosing pump-2, PET-3 → crystallizing and drying-3 → screw extruding
The Liang Gu island component melt that machine-3 → dosing pump-3 is formed sends into three component spinning groups together with sea component melt
In part, the spinneret of this filament spinning component is as it is shown in figure 1, the spinneret orifice 2 on spinneret 1 is divided into spinneret orifice one (21)
With spinneret orifice two (22) two district, melt is extruded by the spinneret orifice 2 of both sides, extrudes black melt respectively and white melts
Body, then cool down through cross air blasting, oil, GR1, GR2, FDY winding i.e. forms double-colored island composite filament, specifically
Technological process is shown in Figure 2.
The elaboration of technical scheme is carried out below in conjunction with specific embodiment.
Embodiment 1
The present embodiment is the processing technique of a kind of double-colored polyester fiber of same plate, the intrinsic viscosity of sea component COPET
(by GB/T 14190-2008, detect as solvent with sym-tetrachloroethane 1:1 with phenol) 0.70dl/g, dry
Section moisture content is less than 50ppm., screw rod each district temperature 260～280 DEG C；The spy of island component one (PET-3)
Property viscosity 0.685dl/g, dry section moisture content is less than 50ppm, screw rod each district temperature 270～290 DEG C；Island group
The intrinsic viscosity 0.685dl/g of two (PET-1), dry section moisture content is divided to add less than 50ppm, black agglomerate
6wt%, screw rod each district temperature 270～290 DEG C.
The ratio on Hai Yu island is 30:70, and sea/island spinning body temperature is respectively 270/285 DEG C, cross air blasting wind
Speed 0.4m/s；First hot-rolling speed 2000m/min, temperature 70 C；Second hot-rolling speed 4200m/min,
Temperature 130 DEG C；Prepare the black and white sea-island FDY of 100dtex/24f × 37i.
Embodiment 2
The present embodiment is identical with the setting of embodiment 1 and operation principle, and difference is: black Masterbatch adds 9
The ratio on wt%, Hai Yu island is all 25:75.Sea/island spinning body temperature is respectively 275/290 DEG C, side-blown
Wind wind speed 0.5m/s；First hot-rolling speed 2250m/min, temperature 80 DEG C；Second hot-rolling speed 4350m/min,
Temperature 140 DEG C；Prepare the black and white sea-island FDY of 200dtex/36f × 37i.
Embodiment 3
The present embodiment is identical with the setting of embodiment 1 and operation principle, and difference is: black Masterbatch adds 12
The ratio on wt%, Hai Yu island is 25:75.Sea/island spinning body temperature is respectively 275/290 DEG C, cross air blasting
Wind speed 0.5m/s；First hot-rolling speed 2250m/min, temperature 80 DEG C；Second hot-rolling speed 4350m/min,
Temperature 140 DEG C；Prepare the black and white sea-island FDY of 200dtex/36f × 37i.
Embodiment 4
The present embodiment is identical with the setting of embodiment 1 and operation principle, and difference is: black Masterbatch adds 15
Wt%.The ratio on Hai Yu island is all 20:80.Sea/island spinning body temperature is respectively 280/295 DEG C, cross air blasting
Wind speed 0.6m/s；First hot-rolling speed 2500m/min, temperature 90 DEG C；Second hot-rolling speed 4500m/min,
Temperature 150 DEG C；Prepare the black and white sea-island FDY of 300dtex/48f × 37i.
Fracture strength and elongation at break to the FDY prepared by above-described embodiment are tested, testing standard
For: " GB/T 14344-2008 chemical fiber filament Erichsen test method ", concrete outcome sees table 1
Shown in.
The main preparation technology of table 1 and fibrous physics index
In conjunction with above-described embodiment and table 1 comparing result, the application using alkali soluble copolymer polyester (COPET) as
Common sea component, normal polyester (PET) melt is one of them island component, in normal polyester (PET)
The melt being added with Masterbatch is another island component, uses three components of composite spinning equipment and particular design to spin
Silk assembly, sprays double-colored island compounding flux from same spinneret, cooled, oil, drawing-off, thermal finalization,
Winding, prepares double-colored island polyester fiber, the especially operation with embodiment 3 and embodiment 4 the most typical.
The fabric being made into this fiber, after Alkali reduction, is not required to carry out the dyeing of rear road again, i.e. can get double-colored sea
Island ultrafine fiber fabric.One pack system need to be prepared respectively with general double-colored island superfine fiber or monochromatic island is fine
Dimension, the two step method using network to pool capital the most again is different, and the technological process of production shortens, product quality improves, one-tenth
This reduction；Eliminate poststaining operation simultaneously, be a kind of more environmentally-friendly, energy-conservation mode of production.
Claims (8)
1. the processing technique with plate double-colored superfine composite polyester fiber, it is characterised in that: using alkali soluble copolymer polyester as common sea component, non-pigmented polyester melt is island component one, and the polyester fondant being added with Masterbatch is island component two；Sea component and island component one, island component two melt respectively through screw extruding, carry, measure, enter multicomponent composite spining module, double-colored island compounding flux is sprayed respectively from the left and right sides of same spinneret, cooled, oil, drawing-off, thermal finalization, winding, prepare double-colored island polyester fiber.
A kind of processing technique of same plate double-colored superfine composite polyester fiber, it is characterised in that: described Masterbatch be white carbon black active ingredient be 25 %, carbon black dispersion phase particle diameter is less than 300
The master batch of nm.
A kind of processing technique of same plate double-colored superfine composite polyester fiber, it is characterised in that: described Masterbatch moisture content is less than 80 ppm.
A kind of processing technique of same plate double-colored superfine composite polyester fiber, it is characterized in that: the intrinsic viscosity central value of described sea component alkali soluble copolymer polyester is 0.70 dl/g, dry section moisture content is less than 50 ppm, during screw extruding is melted, its screw rod each district temperature 260～280 DEG C.
A kind of processing technique of same plate double-colored superfine composite polyester fiber, it is characterised in that: the intrinsic viscosity central value of described island component one PET-3 is 0.685
Dl/g, dry section moisture content is less than 50
Ppm, island is combined ratio 20～30:80～70, during screw extruding is melted, screw rod each district temperature 270～290 DEG C.
A kind of processing technique of same plate double-colored superfine composite polyester fiber, it is characterised in that: the intrinsic viscosity central value of described island component two PET-1 is 0.685
Dl/g, dry section moisture content is less than 50
ppm。
A kind of processing technique of same plate double-colored superfine composite polyester fiber, it is characterised in that: in described spinning process, Masterbatch adds 6～15 wt%, and island is combined ratio 20～30:80～70, screw rod each district temperature 270～290 DEG C；Spinning body temperature 270 ~ 295 DEG C, cross air blasting wind speed 0.4 ~ 0.6 m/s；First hot-rolling speed 2000 ~ 2500 m/min, temperature 70-90 DEG C；Second hot-rolling speed 4200 ~ 4500
M/min, temperature 130-150 DEG C；Oil applying rate 0.8～1.0 %.
8. the processing technique of a kind of same plate double-colored superfine composite polyester fiber as described in any one of claim 1-7, it is characterized in that: in described double-colored island polyester fiber, the fiber number of each color fiber and hole count scope are 50～150 dtex/12～24f × 37i, and total specification is 100～290 dtex/24～48f × 37i.
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106381535A (en) * | 2016-11-14 | 2017-02-08 | 浙江古纤道股份有限公司 | Processing technology of veneer differential shrinkage PA (polyamide) |
| CN106400132A (en) * | 2016-11-14 | 2017-02-15 | 浙江理工大学 | Processing technology of veneer two-tone polypropylene filament yarn |
| CN106435783A (en) * | 2016-11-14 | 2017-02-22 | 浙江古纤道股份有限公司 | Process for processing self-crimping nylon fibers |
| CN109943909A (en) * | 2019-02-27 | 2019-06-28 | 广东省化学纤维研究所 | A kind of PE/PET figured islands-in-sea fiber and preparation method thereof |
| CN112593303A (en) * | 2020-11-18 | 2021-04-02 | 江苏盛恒化纤有限公司 | Processing technology of white pure sea island interlaced yarn |
| CN114103188A (en) * | 2021-10-18 | 2022-03-01 | 浙江古纤道股份有限公司 | Preparation method of multifunctional flat yarn |
| CN115142173A (en) * | 2022-06-01 | 2022-10-04 | 南通帝人有限公司 | A sea-island fiber elastic fabric |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106381535A (en) * | 2016-11-14 | 2017-02-08 | 浙江古纤道股份有限公司 | Processing technology of veneer differential shrinkage PA (polyamide) |
| CN106400132A (en) * | 2016-11-14 | 2017-02-15 | 浙江理工大学 | Processing technology of veneer two-tone polypropylene filament yarn |
| CN106435783A (en) * | 2016-11-14 | 2017-02-22 | 浙江古纤道股份有限公司 | Process for processing self-crimping nylon fibers |
| CN109943909A (en) * | 2019-02-27 | 2019-06-28 | 广东省化学纤维研究所 | A kind of PE/PET figured islands-in-sea fiber and preparation method thereof |
| CN112593303A (en) * | 2020-11-18 | 2021-04-02 | 江苏盛恒化纤有限公司 | Processing technology of white pure sea island interlaced yarn |
| CN114103188A (en) * | 2021-10-18 | 2022-03-01 | 浙江古纤道股份有限公司 | Preparation method of multifunctional flat yarn |
| CN114103188B (en) * | 2021-10-18 | 2023-12-01 | 浙江古纤道股份有限公司 | Preparation method of multifunctional flat yarn |
| CN115142173A (en) * | 2022-06-01 | 2022-10-04 | 南通帝人有限公司 | A sea-island fiber elastic fabric |
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Application publication date: 20160810 |