CN102095807A - Method for determining blending proportion of expanded cut stem in cut tobacco - Google Patents
Method for determining blending proportion of expanded cut stem in cut tobacco Download PDFInfo
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- CN102095807A CN102095807A CN2011100043111A CN201110004311A CN102095807A CN 102095807 A CN102095807 A CN 102095807A CN 2011100043111 A CN2011100043111 A CN 2011100043111A CN 201110004311 A CN201110004311 A CN 201110004311A CN 102095807 A CN102095807 A CN 102095807A
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Abstract
The invention relates to a method for determining the blending proportion of expanded cut stem in cut tobacco. The method comprises the following steps of: a, manually blending the expanded cut stem with other components of the cut tobacco according to a preset blending proportion and recording the proportional value; b, balancing the blended cut tobacco; c, determining the total plant alkaloid content of the balanced cut tobacco by utilizing a flow analyser; d, fitting according to the value of the total plant alkaloid content and the recorded blending proportional ratio value to obtain an expanded cut stem blending proportion predicting model; e, balancing the cut tobacco in formula content the expanded cut stem blending proportion of which is required to be determined in the actual process; f, determining the total plant alkaloid content of the balanced cut tobacco by utilizing the flow analyser; and g, calculating the expanded cut stem blending proportion of the cut tobacco in formula content in the actual process. By applying the invention, technical parameters can be provided for correctly controlling the blending proportion of the cut stem in the cut tobacco in formula content, and support can be provided for stabilizing the physical quality and sensory quality of cigarette products.
Description
Technical field
The present invention relates to a kind of method that expanded cut stem in the pipe tobacco is mixed ratio of measuring.
Background technology
Offal accounts for about 30% of tobacco leaf total amount, is the main accessory substance of tobacco industry, because tobacco stalk fibre cellulose content height, compositions such as sugar alkali are lower, usually the filling value that is used as stem or laminates and prop up with the increase cigarette helps falling Jiao, and this also is one of main path of offal utilization.
Respectively mixing in cutting filler joined the owner and will be comprised: leaf silk, expansive cut tobacco, expanded cut stem, paper process thin slice, roll-in method thin slice, sheet and shreds etc.Present domestic tobacco enterprise adopts the demi-inflation stem as the batching pipe tobacco and roll into tobacco product and prop up usually, but mix a certain proportion of expanded cut tobacco when cutting filler in after, smoke components can change, and influences bigger to the aesthetic quality of cigarette.Therefore, the ratio of mixing expanded cut stem during control cuts filler is to significant with control finished product tobacco quality.
Chinese patent application 200610018051.2,200610018050.8,200910065223.5 all be to utilize the middle difference that cuts filler to mix the difference that combo is divided the tobacco apparent density, adopting the method that disposes the different densities organic solvent that difference in cutting filler is mixed the combo branch separates, and then obtain to mix and join thing and in cutting filler, mix mixing ratio, since the density of expansive cut tobacco with cut filler in other mix that to join the thing difference bigger, therefore utilize the method for above-mentioned patent effectively to separate to expansive cut tobacco, but the density difference of expanded cut stem and Ye Si and sheet and shreds is very little in the real process, is difficult for selecting the organic solvent of proper density that it is separated.
And the method that Chinese patent application 200610018085.8 relates to is by dividing different external appearance characteristics to carry out craft to select according to respectively mixing combo in cutting filler under magnifier, therefore the numerous and diverse and inefficiency of process need find a kind of simple effective method that expanded cut stem in the pipe tobacco is mixed ratio and measure.
Summary of the invention
Expanded cut stem was mixed the method for ratio during a kind of mensuration that purpose of the present invention provides specially at existing problem in the above-mentioned prior art just cut filler.
Purpose of the present invention can realize by following technique measures:
A kind ofly measure the method that expanded cut stem in the pipe tobacco is mixed ratio, this method comprises the steps:
A, manually mix ratio expanded cut stem and all the other components that cut filler are mixed and joined, and record is set and mixed ratio value in setting;
B, will mixing pipe tobacco after joining, to put into temperature be 20 ± 2 ℃, and humidity is balance 24 ± 2 hours in 65% ± 5% the environment;
C, utilize the total alkaloid content of pipe tobacco after the flow analysis instrument determination step b balance;
D, utilize the total alkaloid content value that step c records and the ratio value of mixing of step a record to carry out match, obtain expanded cut stem and mix scale prediction model: Y=R1-R2*X,
In the formula: Y: be the ratio of mixing of expanded cut stem
R1, R2: be concrete fitting parameter
X: be total alkaloid content;
E, get real process and need measure expanded cut stem and mix cutting filler of ratio, putting it into temperature is 20 ± 2 ℃, and humidity is balance 24 ± 2 hours in 65% ± 5% the environment;
F, utilize the total alkaloid content of pipe tobacco after the flow analysis instrument determination step e balance;
G, the expanded cut stem that utilizes steps d to obtain are mixed the scale prediction model, calculate the real process expanded cut stem that cuts filler and mix ratio.
The assay method of total alkaloid described in the present invention, according to tobacco business standard YC/T160-2002 tobacco and tobacco product total alkaloid mensuration---continuous flow method is measured.
The present invention mixes ratio for expanded cut stem in the simple and effective mensuration pipe tobacco a kind of comparatively complete, feasible method is provided, the employing of the method can be correct control cut filler in the ratio of mixing of expanded cut stem technical parameter is provided, and the physical quality and the aesthetic quality that can be the stable roll tobacco product provide support.
Description of drawings
Fig. 1 mixes ratio and total alkaloid content correlationship fitting data figure for expanded cut stem.
Embodiment
The present invention is described further below in conjunction with embodiment, but does not limit the present invention:
Sample is domestic certain trade mark Virginian-type cigarette
1, manually mix ratio expanded cut stem and all the other components that cut filler are mixed and joined, and record is set and mixed ratio value in setting;
2, will mixing pipe tobacco after joining, to put into temperature be 20 ± 2 ℃, and humidity is balance 24 ± 2 hours in 65% ± 5% the environment;
3, utilize the flow analysis instrument to measure the total alkaloid content of pipe tobacco after the balance, the result is:
Numbering | Mix mixing ratio (%) | Leaf silk content (g) | Expanded cut stem content (g) | Total alkaloid content (%) |
B1 | 8 | 23 | 2 | 2.23 |
B2 | 12 | 22 | 3 | 2.22 |
B3 | 16 | 21 | 4 | 2.05 |
B4 | 20 | 20 | 5 | 1.94 |
B5 | 24 | 19 | 6 | 1.87 |
B6 | 28 | 18 | 7 | 1.85 |
B7 | 32 | 17 | 8 | 1.79 |
B8 | 36 | 16 | 9 | 1.66 |
B9 | 40 | 15 | 10 | 1.61 |
B10 | 44 | 14 | 11 | 1.49 |
4, obtain expanded cut stem and mix scale prediction model: Y=1.163-0.483*X, coefficient R
2=97.8%, see accompanying drawing 1;
5, get real process and need measure expanded cut stem and mix cutting filler of ratio, putting it into temperature is 20 ± 2 ℃, and humidity is balance 24 ± 2 hours in 65% ± 5% the environment;
6, utilize the flow analysis instrument to measure the total alkaloid content of pipe tobacco after the balance;
7, the expanded cut stem that utilizes step 4 to obtain is mixed the scale prediction model, and expanded cut stem was mixed ratio during calculating acquisition real process cut filler, and result of calculation is:
Numbering | Total alkaloid content (%) | Expanded cut stem is mixed ratio (%) |
E1 | 1.80 | 29.6 |
E2 | 1.80 | 29.6 |
E3 | 1.80 | 29.6 |
E4 | 1.77 | 30.8 |
E5 | 1.81 | 28.9 |
E6 | 1.80 | 29.4 |
E7 | 1.77 | 30.8 |
E8 | 1.83 | 27.9 |
E9 | 1.80 | 29.6 |
E10 | 1.78 | 30.3 |
Average | 1.79 | 29.7 |
Standard deviation | 0.02 | 0.9 |
Claims (1)
1. measure the method that expanded cut stem in the pipe tobacco is mixed ratio for one kind, it is characterized in that this method may further comprise the steps:
A, manually mix ratio expanded cut stem and all the other components that cut filler are mixed and joined, and record is set and mixed ratio value in setting;
B, will mixing pipe tobacco after joining, to put into temperature be 20 ± 2 ℃, and humidity is balance 24 ± 2 hours in 65% ± 5% the environment;
C, utilize the total alkaloid content of pipe tobacco after the flow analysis instrument determination step b balance;
D, utilize the total alkaloid content value that step c records and the ratio value of mixing of step a record to carry out match, obtain expanded cut stem and mix scale prediction model: Y=R1-R2*X,
In the formula: Y: be the ratio of mixing of expanded cut stem
R1, R2: be concrete fitting parameter
X: be total alkaloid content;
E, get real process and need measure expanded cut stem and mix cutting filler of ratio, putting it into temperature is 20 ± 2 ℃, and humidity is balance 24 ± 2 hours in 65% ± 5% the environment;
F, utilize the total alkaloid content of pipe tobacco after the flow analysis instrument determination step e balance;
G, the expanded cut stem that utilizes steps d to obtain are mixed the scale prediction model, calculate the real process expanded cut stem that cuts filler and mix ratio.
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CN2011100043111A CN102095807A (en) | 2011-01-11 | 2011-01-11 | Method for determining blending proportion of expanded cut stem in cut tobacco |
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CN2011100043111A CN102095807A (en) | 2011-01-11 | 2011-01-11 | Method for determining blending proportion of expanded cut stem in cut tobacco |
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Cited By (11)
Publication number | Priority date | Publication date | Assignee | Title |
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CN102519819A (en) * | 2011-10-20 | 2012-06-27 | 中国烟草总公司郑州烟草研究院 | Method for measuring mixing uniformity of tobacco shreds of cigarettes |
CN102519821A (en) * | 2011-10-31 | 2012-06-27 | 江苏中烟工业有限责任公司 | Method for evaluating cut tobacco mixing uniformity |
CN103115842A (en) * | 2013-03-04 | 2013-05-22 | 江苏中烟工业有限责任公司 | Method for measuring recycled stem backfilling rate |
CN103263069A (en) * | 2013-05-09 | 2013-08-28 | 红云红河烟草(集团)有限责任公司 | Method for representing blending uniformity of cut leaves, expanded cut tobacco and cut stems |
CN103645111A (en) * | 2013-12-04 | 2014-03-19 | 红塔烟草(集团)有限责任公司 | Determination method for blending ratio of expanded cut tobaccos in cut tobaccos |
CN104132937A (en) * | 2014-07-08 | 2014-11-05 | 国家烟草质量监督检验中心 | Continuous flow method for measuring total alkaloid in tobacco or tobacco products |
CN108444861A (en) * | 2018-03-15 | 2018-08-24 | 江苏鑫源烟草薄片有限公司 | A kind of assay method of reconstruction stem product backfill rate |
CN109297854A (en) * | 2018-09-20 | 2019-02-01 | 云南中烟工业有限责任公司 | A kind of stem run in item silk mixes the rapid assay methods of ratio in fact |
CN111289444A (en) * | 2020-03-03 | 2020-06-16 | 红云红河烟草(集团)有限责任公司 | Method for determining cut stem content in cut tobacco based on color difference method |
CN111307724A (en) * | 2020-03-03 | 2020-06-19 | 红云红河烟草(集团)有限责任公司 | Method for establishing model for determining cut stem content in cut tobacco based on color difference method |
CN114113391A (en) * | 2021-11-24 | 2022-03-01 | 贵州中烟工业有限责任公司 | Method for detecting content of expansion medium |
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CN101095556A (en) * | 2006-06-30 | 2008-01-02 | 湖南中烟工业公司 | Processing method of tobacco stem and the device thereof |
CN101581648A (en) * | 2009-06-19 | 2009-11-18 | 中国烟草总公司郑州烟草研究院 | Method for testing tobacco flakes mixing ratio of cut tobacco blend |
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Cited By (18)
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CN102519819B (en) * | 2011-10-20 | 2013-07-10 | 中国烟草总公司郑州烟草研究院 | Method for measuring mixing uniformity of tobacco shreds of cigarettes |
CN102519819A (en) * | 2011-10-20 | 2012-06-27 | 中国烟草总公司郑州烟草研究院 | Method for measuring mixing uniformity of tobacco shreds of cigarettes |
CN102519821A (en) * | 2011-10-31 | 2012-06-27 | 江苏中烟工业有限责任公司 | Method for evaluating cut tobacco mixing uniformity |
CN102519821B (en) * | 2011-10-31 | 2013-07-10 | 江苏中烟工业有限责任公司 | Method for evaluating cut tobacco mixing uniformity |
CN103115842B (en) * | 2013-03-04 | 2015-05-13 | 江苏中烟工业有限责任公司 | Method for measuring recycled stem backfilling rate |
CN103115842A (en) * | 2013-03-04 | 2013-05-22 | 江苏中烟工业有限责任公司 | Method for measuring recycled stem backfilling rate |
CN103263069A (en) * | 2013-05-09 | 2013-08-28 | 红云红河烟草(集团)有限责任公司 | Method for representing blending uniformity of cut leaves, expanded cut tobacco and cut stems |
CN103645111A (en) * | 2013-12-04 | 2014-03-19 | 红塔烟草(集团)有限责任公司 | Determination method for blending ratio of expanded cut tobaccos in cut tobaccos |
CN104132937A (en) * | 2014-07-08 | 2014-11-05 | 国家烟草质量监督检验中心 | Continuous flow method for measuring total alkaloid in tobacco or tobacco products |
CN104132937B (en) * | 2014-07-08 | 2017-09-05 | 国家烟草质量监督检验中心 | A kind of method that total alkaloid in tobacco or tobacco product is determined with continuous flow method |
CN108444861A (en) * | 2018-03-15 | 2018-08-24 | 江苏鑫源烟草薄片有限公司 | A kind of assay method of reconstruction stem product backfill rate |
CN109297854A (en) * | 2018-09-20 | 2019-02-01 | 云南中烟工业有限责任公司 | A kind of stem run in item silk mixes the rapid assay methods of ratio in fact |
CN111289444A (en) * | 2020-03-03 | 2020-06-16 | 红云红河烟草(集团)有限责任公司 | Method for determining cut stem content in cut tobacco based on color difference method |
CN111307724A (en) * | 2020-03-03 | 2020-06-19 | 红云红河烟草(集团)有限责任公司 | Method for establishing model for determining cut stem content in cut tobacco based on color difference method |
CN111289444B (en) * | 2020-03-03 | 2023-03-07 | 红云红河烟草(集团)有限责任公司 | Method for determining cut stem content in cut tobacco based on color difference method |
CN111307724B (en) * | 2020-03-03 | 2023-03-14 | 红云红河烟草(集团)有限责任公司 | Method for establishing model for determining cut stem content in cut tobacco based on color difference method |
CN114113391A (en) * | 2021-11-24 | 2022-03-01 | 贵州中烟工业有限责任公司 | Method for detecting content of expansion medium |
CN114113391B (en) * | 2021-11-24 | 2024-03-26 | 贵州中烟工业有限责任公司 | Method for detecting content of expansion medium |
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Application publication date: 20110615 |