CN102153207A - No-pollution anti-disease water purifying agent for aquiculture and preparation method thereof - Google Patents

No-pollution anti-disease water purifying agent for aquiculture and preparation method thereof Download PDF

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Publication number
CN102153207A
CN102153207A CN 201010602618 CN201010602618A CN102153207A CN 102153207 A CN102153207 A CN 102153207A CN 201010602618 CN201010602618 CN 201010602618 CN 201010602618 A CN201010602618 A CN 201010602618A CN 102153207 A CN102153207 A CN 102153207A
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China
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group
diatomite
aquiculture
titanium dioxide
water purifying
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CN 201010602618
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Chinese (zh)
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谢钦铭
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Jimei University
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Jimei University
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Priority to CN 201010602618 priority Critical patent/CN102153207A/en
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  • Farming Of Fish And Shellfish (AREA)
  • Purification Treatments By Anaerobic Or Anaerobic And Aerobic Bacteria Or Animals (AREA)

Abstract

The invention discloses a no-pollution anti-disease water purifying agent for aquiculture and a preparation method thereof. The water purifying agent comprises the following components in percentage by weight: 7-18% of Bacillus subtilis group, 3-10% nitrobacteria group, 2-10% of actinomycete group, 50-80% of diatomite and 8-12% of titanium dioxide. By adding multiple components in scientific and reasonable proportions to the micro-ecological regulator comprising nano materials, the compound water purifying agent has the advantages of favorable stress resistance, obvious effects of purification and degradation, easy formation of stable groups, long acting time and complementary functions, and has certain functions of disease prevention and the like. The production method disclosed by the invention is simple and convenient, and the components can be easily preserved under normal temperature and pressure.

Description

Nuisanceless diseases prevention water purification agent of used for aquiculture and preparation method thereof
Technical field
The present invention relates to a kind of water purification agent, particularly relate to nuisanceless diseases prevention water purification agent of a kind of used for aquiculture and preparation method thereof.It is a kind of with nano material-and protective material carrier diatomite and nano titanium oxide be main carrier, added the complex aquatic of multiple beneficial microbiobacterial agent and cultured probiotics and compound method thereof.
Background technology
Existing microbial water-purifying agent, contained composition is comparatively single, and beneficial microorganism do not have stable survival and development place and buffering space, so the ecological regulation and control effect is difficult to bring into play, causes the cultivation water regulating effect not ideal.And existing chemical water purification agent, contained composition mostly is synthetics, mostly to the toxic effect of biology, especially bigger to the beneficial microorganism damaging action, can destroy existing, stable microecological balance in the water body, to culturing aquatic animal bad toxic action be arranged simultaneously, reduce the immunizing power of aquatic animal, and the chemical substance that has also has certain biological accumulation toxic action to human body, so can not be applicable to nuisanceless aquaculture.
Summary of the invention
The object of the present invention is to provide toxic substance and objectionable impurities in a kind of efficient degradation water body, and can improve the nuisanceless diseases prevention water purification agent of the used for aquiculture of aquatic animal immunizing power effectively.
Another object of the present invention is to provide a kind of preparation method who processes the nuisanceless diseases prevention water purification agent of simple, suitable used for aquiculture.
For achieving the above object, technical solution of the present invention is:
The present invention is a kind of nuisanceless diseases prevention water purification agent of used for aquiculture, and its components in weight percentage content is: bacillus group 7%-18%, nitrifying bacteria community 3%-10%, actinomycete group 2-10%, diatomite 50%-80%, titanium dioxide 8%-12%.
The present invention is a kind of preparation method of nuisanceless diseases prevention water purification agent of used for aquiculture, and it may further comprise the steps:
(1) gets diatomite, titanium dioxide, bacillus subtilis bacteria powder, nitrobacteria pulvis, actinomycete group pulvis, by bacillus group 7%-18%, nitrifying bacteria community 3%-10%, actinomycete group 2-10%, diatomite 50%-80%, the ratio of titanium dioxide 8%-12% obtains powdered mixture with above-mentioned powder mixes, and this powdered mixture is little yellow powder-type;
(2) use the low-temperature vacuum drying method with the powdered mixture drying;
(3) get powdered mixture and pack in the container pack into according to quantity packing bag and vacuum sealed package into.
After adopting such scheme, owing to the invention provides a kind of nano material that contains---the complex microorganism water purification agent and the compound method thereof of diatomite and titanium dioxide, described nano material complex microorganism water purification agent, form by natural diatomite, nano titanium oxide, subtilis, nitrobacteria and actinomycetes, can Secure Application in nuisanceless aquaculture; And produce the objectionable impurities-too much ammonia salt of self-pollution in the energy efficient degradation water body by aquaculture, too much nitrite and too much phosphoric acid salt; Simultaneously can improve the immunizing power of aquatic animal more significantly.
The present invention is further illustrated below in conjunction with specific embodiment.
Embodiment
One, prescription:
The present invention is a kind of nuisanceless diseases prevention water purification agent of used for aquiculture, and its components in weight percentage content is: bacillus group 7%-18%, nitrifying bacteria community 3%-10%, actinomycete group 2-10%, diatomite 50%-80%, titanium dioxide 8%-12%.
Example one: the percentile component concentration of Nano type aquatic products probiotics is: the bacillus group is 8.5%, and nitrifying bacteria community is 4.5%, actinomycete group 6%, diatomite 72%, titanium dioxide 9%.
Example two: the percentile component concentration of Nano type aquatic products probiotics is: the bacillus group is 10%, and nitrifying bacteria community is 5%, actinomycete group 5%, diatomite 71%, titanium dioxide 9%.
Example three: the percentile component concentration of Nano type aquatic products probiotics is: the bacillus group is 12%, and nitrifying bacteria community is 7%, actinomycete group 6%, diatomite 65%, titanium dioxide 10%.
Example four: the percentile component concentration of Nano type aquatic products probiotics is: the bacillus group is 7%, and nitrifying bacteria community is 3%, actinomycete group 2%, diatomite 80%, titanium dioxide 8%.
Example five: the percentile component concentration of Nano type aquatic products probiotics is: bacillus group 18%, nitrifying bacteria community 10%, actinomycete group 10%, diatomite 50%, titanium dioxide 12%.
Most preferred embodiment: the percentile component concentration of Nano type aquatic products probiotics is: the bacillus group is 16%(14%-18%), nitrifying bacteria community is 9%(8%-10%), actinomycete group 8%(6%-10%), diatomite 58.5%(50%-67%), titanium dioxide 8.5%(8%-9%).
Two, preparation method:
The present invention also provides a kind of preparation method of nuisanceless diseases prevention water purification agent of used for aquiculture, and it may further comprise the steps:
(1) gets diatomite, titanium dioxide, bacillus subtilis bacteria powder, nitrobacteria pulvis, actinomycete group pulvis, by bacillus group 7%-18%, nitrifying bacteria community 3%-10%, actinomycete group 2-10%, diatomite 50%-80%, the ratio of titanium dioxide 8%-12% promptly obtains powder mixture with above-mentioned powder composition after mixing under normal temperature (10-30 ℃), normal pressure and low humidity (55-70%) condition is composite, this powdered mixture is little yellow powder-type;
(2) powdered mixture after composite is carried out the dehumidifier drying under low temperature (4-12 ℃) condition, the moisture that makes mixture is less than 12%, in the prepackage can container of packing into then;
(3) get dried powdered mixture and pack in the container, pack into according to quantity packing bag and vacuum sealed package, and labelled and indicate the date manufactured.
Three, test contrast
The present invention and prior art contrast have following advantage:
1, product of the present invention has no side effect to aquatic animal, can be applied in the nuisanceless aquaculture, can improve the quality of fishery products greatly.
2, the beneficial microbe colony in the product of the present invention is garbled efficient bacterial strain, and purifying water effect is obvious.
3, product application nano material of the present invention effectively solves the problem that beneficial microorganism lacks carrier, and maintain the leading position in market water purification working lipe (be about existing products in markets four times) at home.
4, product of the present invention has solved in the current aquaculture and has poisoned and incidental aquatic animal disease problem owing to the water body self-pollution causes the poisoning of aquatic animal ammonia nitrogen, nitrite nitrogen.
5, because adopted protective material carrier-diatomite and titanium dioxide; so both can be used as the water purification agent of heavy metal contamination; degrading nitrite, ammonia salt and phosphatic effect are arranged again, and simultaneously useful mushroom such as Bacillus subtillis can play the effect of aquatic animal diseases prevention.
The good and bad analytical table of the dissimilar water purification agents of table 1
The chemistry water purification agent Microbial water-purifying agent of the present invention
Product property Organic-inorganic compounds such as copper sulfate, chlorinated lime, malachite green Great majority are aqua or pulvis
The good and bad analysis Although this method cost is lower, the short period of time can play effect, can destroys the little ecologic structure of water body, and aquaculture organism is also had the murder by poisoning effect. Aqua of the type or pulvis microbial water-purifying agent easily disperse after entering water body, and it is bigger to be affected by the external environment, and purifying water effect can not be stablized lastingly.
The technical indicator contrast table of existing water purification agent product of table 2 and product of the present invention
? Ammonia nitrogen decrement (%) Nitrite nitrogen decrement (%) Total phosphorus decrement (%) Vibrios is counted decrement (%) Surviving rate (%)
Control group (CK) 0.00 0.00 0.00 0.00 59.51
The water purification treasured 32.89 11.14 0.00 16.67 61.28
Green little health 32.78 15.25 0.00 48.33 65.57
The water doctor 22.39 21.07 0.00 66.67 68.53
The complex ecological treasured 35.48 25.42 1.25 50.00 63.08
Microbial water-purifying agent of the present invention 62.03 51.82 25.86 73.50 73.45
The timeliness and the expense contrast table of the existing clean agent product of table 3 and the patented product
The probiotics product Character Water purification working lipe Single mu of monthly consumption (not containing manpower)
Green precious water purification agent difficult to understand Liquid 10-15 days 135 yuan
The Verbatim biologic water cleaner Pulvis 7-10 days 100 yuan
Product of the present invention Pulvis About February 130 yuan
Emphasis of the present invention just is:
Product of the present invention has enlarged the decomposer---artificially inoculate the screening of beneficial microbe colony: select high-quality composite microbial preparation for use.
Product screening of the present invention suitable microorganic adhesion matrix, enlarge the living space of decomposer-microorganism from face.Require: growth is fast, and denitrogenation, dephosphorizing capacity are strong, and poor environment has a stronger surge capability to external world, is adapted to fresh water and briny environment.
Product of the present invention is guaranteed the eubiosis of cultivating system by the reparation of being protected property of beneficial microbe colony.Can accomplish few usefulness, without microbiotic; Change water less, do not change water.
Product technology of the present invention is based on eubiosis principle; adopt the novel process of " " diatomite-matrix "+" titanium dioxide-matrix "+beneficial microbe colony "; remedy traditional probiotics and only paid attention to microorganism species quantity, and the defective of the living environment protection of ignorance microorganism.
Product of the present invention enlarges kind and the quantity of strengthening the decomposer, thereby breaks " bottleneck " of the ecosystem, and mediation material cycle approach makes pollutent be degraded timely and transform, to keep ecological balance.
1. use widely, seawater, fresh water, degree of saltiness water can use.Organism in can degradation water, again can precipitation at the bottom of organism.
2. it is strong to fall the ammonia ability, and the nitrite nitrogen lowering speed is fast.The per day clearance of total ammonia attitude reaches about 70%, and the maximum material removal rate of nitrite nitrogen reaches 50.0%.Fall ammonia nitrogen time weak point, only need 3~4 days; The filter bed maturation time is 25 ℃~27 ℃ of 14d(water temperatures).The effect that purifies water is obvious.
3. microorganism species quantity is stable, and can suppress the harmful microorganism growth.In process of the test, generally 3.8 * 10 6~5 * 10 8/ ml.After seedling water is used product of the present invention, after a large amount of breedings of beneficial microorganism, the outer microbiotic of they energy body secretions, these microbiotic can suppress the harmful microbe growth.Therefore, use product filter bed maturation of the present invention after, the amount of vibrio in the water body obviously reduces, thereby reduces the generation of disease.
4. transport, preserve conveniently, use simple.Under the environment below 30 ℃, do not open original packing, its microbic activity and validity can be kept more than 2 years.During use, needn't as the solid bacterium bent cultivate need microorganism and substratum loaded down with trivial details separate formality.
5. not only harmless to culturing object, and can promote growth.
Product of the present invention uses very simple, only need calculate the volume of water, and water per ton restrains products of the present invention (making water be 30/1000000ths concentration, i.e. 30ppm) with 30.After this water purification agent weighed, put into plastic tank, add 20-30 clean water doubly, inflate 24 hours (or regularly stirring 6~8 times),, form milky suspension liquid with the activating microorganisms spore, and then with this suspension liquid full pool spilling head.Add product 500 grams of the present invention, every mu 250 gram after 50 days for every mu after 20 days.
The above, only for preferred embodiment of the present invention, so can not limit scope of the invention process with this, i.e. the equivalence of doing according to the present patent application claim and description changes and modification, all should still belong in the scope that patent of the present invention contains.So carrying out the water purification agent or the probiotics product of assembly, all applying nano materials diatomites and Bacillus subtillis group, nitrifying bacteria community all belong to the scope of protection of the invention.

Claims (2)

1. the nuisanceless diseases prevention water purification agent of a used for aquiculture, it is characterized in that: its components in weight percentage content is: bacillus group 7%-18%, nitrifying bacteria community 3%-10%, actinomycete group 2-10%, diatomite 50%-80%, titanium dioxide 8%-12%.
2. the preparation method of the nuisanceless diseases prevention water purification agent of used for aquiculture according to claim 1, it is characterized in that: it may further comprise the steps:
(1) gets diatomite, titanium dioxide, bacillus subtilis bacteria powder, nitrobacteria pulvis, actinomycete group pulvis, by bacillus group 7%-18%, nitrifying bacteria community 3%-10%, actinomycete group 2-10%, diatomite 50%-80%, the ratio of titanium dioxide 8%-12% obtains powdered mixture with above-mentioned powder mixes, and this powdered mixture is little yellow powder-type;
(2) use the low-temperature vacuum drying method with the powdered mixture drying;
(3) get powdered mixture and pack in the container pack into according to quantity packing bag and vacuum sealed package into.
CN 201010602618 2010-12-23 2010-12-23 No-pollution anti-disease water purifying agent for aquiculture and preparation method thereof Pending CN102153207A (en)

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Application Number Priority Date Filing Date Title
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102897920A (en) * 2012-03-22 2013-01-30 中国环境科学研究院 Application of nano-grade material in low-temperature water body ecological reparation, and low-temperature water body ecological composite nano-grade reparation method
CN109592862A (en) * 2018-10-25 2019-04-09 福建省连江县宏裕水产有限公司 A kind of modifying agent for bottom material of pond for breeding aquatic products

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1528681A (en) * 2003-09-28 2004-09-15 无锡中顺生物技术有限公司 Live bacterial microorganism water modifier equipped with activating culture medium and manufacturing process thereof
CN1807588A (en) * 2005-12-28 2006-07-26 农业部环境保护科研监测所 Composite bacillus subtilis and lactic acid bacteria microbe formulation preparation method
CN101781025A (en) * 2010-02-09 2010-07-21 集美大学 Nano microecological modulator of aquatic product and production method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1528681A (en) * 2003-09-28 2004-09-15 无锡中顺生物技术有限公司 Live bacterial microorganism water modifier equipped with activating culture medium and manufacturing process thereof
CN1807588A (en) * 2005-12-28 2006-07-26 农业部环境保护科研监测所 Composite bacillus subtilis and lactic acid bacteria microbe formulation preparation method
CN101781025A (en) * 2010-02-09 2010-07-21 集美大学 Nano microecological modulator of aquatic product and production method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102897920A (en) * 2012-03-22 2013-01-30 中国环境科学研究院 Application of nano-grade material in low-temperature water body ecological reparation, and low-temperature water body ecological composite nano-grade reparation method
CN102897920B (en) * 2012-03-22 2016-03-30 中国环境科学研究院 The application of nano material in the restoration of the ecosystem of low temperature water body and low temperature water ecology composite Nano restorative procedure
CN109592862A (en) * 2018-10-25 2019-04-09 福建省连江县宏裕水产有限公司 A kind of modifying agent for bottom material of pond for breeding aquatic products

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Application publication date: 20110817