CN102078337A - Propolis natural reduction extraction process method - Google Patents
Propolis natural reduction extraction process method Download PDFInfo
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- CN102078337A CN102078337A CN2011100071573A CN201110007157A CN102078337A CN 102078337 A CN102078337 A CN 102078337A CN 2011100071573 A CN2011100071573 A CN 2011100071573A CN 201110007157 A CN201110007157 A CN 201110007157A CN 102078337 A CN102078337 A CN 102078337A
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Abstract
The invention relates to a propolis extraction process method, in particular to a propolis natural reduction extraction process method. The propolis natural reduction extraction process method is characterized by comprising the following steps of: performing low-temperature treatment on crude propolis at the temperature of -18 DEG C; grinding the crude propolis into 50 meshes at a low temperature; removing visible metal by using a high-efficiency metal detector; dissolving the crude propolis into water according to the weight ratio of the crude propolis to the water of 1:2 at the temperature of 60 DEG C for 30 minutes; standing for 24 hours; filtering 80-mesh mixture; performing freeze drying to obtain water extraction propolis powder for later use; dissolving the crude propolis into absolute ethanol according to the weight ratio of the crude propolis to the absolute ethanol of 1:4; allowing the mixture to pass through a colloid mill; dissolving the mixture by using a sol tank at the temperature of 40 DEG C for 2 hours; standing for 24 hours; filtering 200-mesh mixture; performing vacuum concentration and freeze grinding to obtain alcohol extraction propolis powder for later use; drying undissolved substances in the water extraction propolis powder and the alcohol extraction propolis powder under reduced pressure for 1 hour; mixing the undissolved substances and oil according to the ratio of the undissolved substances to the oil of 1:10 to dissolve; heating the mixture to 60 DEG C; dissolving for 1 hour; and filtering 100-mesh mixture to obtain oil soluble propolis. The propolis natural reduction extraction process method has the advantages of simple extraction method, simpleness and convenience in operation, capacity of maintaining nutritious ingredients, time saving and simple program.
Description
Technical field: the present invention relates to the propolis process for extracting, be specially a kind of propolis and reduce process for extracting naturally.
Background technology: present most of propolis extracts all uses 95% ethanol extraction propolis, causes extraction time long because of it contains water, the temperature height.Influence the effective ingredient of propolis.The composition of propolis and complexity thereof, known just have hundreds of.Only be difficult to effective bee glue components is extracted fully with ethanol extraction.Even extracted propolis, also can lose a lot of primary nutritional labelings.
Summary of the invention: the object of the present invention is to provide a kind of extracting method propolis simple, easy and simple to handle, that keep nutrition to reduce process for extracting naturally.The object of the present invention is achieved like this: at first hair glue is put-18 ℃ of K cryogenic treatment, be crushed to 50 orders at low temperatures, screen out visible metal with the efficient metal detector, hair glue and water are to dissolve with 1: 2 by weight, with 60 ℃ of dissolving 30min, leave standstill 24h, filter 80 orders, lyophilization, obtaining water, to carry propolis powder standby.Hair glue and dehydrated alcohol dissolved, cross colloid mill with 1: 4 by weight, and with 40 ℃ of glue pots dissolving 2h, leave standstill 24h and filter 200 orders, vacuum concentration, freezing and pulverizing, it is standby to obtain the alcohol extraction propolis powder.Water is carried insoluble matter drying under reduced pressure 1h in propolis powder and the alcohol extraction propolis powder, with oil with 1: 10 mixed dissolution, heat 60 ℃ the dissolving 1h filter 100 orders, obtain oil-soluble propolis.Advantage of the present invention is: extracting method is simple, easy and simple to handle, keep nutrition, saves time, single between program.
The specific embodiment: at first hair glue is put-18 ℃ of K cryogenic treatment, be crushed to 50 orders at low temperatures, screen out visible metal with the efficient metal detector, hair glue and water with 60 ℃ of dissolving 30min, leave standstill 24h with by weight with dissolving in 1: 2, filter 80 orders, lyophilization, obtaining water, to carry propolis powder standby.Hair glue and dehydrated alcohol dissolved, cross colloid mill with 1: 4 by weight, and with 40 ℃ of glue pots dissolving 2h, leave standstill 24h and filter 200 orders, vacuum concentration, freezing and pulverizing, it is standby to obtain the alcohol extraction propolis powder.Water is carried insoluble matter drying under reduced pressure 1h in propolis powder and the alcohol extraction propolis powder, with oil with 1: 10 mixed dissolution, heat 60 ℃ the dissolving 1h filter 100 orders, obtain oil-soluble propolis.
Claims (3)
1. a propolis reduces process for extracting naturally, it is characterized in that: at first hair glue is put-18 ℃ of K cryogenic treatment, be crushed to 50 orders at low temperatures, screen out visible metal with the efficient metal detector, hair glue and water dissolve 30min with by weight with dissolving in 1: 2 with 60 ℃, leave standstill 24h, filter 80 orders, lyophilization, obtaining water, to carry propolis powder standby.
2. a kind of propolis according to claim 1 reduces process for extracting naturally, it is characterized in that: hair glue and dehydrated alcohol by weight with dissolving in 1: 4, cross colloid mill, dissolve 2h with 40 ℃ of glue pots, leave standstill 24h and filter 200 orders, vacuum concentration, freezing and pulverizing, it is standby to obtain the alcohol extraction propolis powder.
3. a kind of propolis according to claim 1 reduces process for extracting naturally, it is characterized in that: water is carried insoluble matter drying under reduced pressure 1h in propolis powder and the alcohol extraction propolis powder, with oil with 1: 10 mixed dissolution, heat 60 ℃ the dissolving 1h filter 100 orders, obtain oil-soluble propolis.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011100071573A CN102078337A (en) | 2011-01-14 | 2011-01-14 | Propolis natural reduction extraction process method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011100071573A CN102078337A (en) | 2011-01-14 | 2011-01-14 | Propolis natural reduction extraction process method |
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| Publication Number | Publication Date |
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| CN102078337A true CN102078337A (en) | 2011-06-01 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN2011100071573A Pending CN102078337A (en) | 2011-01-14 | 2011-01-14 | Propolis natural reduction extraction process method |
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| CN (1) | CN102078337A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103125802A (en) * | 2013-03-11 | 2013-06-05 | 宁夏原野蜂业有限公司 | Nutrition taking propolis cream, medlar cream, honey and desert ginseng powder as raw materials and preparation method of nutrition |
| CN106213386A (en) * | 2016-07-25 | 2016-12-14 | 福建省神蜂科技开发有限公司 | A kind of bee glue soft capsule and preparation method thereof |
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| CN1342464A (en) * | 2001-09-18 | 2002-04-03 | 姜德勇 | Antivirus antioxidizing active extract of proplis and its molecular inclusion compound |
| CN1555814A (en) * | 2004-01-08 | 2004-12-22 | 兰州大学 | Extracting method of propolis effective component and its use |
| CN101049320A (en) * | 2007-05-11 | 2007-10-10 | 山东大学 | Buccal tablets of extractive of propolis alcohol |
| CN101081234A (en) * | 2007-02-02 | 2007-12-05 | 北京蜜香村蜂胶有限责任公司 | Method for preparation of claybank propolis soft capsules |
| CN101199554A (en) * | 2007-12-24 | 2008-06-18 | 中国农业科学院蜜蜂研究所 | Oil-soluble propolis soft capsule and preparing method thereof |
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2011
- 2011-01-14 CN CN2011100071573A patent/CN102078337A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1342464A (en) * | 2001-09-18 | 2002-04-03 | 姜德勇 | Antivirus antioxidizing active extract of proplis and its molecular inclusion compound |
| CN1555814A (en) * | 2004-01-08 | 2004-12-22 | 兰州大学 | Extracting method of propolis effective component and its use |
| CN101081234A (en) * | 2007-02-02 | 2007-12-05 | 北京蜜香村蜂胶有限责任公司 | Method for preparation of claybank propolis soft capsules |
| CN101049320A (en) * | 2007-05-11 | 2007-10-10 | 山东大学 | Buccal tablets of extractive of propolis alcohol |
| CN101199554A (en) * | 2007-12-24 | 2008-06-18 | 中国农业科学院蜜蜂研究所 | Oil-soluble propolis soft capsule and preparing method thereof |
Non-Patent Citations (3)
| Title |
|---|
| 梁宝军等: "温浸醇提除蜡蜂胶总黄酮的工艺研究", 《中国实验方剂学杂志》 * |
| 石憬林: "蜂胶牙膏的制法", 《中国蜂业》 * |
| 钱立立等: "蜂胶中总黄酮的提取及含量测定", 《黑龙江医药》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103125802A (en) * | 2013-03-11 | 2013-06-05 | 宁夏原野蜂业有限公司 | Nutrition taking propolis cream, medlar cream, honey and desert ginseng powder as raw materials and preparation method of nutrition |
| CN106213386A (en) * | 2016-07-25 | 2016-12-14 | 福建省神蜂科技开发有限公司 | A kind of bee glue soft capsule and preparation method thereof |
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Application publication date: 20110601 |