CN102070980B - Taxus chinensis polyurethane paint - Google Patents

Taxus chinensis polyurethane paint Download PDF

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CN102070980B
CN102070980B CN 201110007197 CN201110007197A CN102070980B CN 102070980 B CN102070980 B CN 102070980B CN 201110007197 CN201110007197 CN 201110007197 CN 201110007197 A CN201110007197 A CN 201110007197A CN 102070980 B CN102070980 B CN 102070980B
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李乾元
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李乾元
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Abstract

本发明涉及一种红豆杉聚氨酯漆,由主漆、固化剂、稀释剂按重量分数1∶0.5∶0.4比例混合制成。 The present invention relates to a polyurethane paint yew, the main lacquer, curing agent, diluent fraction 1:0.5:0.4 weight ratio blend. 本发明通过多重复合加注紫杉醇因子的方式,能使制得的聚氨酯漆产品除了具有较高的硬度、丰满度、附着力、抗高温回粘性、耐水性及良好的施工应用性外,且可迅速分解吸收甲醛等有机化合物。 The present invention multiple composite filling factor of paclitaxel manner, can prepare polyurethane paint products in addition to having a high hardness, fullness, adhesion, high temperature adhesive back, and good water resistance of the outer construction applications, and may be decompose rapidly absorb formaldehyde and other organic compounds.

Description

红豆杉聚氨酯漆 Yew polyurethane paint

[0001] 技术领域:本发明涉及一种油漆,特别是一种红豆杉聚氨酯漆。 [0001] Technical Field: The present invention relates to a paint, in particular a polyurethane paint yew.

[0002] 背景技术:室内装饰装修需要大量油漆,目前市面上一般是普通油性漆或水性漆,并没有吸除有害物的性能。 [0002] BACKGROUND: interior decoration requires a lot of paint, currently on the market are generally ordinary oil paint or water-based paint, and no suction performance pests. 产品主要包括聚氨酯分散体型和水性丙烯酸乳液型,一般油漆虽然施工简便、成本较低,但气味大,施工后很久还没挥发本身气味,更不用说要吸收其他物质的气味了,为提高漆的环保性能,必须研制出能吸收室内多种有害VOC的高性能水性漆。 The major products include polyurethane dispersion type and water-based acrylic emulsion type, general paint though construction is simple, low cost, but the smell, not long after construction volatile odor itself, let alone to absorb the odors of other substances, in order to improve paint environmental performance, have developed a variety of high-performance water can absorb indoor harmful VOC paint of. 接近在室内置放植物来净化空气所产生的效果。 Placed near the indoor plants to purify the air effect generated.

[0003] 发明内容:针对上述现有技术的不足,本发明提供了一种环保无害且具有吸附清除污染物的红豆杉聚氨酯漆。 [0003] Summary of the invention: the deficiency of the above-described prior art, the present invention provides an environmentally friendly and has an adsorption remove contaminants Taxus polyurethane paint.

[0004] 为实现上述目的,本发明采用的技术方案是:红豆杉聚氨酯漆,由主漆、固化剂、稀释剂按重量分数1: 0.5: 0.4比例混合制成。 [0004] To achieve the above object, the technical solution of the present invention is that: yew polyurethane paint, a main paint, curing agent, diluent, by weight fraction of 1: 0.5: 0.4 ratio blend.

[0005] 主漆由无苯环保树脂、红豆杉提炼的紫杉醇因子、消泡剂、增稠剂、表面流变剂、润湿分散剂、消光剂、颜料、填料、溶剂、及其他助剂组成;其制备方法为:在不锈钢容器中加入无苯环保树脂,开动搅拌,分别投入各种助剂和颜料、填料等,然后充分分散,最后加及紫杉醇因子,再分散,检测合格后过滤。 [0005] a main paint benzene green resin, Taxus extract paclitaxel factor, defoamers, thickeners, surface rheological agent, wetting and dispersing agents, matting agents, pigments, fillers, solvents, and other additives ; the preparation method as: benzene green resin was added in a stainless steel container, stirring was started, and various additives were put pigments, fillers and the like, and then well dispersed, and finally add and taxol factor, redispersion, after passing the filter.

[0006] 固化剂由异氰酸酯物质及助剂组成;其制备方法为:在不锈钢容器中按配方量将选取的异氰酸酯物质及助剂等加入到溶剂中,搅拌均匀后过滤。 [0006] The isocyanate curing agent and additives material composition; the preparation method: In a stainless steel container according to the formula amount of an isocyanate selected materials and additives added to the solvent, stir and filter.

[0007] 稀释剂由醋酸丁酯和丙二醇甲醚丙酸酯按照重量份数3: I组成;其制备方法为:在不锈钢容器中按配方量加入醋酸丁酯和丙二醇甲醚丙酸酯溶剂,搅拌均匀后过滤。 [0007] The diluent of butyl acetate and propylene glycol methyl ether propionate in a weight parts 3: I composition; The preparation method as follows: In a stainless steel container according to the formula amount of butyl acetate was added and the solvent is propylene glycol methyl ether propionate, stir filtration.

[0008] 本发明通过多重复合加注紫杉醇因子的方式,能使制得的聚氨酯漆产品除了具有较高的硬度、丰满度、附着力、 抗高温回粘性、耐水性及良好的施工应用性外,且可迅速分解吸收甲醛等有机化合物。 [0008] The present invention multiple composite filling factor of paclitaxel manner, can prepare polyurethane paint products in addition to having a high hardness, fullness, adhesion, high temperature adhesive back, water resistance, and good applicability outer Construction and can be quickly broken down and absorbed organic compounds such as formaldehyde.

具体实施方式: Detailed ways:

[0009] 1、主漆 [0009] 1, the main paint

[0010] 1.11无苯环保树脂 [0010] 1.11 benzene green resin

[0011] 本发明选用的是刷涂性好,耐黄变性佳、干燥速度快,硬度高且不含苯类溶剂的NOVALKYD 3801 (DSM公司),其用量为主漆总重量的48%。 [0011] The present invention is selected brushing good, good resistance to yellowing, fast drying, high hardness and free from benzene solvent NOVALKYD 3801 (DSM company) in an amount of 48% based on the total weight of the paint.

[0012] 1.12 消泡剂 [0012] 1.12 defoamers

[0013] 消泡剂是用来在溶剂型涂料系统中在涂料生产、包装和应用期间防止泡沫和起泡生成。 [0013] a defoaming agent is used to prevent foaming and the foam generated during paint production, packaging and application of solvent-based coating systems. 消泡剂加入量须经过试验确定,若加入量太少,起不到想要的消泡效果;太多,则会引起漆膜缩孔及重涂性欠佳等病态。 Defoamers amount subject to testing to determine if the amount is too small, will not achieve the desired anti-foaming effect; too much, it will cause shrinkage and re-coating paint and other poor sick. 可选取BYK系列消泡剂,用量为0.1〜0.3%左右为佳。 Defoamer BYK series can be selected, preferably in an amount of about 0.1~0.3%. 选取BYK-066N,其用量为主漆总重量的0.2%。 Select BYK-066N, in an amount of 0.2% based on the total weight of the paint.

[0014] 1.13 增稠剂 [0014] 1.13 thickeners

[0015] 增稠剂的主要作用有:提供静态粘度,储存时防止固体份的沉降;满足施工要求,提供流平和流挂的平衡;提高剪粘度,赋予漆膜良好的厚度和丰满度等。 The main role of [0015] thickener: providing a static viscosity to prevent sedimentation upon storage of the solid; meet the construction requirements, to provide the balance of flow and sagging; increase shear viscosity, to impart good film thickness and fullness. 溶剂型涂料常用流变增稠剂聚酰胺蜡、有机改性膨润土、气相二氧化硅、氢化蓖麻油等。 Solvent-based coatings commonly used polyamide wax rheological thickeners, organic modified bentonite, fumed silica, hydrogenated castor oil and the like. 无苯环保涂料可选择气相二氧化硅、有机改性膨润土等如M-5、SD-1。 Alternatively benzene green paint fumed silica, organically modified bentonite, such as M-5, SD-1. 使用量根据产品粘度需要来确定。 The amount of the product is determined according to the desired viscosity. 选取SD-1,其用量为主漆总重量的0.8%。 Select SD-1, in an amount of 0.8% based on the total weight of the paint.

[0016] 1.14表面流变剂 [0016] surface of the rheological agent 1.14

[0017] 它的主要作用为改善漆的流平性和漆膜表面的平整度,提高漆膜手感、抗划伤性能和抗粘连性。 [0017] Its main role is to improve the smoothness and leveling of the paint film surface, improve the film feel, scratch resistance and blocking resistance. 在哑光漆中还可以改善消光粉的定向排布,使漆膜光泽均匀、手感滑爽。 In matt paints may also improve the orientation of matting arrangement, a uniform paint film luster, smooth feel. 选用时应注意它与体系的相容性,如果使用不当,可能会产生气泡和缩孔,并影响重涂性及层间附着力。 Selection should pay attention to its compatibility with the system, if used improperly, bubbles may be generated and shrinkage, and impact resistance and inter-layer adhesion of recoat. 可用的表面流变剂主要是有机硅类、有机氟类等。 Rheological agents useful surface primarily silicone-based, fluorine-based organic. 可选择不同类型的表面流变剂组合使用,以求最佳板面效果。 Alternatively the surface of different types of rheological agent used in combination, in order to board the best results. 实验表明,TEGO GLIDE系列产品与BYK333组合使用,力口量约为0.2%,膜面效果最好。 Experiments show that, TEGO GLIDE series combination with BYK333, opening force of about 0.2%, the best film surface. 选用BYK333,其用量为主漆总重量的0.1%。 Selection BYK333, in an amount of 0.1% based on the total weight of the paint.

[0018] 1.15润湿分散剂 [0018] 1.15 wetting and dispersing agents

[0019] 润湿剂能降低液体基料与颜、填料间的界面张力,它吸附于颜、填料颗粒表面取代原附着于颜、填料表面的空气和水,使漆料易于在颜、填料颗粒表面形成包覆膜。 [0019] The wetting agent reduces the interfacial tension between the liquid base and pigment, a filler, it is adsorbed on the pigment, filler particles adhered to the surface to replace the original color, air and water filler surface so that the pigment is easy to paint, filler particles surface coating film. 在机械力作用下,颜、填料聚集体和附聚体被解聚集成为原级粒子大小,并被润湿剂和漆料包覆粒子表面而减少了颜、填料颗粒间的吸引力;分散剂能通过空间位阻效应和电荷稳定作用将解聚集后的颜、填料粒子稳定的分散在涂料中,不再聚集或絮凝,保持颜、填料分散体系长久的稳定性。 Under mechanical force, pigments, fillers, aggregates and agglomerates are deagglomerated to become primary-particle size, and wetting agents and surface paint coating particles reduces the attractive force between the pigment, filler particles; dispersing pigment, filler particles dispersed in the coating in a stable by the effect of steric stabilization and charge bit deagglomeration, no aggregation or flocculation, maintain long-term stability of the pigment, filler dispersion system. 颜、填料分散剂大多数既具有润湿功能又具有分散稳定作用。 Pigments, fillers having both wetting dispersant Most function and the dispersion stabilizing effect. 分散效果好的润湿分散剂主要有以下几类:①、低分子量的羧酸酰胺盐及酸性聚酯盐、高分子量羧酸酯类聚合物、含锚定基团的高分子聚合物或嵌段共聚物;润湿分散剂多用于实色漆中。 Good wetting and dispersing agent dispersion are the following categories: ①, salts of carboxylic acid amides and acid polyesters of low molecular weight salts, high-molecular weight carboxylic acid esters, polymers comprising groups anchored or embedded polymer block copolymers; wetting and dispersing agents are used for the solid color paint. 选用Disperbyk-167,其用量为主漆总重量的0.4%。 Selection Disperbyk-167, in an amount of 0.4% based on the total weight of the paint.

[0020] 1.16 消光剂 [0020] The matting agent 1.16

[0021] 消光剂俗称哑粉,一般为气相二氧化硅。 [0021] The matting agent known as matte, typically fumed silica. 通过综合评估消光剂分散性、抗沉降性及对涂膜的消光效果、透明度、手感等影响来选取合适产品,并根据漆的具体光泽要求来确定它的添加量。 By comprehensive evaluation dispersible matting agents, anti-settling and influence the coating of matting effect, transparency, and feeling on to select the appropriate product, and its addition amount is determined according to the specific requirements of the gloss paint. 可选取0K-607(德固萨产品)或SYL0IDC-906(格雷斯产品)等哑粉,也可几种进行搭配使用,效果较好。 Can be selected 0K-607 (Degussa product) or SYL0IDC-906 (Grace) and the like matte, it can be used with several, the better. 有些蜡粉或蜡浆有一定消光性,可适量选用。 Some have a wax or paste wax extinction, the choice may be appropriate. 选用SYL0IDC-906,其用量为主漆总重量的6%。 Selection SYL0IDC-906, an amount of 6% based on the total weight of the paint.

[0022] 1.17颜料和填料 [0022] Pigments and fillers 1.17

[0023] 颜(填)料的品种按其在油漆中的作用不同可分为着色颜料、体质颜(填)料和特种颜料四类。 [0023] pigment (filler) material varieties their role in the paint can be divided into different colored pigment, extender pigment (filler) materials and special pigments four. 着色颜料在涂料中起着色和遮盖的作用,并能提高漆膜的耐久性和耐磨性等。 Since the colored and the coloring pigment in the paint covered the role, and can improve the film durability and wear resistance. 颜色可分为黄、红、橙、紫、蓝、绿、黑及金属光泽等几类,代表性的计有铁黄、铁红、酞箐绿、酞箐蓝、氧化锌、钛白粉、碳黑、铝粉、铜粉等,主要用于配制各种实色漆如天蓝、粉红、果绿色等;体质颜料的使用可降低漆的成本,提高漆的性能和重量,如硫酸钡、滑石粉、云母粉、硅藻土、玻璃微珠等,主要用于腻子、底漆及某些色漆的配制;特种颜料包括效应颜料、荧光颜料、抗静电填料等。 Color can be divided into yellow, red, orange, purple, blue, green, black, and other types of metallic luster, yellow iron representative namely, red iron oxide, phthalocyanine green, phthalocyanine blue, zinc oxide, titanium dioxide, carbon black, aluminum powder, copper powder, mainly for the preparation of various solid colors, such as sky blue, pink, green fruit and the like; extender pigments used in paints can reduce the cost and improve the performance of the paint and the weight, such as barium sulfate, talc , mica, diatomaceous earth, glass beads, etc., mainly for the preparation of putty, primer and paint some of; special effect pigment comprises a pigment, a fluorescent pigment, an antistatic filler. 染料俗称色精,用于配制各种色泽的有色透明清漆,如仿红木、柚木、胡桃木等色。 Fine color dyes commonly known for the preparation of colored transparent varnish of various colors, such as imitation mahogany, teak, walnut and other colors. 水性漆采用的主要是水油两用的金属络合染料,选择染料时,须先检查它与体系的相容性和稳定性,不能有起粒现象。 Water-based paint is used mainly a metal complex dye of the dual-use water and oil, the choice of dye, must first check the compatibility and stability of the system it can not have graining phenomenon. 选用颜(填)料和染料时,要注意环保指标的检测和监控,特别是要防止有害重金属超标。 The selection of color (fill) material and a dye, to be noted that the detection and monitoring environmental indicators, in particular, to prevent excessive harmful heavy metals. 选用5000目滑石粉为填料,其用量为主漆总重量的10% ;选用杜邦R-706钛白粉为颜料,其用量为主漆总重量的20%。 Selection 5000 mesh talc filler in an amount of 10% based on the total weight of the paint; selection DuPont R-706 titanium dioxide pigment in an amount of 20% based on the total weight of the paint.

[0024] 1.18 溶剂 [0024] Solvent 1.18

[0025] 宜选低毒环保的丙二醇甲醚丙酸酯(PMP)、醋酸丁酯。 [0025] Yi is selected from propylene glycol methyl ether propionate (PMP), butyl acetate environmental toxicity. 选用丙二醇甲醚丙酸酯和醋酸丁酯,其用量分别为主漆总重量的5%和6.5%。 Selection ether propionate and propylene glycol butyl acetate, in an amount of 5% based on the total weight and 6.5%, respectively, of the paint.

[0026] 1.19其它助剂 [0026] Other additives 1.19

[0027] 其它助剂计有香精、打磨助剂、紫外光吸收剂、防结皮剂、催干剂等,可根据具体要求酌情添加。 [0027] Other flavor additives namely, grinding aids, ultraviolet light absorbers, anti-skinning agents, driers and the like, may be added as appropriate according to specific requirements.

[0028] 1.20紫杉醇因子 [0028] Paclitaxel factor 1.20

[0029] 选用红豆杉提炼的紫杉醇因子,其用量为主漆总重量的3%。 [0029] The factor chosen Taxus extract paclitaxel in an amount of 3% based on the total weight of the paint.

[0030] 2、固化剂 [0030] 2, a curing agent

[0031] 选取40%的醋酸丁酯、22%的Bayer N3390和38%的SAPICI 0K.DS,搅拌均匀后过滤。 [0031] Select butyl acetate 40%, 22% and 38% of the Bayer N3390 SAPICI 0K.DS, stir and filter.

[0032] 3、稀释剂 [0032] 3, diluent

[0033] 选取75%的醋酸丁酯和25%的丙二醇甲醚丙酸酯,搅拌均匀后过滤。 [0033] Select 75% butyl acetate and 25% propylene glycol methyl ether propionate, stir and filter.

Claims (8)

1.红豆杉聚氨酯漆,由主漆、固化剂、稀释剂按重量分数1: 0.5: 0.4比例混合制成;主漆由无苯环保树脂、红豆杉提炼的紫杉醇因子、消泡剂、增稠剂、表面流变剂、润湿分散剂、消光剂、颜料、填料、溶剂及其他助剂组成;其中无苯环保树脂用量为主漆总重量的48%,消泡剂用量为主漆总重量的0.1% _0.3%,增稠剂用量为主漆总重量的0.8%,表面流变剂用量为主漆总重量的0.1 %,润湿分散剂用量为主漆总重量的0.4%,消光剂用量为主漆总重量的6%,颜料用量为主漆总重量的20%,填料用量为主漆总重量的10%,溶剂用为主漆总重量的11.5%,红豆杉提炼的紫杉醇因子用量为主漆总重量的3% ;固化剂由40%异氰酸酯物质及60%的助剂组成;稀释剂由醋酸丁酯和丙二醇甲醚丙酸酯按照重量份数3: I组成。 1. Taxus polyurethane paint, a main paint, curing agent, diluent, by weight fraction of 1: 0.5: 0.4 ratio blend; primary binder resin of environmental benzene, Taxus extract paclitaxel factors, antifoaming agents, thickening agents, surface rheological agents, wetting dispersing agents, matting agents, pigments, fillers, solvents and other additives; green resin wherein the amount of benzene of 48% of the total weight based paint, an antifoaming agent based on the total weight amount of paint _0.3%, 0.1%, 0.8% thickening agent based on the total weight of the paint, the amount of surface rheological agent 0.1% based on the total weight of the paint, the amount of wetting and dispersing agent of 0.4% based on the total weight of the paint, a matting dosage of 6% based on the total weight of the paint, 20% of the amount of pigment based on the total weight of the paint, filler loading of 10% based on the total weight of the paint, a solvent of 11.5% based on the total weight of the paint, Taxus extract paclitaxel factor the amount of 3% based on the total weight of the paint; curing agent from 40% diisocyanate and 60% adjuvant materials composed; diluent of butyl acetate and propylene glycol methyl ether propionate in a weight parts 3: I composition.
2.如权利要求1所述的红豆杉聚氨酯漆,其特征在于:所述的无苯环保树脂为NOVALKYD 3801 ;消泡剂为BYK系列消泡剂;增稠剂为气相二氧化硅或有机改性膨润土。 2. Taxus polyurethane paint according to claim 1, wherein: said resin is a benzene environmental NOVALKYD 3801; defoamer BYK series of defoamer; thickening agent is fumed silica or organically modified bentonite.
3.如权利要求2所述的红豆杉聚氨酯漆,其特征在于:所述的消泡剂为BYK-066N,其用量为主漆总重量的0.2% ;增稠剂为SD-1。 3. Taxus polyurethane paint according to claim 2, wherein: said defoamer is BYK-066N, in an amount of 0.2% based on the total weight of the paint; thickeners SD-1.
4.如权利要求1所述的红豆杉聚氨酯漆,其特征在于:所述的表面流变剂为BYK333 ;所述的润湿分散剂为Disperbyk-167。 4. Taxus polyurethane paint according to claim 1, wherein: the rheological agent is BYK333 surface; as the wetting and dispersing agent Disperbyk-167.
5.如权利要求1所述的红豆杉聚氨酯漆,其特征在于:所述的消光剂为气相二氧化硅。 5. Taxus polyurethane paint according to claim 1, wherein: said matting agent is fumed silica.
6.如权利要求5所述的红豆杉聚氨酯漆,其特征在于:所述的消光剂为SYL0IDC-906。 6. Taxus polyurethane paint according to claim 5, wherein: said matting agent is SYL0IDC-906.
7.如权利要求1所述的红豆杉聚氨酯漆,其特征在于:所述的颜料为杜邦R-706钛白粉;填料为5000目滑石粉;溶剂为5%的丙二醇甲醚丙酸酯和6.5%的醋酸丁酯;其它助剂计有香精、打磨助剂、紫外光吸收剂、防结皮剂、催干剂。 7. Taxus polyurethane paint according to claim 1, wherein: the pigment is DuPont R-706 titanium dioxide; 5000 mesh filler talc; 5% of the solvent is propylene glycol methyl ether propionate and 6.5 % of the butyl acetate; other additives namely, flavor, grinding aids, ultraviolet light absorbers, anti-skinning agents, driers.
8.如权利要求1所述的红豆杉聚氨酯漆,其特征在于:所述的稀释剂为75%的醋酸丁酯和25%的丙二醇甲醚丙酸酯。 8. Taxus polyurethane paint according to claim 1, wherein: the diluent is 75% to 25% of butyl acetate and propylene glycol methyl ether propionate.
CN 201110007197 2011-01-13 2011-01-13 Taxus chinensis polyurethane paint CN102070980B (en)

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CN103059253B (en) * 2013-01-25 2014-10-08 福建农林大学 One kind of urethane sponge and its preparation method Taxus
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