CN102181191A - Alloy antiseptic composite coating for coal mine underground gas pipe - Google Patents
Alloy antiseptic composite coating for coal mine underground gas pipe Download PDFInfo
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- CN102181191A CN102181191A CN 201110086784 CN201110086784A CN102181191A CN 102181191 A CN102181191 A CN 102181191A CN 201110086784 CN201110086784 CN 201110086784 CN 201110086784 A CN201110086784 A CN 201110086784A CN 102181191 A CN102181191 A CN 102181191A
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Abstract
The invention discloses an alloy antiseptic composite coating for a coal mine underground gas pipe. The coating is formed by compounding an aluminum, zinc and chromium coating which is formed by sintering a coating sprayed onto a pipe wall at the temperature of between 300 and 350 DEG C, and a flame retardant antistatic antiseptic coating II which is formed by sintering a coating which is sprayed onto the coating II at the temperature of between 160 and 180 DEG C. The hardness of the alloy antiseptic composite coating is more than or equal to 2H; the impact intensity is more than or equal to 50kg.cm; the coating adhesion is more than or equal to a level 3; neutral salt spray resistance is more than 500h; the indexes of the flam resistance are that: the arithmetic mean value of the flame combustion time of six test pieces is less than or equal to 3s, the arithmetic mean value of the flame combustion time of one test piece is less than or equal to 8s; and the arithmetic mean value of the spark combustion time of six test pieces is 0s and the unit value of the spark combustion time of one test piece is 0s; and the index of conductivity performance is that: surface resistance is less than or equal to 1*10<6>Omega.
Description
One, technical field
The present invention relates to a kind of pipeline anti-corrosive paint, exactly is a kind of coal mine gas pipe alloy anticorrosive composite coating.
Two, background technology
Methane gas is one of principal element of harm coal mine production safety, and the extraction of methane gas is most important in the Coal Production.At present, the gas drainage pipe in the colliery divides nonmetal pipeline and steel pipe.Nonmetal pipeline mainly comprises Glass Steel Tube, polyvinyl chloride (PVC) pipe, polyethylene (PE) pipe.There are shortcomings such as fragility is big, shock resistance difference in Glass Steel Tube, and the pressure-bearing of polyvinyl chloride (PVC) pipe, polyethylene (PE) pipe is not strong, and ageing-resistant performance is relatively poor.Therefore, the gas drainage pipe in the colliery is a steel pipe mostly at present, but there was dampness in the air under the coal mine, there are inflammable easily sudden and violent dust and gas, various corrosive gases and liquid, steel pipe is perishable, need carry out rotproofing to steel conduit, to improve its work-ing life and safety.
In steel tube surface plastic-coated or coating is a kind of effective way of colliery with steel pipe corrosion-proof, has overcome the defective of easily the getting rusty of steel pipe itself existence, burn into high pollution.Patent CN201028165 discloses a kind of underground mine use polymer steel-plastic composite pressure pipe, is provided with the corrosion protection coating that high-molecular polythene or epoxy are made at stainless steel tube or weldless steel tube tube wall.Patent CN200993270 discloses the steel-plastics composite pipe of a kind of mine, oil field use, is coated with the polypropylene corrosion-resistant coating at metal body inner-wall surface.CN201014071 discloses a kind of underground mine use polyethylene coating composite steel tube, is compounded with the anti-electrostatic flame-retardant polyvinyl coating in the inner and outer circumferential surfaces of steel pipe.CN201225492 discloses a kind of mining steel pipe that has aliphatics polyureas coating, utilizes aliphatics polyureas coating that the steel pipe inside and outside wall is covered.These bibliographical informations colliery steel pipe corrosion-proof technology, but the high molecule plastic shock-resistance of steel-plastics composite pipe is not high, come off easily after being impacted in the transportation installation work, and the corrosion resistance nature of single corrosion protection coatings such as epoxy, aliphatics polyureas often can not satisfy the requirement for anticorrosion of gas drainage pipe.
Three, summary of the invention
The present invention aims to provide a kind of long-life coal mine gas pipe, and technical problem to be solved is that the inside and outside wall at gas pipe imposes compound coating, and this coating had both had strong adhesion, shock resistance, had antistatic, fire-retardant and non-corrosibility again.
Thinking of the present invention is to be superposeed regularly by ultra-fine squamous zinc powder and aluminium powder in steel tube surface to form, with the mineral compound is binding agent, stick to the metallic surface, behind sintering, form splendid aluminium zinc chrome (alloy) coating of one deck protection against corrosion impact resistance, antistatic at its surface-coated one deck then, fire retardant, anticorrosive coating form the alloy anticorrosive composite coating.
Gas pipe alloy anticorrosive composite coating of the present invention is composited by aluminium zinc-chromium coating I and flame-retardant and anti-static corrosion protection coating II.The coating of coating I by A, B component by 1: the 1.0-2.0 mass ratio mixes, and disperses, is sprayed on that sintering forms coating I on the tube wall through physics.
The A component comprises each component of following weight part:
The B component comprises each component of following weight part:
Chromic anhydride (CrO
3) 1-10 part
Deionized water 70-90 part;
The coating of coating II comprises each component of following weight part, disperses, is sprayed on coating I through physics and upward form coating II through sintering:
Described aluminium flake, zinc metal sheet are flakey, are of a size of 0.1-0.2 * 10 * 15um.
Described dispersion agent is selected from one or more mixed dispersants in dodecyl Soxylat A 25-7, polyoxyethylene octyl phenol ether, polyalkylene glycol alkyl phenol polyethenoxy ether or the ethylene glycol.
Described thickening material is selected from carboxymethyl cellulose or sodium polyacrylate.
Described Resins, epoxy is selected from brominated epoxy resin or phosphorous epoxy resin.
Described antistatic black pigment is selected from graphite, graphitized carbon black or Fe
3O
4In one or more hybrid pigments.
Described fire retardant is selected from one or more mixed fire retardants in antimonous oxide, triphenylphosphate, eight bromo ether or the hexabromocyclododecane.
Described solidifying agent is selected from one or more mixed curing agents in tung oil acid anhydride, polyamide resin or the linear H phenolic aldehyde.
Described solvent is selected from benzene,toluene,xylene, Virahol, ethanol, propyl carbinol, industrial naptha, acetone, the kerosene mixed solvent more than three kinds or three kinds.
The preparation method of this coal mine gas pipe alloy anticorrosive composite coating be at first with the paint spay-coating of coating I on the pipe inside and outside wall after the derusting by sandblast, dry back forms coating I in 300-350 ℃ of sintering 30-60min, then with the paint spay-coating of coating II on coating I, dry back forms coating II in 160-180 ℃ of sintering 30-60min.
The coal mine gas pipe alloy anticorrosive composite coating of the present invention's preparation, high comprehensive performance, cost performance height.Advantage of the present invention is mainly reflected in:
1, erosion resistance is extremely strong
Carry out the alloy fire retardant, anticorrosive simultaneously at the steel pipe surfaces externally and internally, integrate physical isolation and electrochemical anti-corrosive technology.This compound coating sticking power 〉=3 grade, hardness 〉=2H, shock strength 〉=50kgcm.The pipeline erosion resistance is extremely strong, but acid-alkali-corrosive-resisting, and anti-middle salt fog>500h is specially adapted to colliery delivered downhole high-sulfur, calcic, the isoionic water of magnesium and corrosive gases.
2, flame retardant properties excellence
Aluminium zinc-chromium coating I and flame-retardant and anti-static corrosion protection coating II are composited, its flame retardant properties index excellence (flame time: the arithmetical av≤3s of 6 test specimens, 1 test specimen monodrome≤8s; Mars combustion time: the arithmetical av 0s of 6 test specimens, 1 test specimen monodrome 0s), be applicable to places such as the down-hole is inflammable, explosive.
3, antistatic property is outstanding
Coating contains a large amount of metals and metal oxide, and the pigment of selecting for use is conducting pigment, and antistatic property is outstanding, pipeline surfaces externally and internally resistance≤1 * 10
6Ω.
4, borehole operation, easy construction
Tubing is easy to connect reliable, can adopt modes such as flange, welding to connect as required.
Four, embodiment
Non-limiting examples is described below:
Embodiment 1
100g aluminium flake, 5g zinc metal sheet, 10g polyoxyethylene octyl phenol ether, 1g carboxymethyl cellulose mix and obtain mashed prod A; The 5g chromic anhydride dissolves in the 80g deionized water and obtains solution B.After A, B component were mixed by 1: 1.5 mass ratio, dispersed with stirring was even, is sprayed at the parent tube surface, 300 ℃ of sintering 45min, and the parent tube surface forms aluminium zinc-chromium coating I.
100g brominated epoxy resin, 40g graphitized carbon black, 3g triphenylphosphate, 80g low molecule pa resin, 150g toluene, 150g Virahol, 150g kerosene dispersed with stirring are even, be sprayed at aluminium zinc-chromium coating I surface, 170 ℃ of sintering 45min behind the surface drying, form flame-retardant and anti-static corrosion protection coating II on aluminium zinc-chromium coating I surface, obtain coal mine gas pipe alloy anticorrosive composite coating.
Embodiment 2
100g aluminium flake, 10g zinc metal sheet, 20g polyalkylene glycol alkyl phenol polyethenoxy ether, 2g carboxymethyl cellulose mix and obtain mashed prod A; The 5g chromic anhydride dissolves in the 70g deionized water and obtains solution B.After A, B component were mixed by 1: 1.5 mass ratio, dispersed with stirring was even, is sprayed at the parent tube surface, 350 ℃ of sintering 30min, and the parent tube surface forms aluminium zinc-chromium coating I.
100g brominated epoxy resin, 40g graphite, 3g antimonous oxide, 100g low molecule pa resin, 100g benzene, 150g Virahol, 200g kerosene dispersed with stirring are even, be sprayed at aluminium zinc-chromium coating I surface, 180 ℃ of sintering 30min behind the surface drying, form flame-retardant and anti-static corrosion protection coating II on aluminium zinc-chromium coating I surface, obtain coal mine gas pipe alloy anticorrosive composite coating.
Embodiment 3
100g aluminium flake, 20g zinc metal sheet, 30g dodecyl Soxylat A 25-7,1g sodium polyacrylate mix and obtain mashed prod A; The 10g chromic anhydride dissolves in the 80g deionized water and obtains solution B.After A, B component were mixed by 1: 1.5 mass ratio, dispersed with stirring was even, is sprayed at the parent tube surface, 330 ℃ of sintering 35min, and the parent tube surface forms aluminium zinc-chromium coating I.
100g brominated epoxy resin, 30g Fe
3O
4, 5g antimonous oxide, 60g low molecule pa resin, 20g tung oil acid anhydride, 100g benzene, 150g Virahol, 200g acetone dispersed with stirring be even, be sprayed at aluminium zinc-chromium coating I surface, 170 ℃ of sintering 40min behind the surface drying, form flame-retardant and anti-static corrosion protection coating II on aluminium zinc-chromium coating I surface, obtain coal mine gas pipe alloy anticorrosive composite coating.
Embodiment 4
100g aluminium flake, 25g zinc metal sheet, 20g ethylene glycol, 10g dodecyl Soxylat A 25-7,5g carboxymethyl cellulose mix and obtain mashed prod A; The 8g chromic anhydride dissolves in the 70g deionized water and obtains solution B.After A, B component were mixed by 1: 1.5 mass ratio, dispersed with stirring was even, is sprayed at the parent tube surface, 320 ℃ of sintering 40min, and the parent tube surface forms aluminium zinc-chromium coating I.
The linear H phenolic aldehyde of 100g brominated epoxy resin, 30g graphite, 3g hexabromocyclododecane, 70g low molecule pa resin, 10g, 150g dimethylbenzene, 150g Virahol, 200g acetone dispersed with stirring are even, be sprayed at aluminium zinc-chromium coating I surface, 180 ℃ of sintering 30min behind the surface drying, form flame-retardant and anti-static corrosion protection coating II on aluminium zinc-chromium coating I surface, obtain coal mine gas pipe alloy anticorrosive composite coating.
Embodiment 5
100g aluminium flake, 20g zinc metal sheet, 20g dodecyl Soxylat A 25-7,3g carboxymethyl cellulose mix and obtain mashed prod A; The 6g chromic anhydride dissolves in the 80g deionized water and obtains solution B.After A, B component were mixed by 1: 1.5 mass ratio, dispersed with stirring was even, is sprayed at the parent tube surface, 300 ℃ of sintering 50min, and the parent tube surface forms aluminium zinc-chromium coating I.
The linear H phenolic aldehyde of 100g phosphorous epoxy resin, 30g graphite, 3g hexabromocyclododecane, 70g low molecule pa resin, 10g, 150g dimethylbenzene, 150g Virahol, 200g acetone dispersed with stirring are even, be sprayed at aluminium zinc-chromium coating I surface, 170 ℃ of sintering 45min behind the surface drying, form flame-retardant and anti-static corrosion protection coating II on aluminium zinc-chromium coating I surface, obtain coal mine gas pipe alloy anticorrosive composite coating.
Embodiment 6
100g aluminium flake, 15g zinc metal sheet, 10g ethylene glycol, 20g polyoxyethylene octyl phenol ether, 2g sodium polyacrylate mix and obtain mashed prod A; The 10g chromic anhydride dissolves in the 90g deionized water and obtains solution B.After A, B component were mixed by 1: 1.5 mass ratio, dispersed with stirring was even, is sprayed at the parent tube surface, 330 ℃ of sintering 40min, and the parent tube surface forms aluminium zinc-chromium coating I.
100g phosphorous epoxy resin, 10g graphite, 30g Fe
3O
4, 4g antimonous oxide, 90g low molecule pa resin, 100g dimethylbenzene, 150g ethanol, 200g acetone dispersed with stirring be even, be sprayed at aluminium zinc-chromium coating I surface, 175 ℃ of sintering 35min behind the surface drying, form flame-retardant and anti-static corrosion protection coating II on aluminium zinc-chromium coating I surface, obtain coal mine gas pipe alloy anticorrosive composite coating.
Embodiment 7
100g aluminium flake, 10g zinc metal sheet, 20g dodecyl Soxylat A 25-7,3g sodium polyacrylate mix and obtain mashed prod A; The 5g chromic anhydride dissolves in the 80g deionized water and obtains solution B.After A, B component were mixed by 1: 1.5 mass ratio, dispersed with stirring was even, is sprayed at the parent tube surface, 320 ℃ of sintering 50min, and the parent tube surface forms aluminium zinc-chromium coating I.
100g phosphorous epoxy resin, 40g conductive carbon black, 3g eight bromo ether, 1g antimonous oxide, 80g low molecule pa resin, 10g tung oil acid anhydride, 150g benzene, 150g Virahol, 200g industrial naptha dispersed with stirring are even, be sprayed at aluminium zinc-chromium coating I surface, 180 ℃ of sintering 35min behind the surface drying, form flame-retardant and anti-static corrosion protection coating II on aluminium zinc-chromium coating I surface, obtain coal mine gas pipe alloy anticorrosive composite coating.
Embodiment 8
100g aluminium flake, 5g zinc metal sheet, 15g ethylene glycol, 10g polyalkylene glycol alkyl phenol polyethenoxy ether, 2g carboxymethyl cellulose mix and obtain mashed prod A; The 3g chromic anhydride dissolves in the 70g deionized water and obtains solution B.After A, B component were mixed by 1: 1.5 mass ratio, dispersed with stirring was even, is sprayed at the parent tube surface, 350 ℃ of sintering 40min, and the parent tube surface forms aluminium zinc-chromium coating I.
100g brominated epoxy resin, 15g graphite, 25g Fe
3O
4, 1g hexabromocyclododecane, 2g antimonous oxide, 100g low molecule pa resin, 150g toluene, 150g Virahol, 150g kerosene dispersed with stirring be even, be sprayed at aluminium zinc-chromium coating I surface, 180 ℃ of sintering 40min behind the surface drying, form flame-retardant and anti-static corrosion protection coating II on aluminium zinc-chromium coating I surface, obtain coal mine gas pipe alloy anticorrosive composite coating.
Claims (9)
1. coal mine gas pipe alloy anticorrosive composite coating is characterized in that: described compound coating is by being sprayed on coating on the tube wall through aluminium zinc-chromium coating I that sintering forms be sprayed on the compound coating that flame-retardant and anti-static corrosion protection coating II that the coating on the coating I forms through sintering constitutes; The coating of coating I be by following A, B component by 1: the 1.0-2.0 mass ratio mixes:
The A component comprises each component of following weight part:
The B component comprises each component of following weight part:
Chromic anhydride 1-10 part
Deionized water 70-90 part;
The coating of coating II comprises each component of following weight part:
2. coating according to claim 1 is characterized in that: described aluminium flake, zinc metal sheet are flakey, are of a size of 0.1-0.2 * 10 * 15um.
3. coating according to claim 1 is characterized in that: described dispersion agent is selected from one or more mixed dispersants in dodecyl Soxylat A 25-7, polyoxyethylene octyl phenol ether, polyalkylene glycol alkyl phenol polyethenoxy ether or the ethylene glycol.
4. coating according to claim 1 is characterized in that: described thickening material is selected from carboxymethyl cellulose or sodium polyacrylate.
5. coating according to claim 1 is characterized in that: described Resins, epoxy is selected from brominated epoxy resin or phosphorous epoxy resin.
6. coating according to claim 1 is characterized in that: described antistatic black pigment is selected from graphite, graphitized carbon black or Fe
3O
4In one or more hybrid pigments.
7. coating according to claim 1 is characterized in that: described fire retardant is selected from one or more mixed fire retardants in antimonous oxide, triphenylphosphate, eight bromo ether or the hexabromocyclododecane.
8. coating according to claim 1 is characterized in that: described solidifying agent is selected from one or more mixed curing agents in tung oil acid anhydride, polyamide resin or the linear H phenolic aldehyde.
9. coating according to claim 1 is characterized in that: described solvent is selected from benzene,toluene,xylene, Virahol, ethanol, propyl carbinol, acetone, industrial naptha, the kerosene mixed solvent more than three kinds or three kinds.
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CN102555344A (en) * | 2011-12-30 | 2012-07-11 | 东风汽车股份有限公司 | Mining light metal mechanical explosion-proof coating and spraying process thereof |
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CN102555344A (en) * | 2011-12-30 | 2012-07-11 | 东风汽车股份有限公司 | Mining light metal mechanical explosion-proof coating and spraying process thereof |
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