CN102100399A

CN102100399A - Application of mango pulp alcohol extract as sensory humectant for cigarette

Info

Publication number: CN102100399A
Application number: CN 200910273359
Authority: CN
Inventors: 蔡冰; 郭国宁; 岳海波; 李丹; 王承明
Original assignee: China Tobacco Hunan Industrial Co Ltd; Wuhan Huanghelou Science and Technology Park Co Ltd
Current assignee: China Tobacco Hunan Industrial Co Ltd; Wuhan Huanghelou Science and Technology Park Co Ltd
Priority date: 2009-12-22
Filing date: 2009-12-22
Publication date: 2011-06-22

Abstract

The invention discloses application of a mango pulp alcohol extract as sensory humectant for cigarette, belonging to the technical field of cigarette perfume. The application of the mango pulp alcohol extract as sensory humectant for cigarette is characterized by adding the mango pulp alcohol extract to tobacco shreds to be served as the sensory humectant according to the proportion of 0.1-0.7% of the total weight of the tobacco shreds. The mango pulp alcohol extract is extracted sequentially by the following steps of: (1) separating and crushing the mango pulp; (2) mixing the mango pulp and the alcohol at the volume ratio of 1 to (5-30), extracting for 40-150 min at 30-70 DEG C, and then evaporating and separating at 35-60 DEG C to obtain steam condensate that is the mango pulp extract. The application disclosed by the invention has a remarkable effect and plays good sensory and humectant roles in the whole perfume of the smoke, dryness, stimulation, remaining taste and spicy feeling and the like after sensory evaluation. The humectant has low manufacturing cost and is convenient to use.

Description

Mango meat alcohol extract is as the application of cigarette sense organ humectant

Technical field

The invention belongs to the cigarette flavors technical field, be specifically related to the application that a kind of alcohol extract with mango meat is used for cigarette sense organ humectant.

Background technology

Mango (Mangifera indica) is the fruit of Anacardiaceae Mangifera plant, originates in the torrid zone, subtropical zone, and is very high in China's output, resource is very abundant, and have that the distribution region is wide, raw material is easy to get even the four seasons such as can adopt at advantage, therefore, mango is by a large amount of industrialization.Find after deliberation, mainly contain hydrocarbon compound, ester and lactone compound, aldehyde, ketonic compound, monoterpene hydrocarbon compound, organic acid, polyphenols in the ripe mango.Studies show that phenolic acid such as gallic acid, m-digallic acid, alkaloid, Quercetin, isoquercitrin, mangiferin etc. have the bacterium of inhibition and alternaric bacteria, high anti-oxidation is active and remove two kinds of biological functions such as free radical.Mango is lost the appetite to thirsty and dry pharynx, indigestion, and dizzy vomiting, the pharyngalgia hoarsen, coughing with a lot of sputum, illness curative effects such as asthma are excellent.

At present, making full use of of mango meat alcohol extract also do not done further investigation, and mango meat alcohol extract as the application of tobacco humectant, yet there are no report in cigarette.

In flavouring essence for tobacco, tobacco humectant all has bigger change at home and abroad.Polyhydroxy substances such as main employing glycerine, propane diols, sorbic alcohol are humectant in China's cigarette industry at present, but the purpose of using this type of humectant only is to keep the moisture content of pipe tobacco in the process, improve the anti-processability of pipe tobacco, and for the keeping of finished cigarettes moisture content, then effect is not ideal to suck the improvement of comfort level.Prior art developed directly at sensory issues, the humectant that dry sensation, excitant, pleasant impression etc. are improved, as 2007, people China Tobacco Guangxi Industrial Corporation such as field rubine, Huang Tianhui were that raw material obtains natural humectant through rational proportion with cloves, basyleaves and eucalyptus camaldulensis leaf.2007, respectively with solvent extraction and refining, moist-keeping flavouring additive agent was made in allotment to people such as the Jiang Mei of Yunnan Reascend Tobacco Tech.(Group) Co., Ltd. is red, kind army of continuing in proportion then with special tobacco, marine alga, vanilla, and their humectation effect is not ideal.

Summary of the invention

Above-mentioned deficiency at prior art, the technical problem to be solved in the present invention provides the application of a kind of mango meat alcohol extract as cigarette sense organ humectant, use back whole fragrance, dry sensation, excitant, pleasant impression, pungent sense etc. and play good sense organ humectation effect, the integral body of cigarette is sucked comfort level play good synergistic effect flue gas.

Technical scheme of the present invention is: mango meat alcohol extract is as the application of cigarette sense organ humectant, be the mango meat alcohol extract that the meat alcohol extract of mango is obtained, add in the pipe tobacco as the sense organ humectant according to 0.1%～0.7% ratio of pipe tobacco gross weight.

Described mango meat alcohol extract step is in the following order extracted and is obtained:

(1) mango meat is separated fragmentation;

(2) with the ethanol of mango meat particle and percent by volume 30%～80% by volume 1: the ratio of (5～30) is mixed, under 30 ℃～70 ℃ temperature, extract 40～150min, separate with the vacuum rotary evaporator evaporation under 35 ℃～60 ℃ temperature then, the gained steam condensate is mango meat alcohol extract;

Advantage of the present invention: effect of the present invention is remarkable, after sensory evaluation, good sense organ humectation effect is played in the whole fragrance of flue gas, dry sensation, excitant, pleasant impression, pungent sense etc.The cost of manufacture of this humectant is cheap, and is easy to use.

The specific embodiment

Below in conjunction with embodiment the relevant technologies problem is described in further detail.The applicant adopts U.S. Varian company (3800/2200) gaseous mass spectrum combined instrument, mango meat alcohol extract has been carried out macromethod mensuration, big quantity of material wherein plays good sense organ humectation effect to the whole fragrance of flue gas, dry sensation, excitant, pleasant impression, pungent sense etc., the integral body of cigarette is sucked comfort level play good synergistic effect.Particularly polyphenols accounts for 72% of total mango alcohol extract in the mango meat, wherein: chlorogenic acid 5.8%, caffeic acid 2.1%, p-methyl phenol 7.4%, eugenol 3.5%, guaiacol 3.6%, they can give good mouthfeel in sucking process, reduce assorted gas, improve the pleasant impression value, reduce dry sensation.

Ester and lactone compound account for 7.5% of total mango alcohol extract, wherein: methyl butyrate 0.83%, methyl pyruvate 1.28%, ethyl acetate 3.02%, 2 Methylpropionic acid ethyl ester 0.09%, ethyl butyrate 1.74%, butenoic acid ethyl 0.58%, ethyl hexanoate 0.39%, 3-hydroxy ethyl caproate 0.04%, ethyl caprilate 1.94%, ethyl caprate 2.01%, undecanoic acid ethyl ester 0.07%, ethyl laurate 0.03%, ethyl myristate 0.05%, ethyl palmitate 3.41%, butyl acetate 2.41%, butyl butyrate 0.31%, 3-hydroxybutyric acid butyl ester 0.26%, 3-hydroxybutyric acid-2-methyl propyl ester 0.05%, butyl hexanoate 0.02%.These ester type compounds, can in and free alkali, regulate the cigarette smoke Acidity of Aikalinity, reduce pungent, the larynx phenomenon of choking of flue gas, make flue gas become comfortable.

Organic acid accounts for 7.34% of alcohol extract total amount, and wherein: the amount that butyric acid, 2-butyric acid, 3-hydroxybutyric acid and caproic acid account for total organic acids is: 0.82%, 0.07%.0.73％、0.35％。The ester type compound that they form is to reducing flue gas excitant, pungent sense, and improving the pleasant impression value has good effect.

In recording organic acid, there is malic acid to account for 3.21% of total acid content, it has good result to eliminating dry sensation, sad, capric acid, octadecenoic acid account for 0.09%, 0.12%, 0.34% of total acid content respectively, they to reduce flue gas alkalescence, excitant has effect preferably.

Above material role promptly is that cigarette sense organ humectant is answered role, the applicant also repeatedly checks and obtains proof, adopt contained useful activity components in proportions basically identical in the mango meat alcohol extract that extracting method of the present invention extracts, therefore in joining pipe tobacco during as humectant, use extract stoste to get final product, do not need to carry out other adjustment.

In addition, also have following compound in the mango meat alcohol extract, they also have better action to the qualities such as suction flavor of cigarette:

Hydrocarbon compound accounts for 4.1% of total mango alcohol extract, wherein: pentamethylene 0.93%, cyclohexane 0.69%, hexahydrotoluene α-selinene 0.82%, β-selinene 0.59%, germacrene D0.14%.

Aldehyde, ketonic compound account for 4.95% of middle mango alcohol extract, wherein: acetaldehyde 0.11%, butyraldehyde 0.49%, hexanal 0.86%, (E)-2-hexenoic aldehyde 0.25%, (E)-2-nonenyl aldehyde 0.12%, α-terpinenes 1.32%; They have pine tree fragrance increases cigarette flavor.

The monoterpene hydro carbons accounts for 6.39% of total alcohol extract, and wherein: laurene accounts for 0.33% of total monoterpene hydro carbons total amount, and it has fresh green grass odor characteristic, increases in tobacco and can cover assorted gas.(Z)-and 3-hexenol, (E)-2-hexenoic aldehyde, (E)-2-hexenol have fresh, blue or green fragrance, constitutes the fragrant fragrance characteristic of mango head with terpene compound, and increasing in tobacco to increase mouthfeel, improves the pleasant impression value of sucking.

In sum, after these chemical composition comprehensive functions in the mango meat alcohol extract, can play good sense organ humectation effect to the whole fragrance of flue gas, dry sensation, excitant, pleasant impression, pungent sense etc.

The applicant adopts extract to feed in raw material, and the sample cigarette has been carried out smokeing panel test the contrast experiment with middle-grade blank (not reinforced and humectant) pipe tobacco, and interpolation scheme and smoking result see Table 1.

The sense organ humectation smoking result of table 1, different applied amounts

The result shows in the table 1, and mango meat alcohol extract of the present invention is that 0.1% of pipe tobacco gross weight～0.7% o'clock humectation is effective in addition.The percentage here is meant and uses alcohol extract stoste of the present invention.Because repeatedly checking, the applicant obtains proof, adopt contained effective active components in proportions basically identical in the mango meat alcohol extract that extracting method of the present invention extracts, therefore in joining pipe tobacco during as humectant, use extract stoste to get final product, do not need to carry out other adjustment.

The explanation of listed data in the his-and-hers watches:

1, all sense organ scores adopt 9 fens systems.

2, excitant is divided into big, medium, little three class, and corresponding score value is respectively 1-3 branch, 4-6 branch, 7-9 branch, and wherein 2,5,8 are divided into each grade intermediate section.Excitant is strong more, and score is low more, and excitant is weak more, and score is high more.Pleasant impression is judged identical with the excitant index with the dry sensation index.

3, harmony be divided into, in, differ from three class, corresponding score value is respectively 7-9 branch, 4-6 branch, 1-3 branch, wherein 8,5,2 are divided into each grade intermediate section.Harmony is good more, and score is high more, and harmony is low more, and score is low more.

Smoke panel test contrast as can be seen from table 1, and its addition of mango meat alcohol extract is outstanding at 0.3% o'clock fragrance, and mouthfeel is better, effectively flavouring, cover assorted and the minimizing excitant.Mango meat alcohol extract plays good sense organ humectation effect to the whole fragrance of flue gas, dry sensation, excitant, pleasant impression, pungent sense etc., the suitable interpolation scope of this extract is 0.1%～0.7% in addition, the integral body of cigarette is sucked comfort level play good synergistic effect.The application extracts mango meat alcohol extract from mango meat, be applied in the cigarette, after sensory evaluation, good sense organ humectation effect is played in the whole fragrance of flue gas, dry sensation, excitant, pleasant impression, pungent sense etc., the integral body of cigarette is sucked comfort level play good synergistic effect.The present invention has developed a kind of new effective use of mango, for the cigarette humectant has been developed a brand-new kind.In China, mango is that a kind of output is very high, the profuse fruit of resource, and its cost of manufacture is cheap, and humectant of the present invention has a extensive future.The result also as can be seen from table, when using with humectant as tobacco, its addition not and be The more the better, the mechanism of action of mango meat alcohol extract is very complicated, prior art still fails all to decode, and the applicant infers that they should be the synergistic results of a system.Though the applicant has made a large amount of research and exploration, still its mechanism of action can not be told about relatively more thoroughly, this also with contain complicated and various compound in the tobacco, some row complicated chemical, physical reactions that between they and the humectant and burning back produces are relevant.

Claims

1. a mango meat alcohol extract is characterized in that as the application of cigarette sense organ humectant: the mango meat alcohol extract that the meat alcohol extract of mango is obtained, add in the pipe tobacco as the sense organ humectant according to 0.1%～0.7% ratio of pipe tobacco gross weight.

2. mango meat alcohol extract according to claim 1 is characterized in that as the application of cigarette sense organ humectant: described mango meat alcohol extract step is in the following order extracted and is obtained:

(1) mango meat is separated fragmentation;

(2) with the ethanol of mango meat particle and percent by volume 30%～80% by volume 1: the ratio of (5～30) is mixed, under 30 ℃～70 ℃ temperature, extract 40～150min, separate with the vacuum rotary evaporator evaporation under 35 ℃～60 ℃ temperature then, the gained steam condensate is mango meat alcohol extract.