CN102125027A - Method for preparing biological pesticide adjuvant by utilizing waste of coniferous plants - Google Patents
Method for preparing biological pesticide adjuvant by utilizing waste of coniferous plants Download PDFInfo
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- CN102125027A CN102125027A CN2010101064746A CN201010106474A CN102125027A CN 102125027 A CN102125027 A CN 102125027A CN 2010101064746 A CN2010101064746 A CN 2010101064746A CN 201010106474 A CN201010106474 A CN 201010106474A CN 102125027 A CN102125027 A CN 102125027A
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- discarded object
- insecticides adjuvant
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- stake
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Abstract
The invention discloses a preparation method of a plant-derived biological pesticide adjuvant, aiming at providing a green plant-derived pesticide adjuvant which is green, environmental-friendly and safe for most beneficial organisms to substitute for organic solvents, i.e. benzene, methylbenzene, dimethylbenzene, and the like and reduce the pollution of chemical toxic solvents on environment. The preparation method comprises the following steps of: placing wastes of piles, roots and branches of coniferous plants in raw materials into a plurality of heated iron bioreactors according to certain lengths and weight; and heating for 8-12 hours to achieve the temperature of 350+/-30 DEG C so that the wastes of the piles, the roots and the branches are cracked into liquid through root distillation and the liquid passes through outlet pipelines of the bioreactors, is cooled and then flows into a storage can and then is stored for standby application. A preparation method of the invention (2) comprises the following steps of: placing first-time initial extract substances into elliptical bioreactors, heating to 300-500 DEG C and cooling through cooling water from a spiral pipe positioned at a right side, wherein the cracked pesticide adjuvant flows into a storage can and is qualified through detection and stored according to unequal iron drums of 200 kilograms and 100 kilograms for standby application.
Description
The present invention is a method of utilizing the biological insecticides adjuvant of the discarded object of conifer plant preparation.The insecticides adjuvant of this biology is mainly used in the solvent of agricultural chemicals source medicine, replaces the organic solvents such as benzene,toluene,xylene in the missible oil, reduces the use of poisonous and harmful solvent, reduces the pollution of environment.To former medicine favorable solubilities such as Avermectin, ivermectin, beta-cypermethrin, fenpropathrin, Buprofezin, Rynaxypyr (the trade name health is wide), matrines, be better than organic solvents such as benzene,toluene,xylene through test.This solvent green non-pollution, residual near zero, environmentally friendly, be to meet the era development trend.
Purpose of the present invention will provide a kind of green, environmental protection exactly, insecticides adjuvant to the green plants source of most beneficial organism safety, replace the organic solvents such as benzene,toluene,xylene in the missible oil, reduce the use of chemical poisonous and harmful solvent, reduce the pollution of environment.The present invention is the insecticides adjuvant method of the discarded object biology of preparation conifer plant.
The raw material of the insecticides adjuvant of the discarded object biology of preparation conifer plant is stake, the root of conifer plant, the extract of branch, is by certain technology and flow process extraction.
The present invention one production technology is with the discarded object of the stake of the conifer plant in the raw material, root, branch, puts into the bio-reactor made of iron that several are heated by certain length and weight.Make each bio-reactor cylindrical, 1 meter of base diameter, high 2 meters, steel plate by 0.5 centimetre is welded, and in drum the safety provisioning request, the discarded object of the stake of the conifer plant of adding 200-300 kilogram, root, branch, iron covering on the top cover, heated 8-12 hour, temperature reaches to 350 ℃ ± 30 ℃, makes the discarded object of stake, root, branch heat up in a steamer cracking through root, extract that obtains and wooden carbon, from the outlet conduit of each bio-reactor, cooling flows into the storage iron flask to extract through cooling tube, after preserve standby again.The by product charcoal, the cooling pack is used for heating, baked foods, or use in the industrial production.
In order to obtain the insecticides adjuvant of required biology, the first extract body material that the discarded object of original stake, root, branch must be obtained through the bio-reactor reaction, under the technological process of regulation, carry out the cracking second time once again, obtain biological insecticides adjuvant and other by product, these by products can be used for making the softening agent and the biopesticide of rubber tyre.
The present invention two production technology is the stake with the conifer plant in the raw material, root, the liquid substance that the discarded object of branch extracts, put into one and add the oval bio-reactor that steel plate is welded, in put into this kind of 3-5 ton liquid substance, bottom at oval bio-reactor, heat 300 ℃-500 ℃, its top is the charging aperture switch, the limit, left side is the by product gate out switch, and right edge one is managed pipeline twist, passes through water quench, the insecticides adjuvant of the biology of cracking becomes liquid to flow into the storage iron flask, after testing, qualified, by 200 kilograms and the 100 kilograms metal bucket storages that do not wait, labelled, standby.
Utilize the biological insecticides adjuvant of discarded object preparation of conifer plant, this auxiliary agent can replace organic solvents such as benzene,toluene,xylene, to former medicine favorable solubilities such as Avermectin, ivermectin, beta-cypermethrin, fenpropathrin, Buprofezin, Rynaxypyr (the trade name health is wide), matrines, being made into preparation, to be used to prevent and treat defoliator effects such as fruit tree, forest, gardens, vegetables, tealeaves, melon and fruit remarkable, no poisoning.Now lift the difference solvability of three kinds of former medicines and dimethylbenzene and conifer plant extraction liquid, as shown in the table.
The solvability (pressing g/L) of three kinds of former medicines of table 1
| Former medicine title | Avermectin | Ivermectin | Beta-cypermethrin |
| The conifer plant extraction liquid | 471 | 450 | 495 |
| Dimethylbenzene | 300 | 285 | 315 |
Through next fixed 25 ℃ of conditions, the former medicine of Avermectin, the former medicine of ivermectin, the solvability of the former medicine of beta-cypermethrin in xylene solvent are respectively 300g/L, 285g/L and 315g/L; And the solvability in the biological insecticides adjuvant of the discarded object of conifer plant preparation is respectively 471g/L, 450g/L and 495g/L; Solubility property obviously is better than the chemical solvent of dimethylbenzene, and solubilising about 57% on year-on-year basis, and this solvent is environmental protection, meets the tendency of the day.
The cream preparation that three kinds of former medicines of table 2 are made into (forming by weight percentage)
In the practical application, the cream preparation 1000-2000 of three kinds of prescriptions times of liquid control just obtained satisfied control efficiency in second day to the larva of cowpea, Phalera flavescens, mandarin jacket wood sawfly, dendrolimus punctatus, prodenia litura.The lethality of the defoliator of these three kinds fill a prescription control fruit tree, forest, vegetables all reaches more than 95%, and plant is not produced poisoning.The lethality of the control defoliator of interim beta-cypermethrin prescription reaches more than 97%, sky surplus the term of validity reaches 15, residual and the pollution of so effective minimizing agricultural chemicals, improve consumer's edible safety, ensure that effectively the civic is healthy, meets the consumption demand of people to green fruit-vegetable, organic fruits and vegetables.Be fit to the production of mountain area medium-sized and small enterprises.
Claims (2)
1. the discarded object of conifer plant prepares the method for biological insecticides adjuvant, it is characterized in that:
(1) the present invention is the method for the insecticides adjuvant of preparation conifer plant refuse biology.The insecticides adjuvant of this biology is mainly used in the solvent of agricultural chemicals source medicine, replaces the organic solvents such as benzene,toluene,xylene in the missible oil, reduces the use of poisonous and harmful solvent, reduces the pollution of environment.
The present invention one production technology is with the discarded object of the stake of the conifer plant in the raw material, root, branch, puts into the bio-reactor made of iron that several are heated by certain length and weight.Each bio-reactor is made cylindrical, 1 meter of base diameter, high 2 meters, steel plate by 0.5 centimetre is welded, and in drum the safety provisioning request, add the conifer plant of 200-300 kilogram stake, root, discarded object, iron covering on the top cover, heated 8-12 hour, temperature reaches to 350 ℃ ± 30 ℃, makes the discarded object of stake, root, branch heat up in a steamer cracking through root, and the extract that obtains is again from the outlet conduit of each bio-reactor, cooling flows into the storage iron flask through cooling tube, after preserve standby.
In order to obtain the insecticides adjuvant of required biology, the discarded object of original stake, root, branch must be reacted the first extract body material that obtains through bio-reactor, under the technological process of regulation, carry out the cracking second time once again, obtain biological insecticides adjuvant
(2) the present invention two production technology is the stake with the conifer plant in the raw material, root, the liquid substance that the discarded object of branch extracts, put into one again and add the oval bio-reactor that steel plate is welded, in put into this kind of 3-5 ton liquid substance, bottom at oval bio-reactor, heat 300 ℃-500 ℃, its top is the charging aperture switch, the limit, left side is the by product gate out switch, and right edge one is managed pipeline twist, passes through water quench, the insecticides adjuvant of the biology of cracking becomes liquid to flow into the storage iron flask, after testing, qualified, by 200 kilograms and the 100 kilograms metal bucket storages that do not wait, labelled, standby.
2. according to the insecticides adjuvant of the discarded object biology of the described preparation of claims 1 conifer plant, it is characterized in that invention one usefulness the conifer plant in the raw material stake, root, discarded object extracting liq under the regulation technological process and the situation of heating; Invention two obtains biological insecticides adjuvant with the cracking of carrying out heating for the second time of first extract under the preceding topic of extract for the first time just.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010106474.6A CN102125027B (en) | 2010-01-20 | 2010-01-20 | Method for preparing biological pesticide adjuvant by utilizing waste of coniferous plants |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010106474.6A CN102125027B (en) | 2010-01-20 | 2010-01-20 | Method for preparing biological pesticide adjuvant by utilizing waste of coniferous plants |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102125027A true CN102125027A (en) | 2011-07-20 |
| CN102125027B CN102125027B (en) | 2014-01-29 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201010106474.6A Expired - Fee Related CN102125027B (en) | 2010-01-20 | 2010-01-20 | Method for preparing biological pesticide adjuvant by utilizing waste of coniferous plants |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1176740A (en) * | 1997-07-25 | 1998-03-25 | 珠海绿色南方保鲜总公司 | Organic copper agent used as bactericide and acaricide, and method for preparing same |
| WO2006020995A1 (en) * | 2004-08-10 | 2006-02-23 | Arch Wood Protection, Inc. | Penetration improvement of copper amine solutions into dried wood by addition of carbon dioxide |
| CA2485063A1 (en) * | 2004-10-18 | 2006-04-18 | Hydralogic Systems Inc. | Method and apparatus for insect repellant system |
| CN1965647A (en) * | 2006-09-25 | 2007-05-23 | 湖南万家丰科技有限公司 | Pesticide containing biological diesel oil solvent and preparation process thereof |
| CN101606517A (en) * | 2009-07-27 | 2009-12-23 | 深圳诺普信农化股份有限公司 | A kind of farm chemical emulsion preparation |
-
2010
- 2010-01-20 CN CN201010106474.6A patent/CN102125027B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1176740A (en) * | 1997-07-25 | 1998-03-25 | 珠海绿色南方保鲜总公司 | Organic copper agent used as bactericide and acaricide, and method for preparing same |
| WO2006020995A1 (en) * | 2004-08-10 | 2006-02-23 | Arch Wood Protection, Inc. | Penetration improvement of copper amine solutions into dried wood by addition of carbon dioxide |
| CA2485063A1 (en) * | 2004-10-18 | 2006-04-18 | Hydralogic Systems Inc. | Method and apparatus for insect repellant system |
| CN1965647A (en) * | 2006-09-25 | 2007-05-23 | 湖南万家丰科技有限公司 | Pesticide containing biological diesel oil solvent and preparation process thereof |
| CN101606517A (en) * | 2009-07-27 | 2009-12-23 | 深圳诺普信农化股份有限公司 | A kind of farm chemical emulsion preparation |
Non-Patent Citations (1)
| Title |
|---|
| 王磊 等: "植物精油在环保型乳油中的应用展望", 《植物保护》 * |
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| CN102125027B (en) | 2014-01-29 |
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Owner name: LISHUI LVGU BIOLOGICAL PHARMACEUTICAL CO., LTD. Free format text: FORMER OWNER: JIANG TULING Effective date: 20130929 |
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Effective date of registration: 20130929 Address after: 323000 science and Technology Pioneer Park, Tianning Industrial Zone, Lishui, Zhejiang Applicant after: Lishui Lvgu Biological Pharmaceutical Co., Ltd. Address before: 323000 science and Technology Pioneer Park, Tianning Industrial Zone, Lishui, Zhejiang Applicant before: Jiang Tuling |
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