CN102031192A - Dual-purpose lubricating agent for rust prevention and washing and preparation method thereof - Google Patents
Dual-purpose lubricating agent for rust prevention and washing and preparation method thereof Download PDFInfo
- Publication number
- CN102031192A CN102031192A CN2010106132006A CN201010613200A CN102031192A CN 102031192 A CN102031192 A CN 102031192A CN 2010106132006 A CN2010106132006 A CN 2010106132006A CN 201010613200 A CN201010613200 A CN 201010613200A CN 102031192 A CN102031192 A CN 102031192A
- Authority
- CN
- China
- Prior art keywords
- agent
- washing
- lubricator
- rust
- antirust
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000005406 washing Methods 0.000 title claims abstract description 42
- 238000002360 preparation method Methods 0.000 title claims description 8
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 title abstract description 11
- 230000002265 prevention Effects 0.000 title abstract description 10
- 239000000314 lubricant Substances 0.000 title abstract description 6
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 37
- 238000003756 stirring Methods 0.000 claims abstract description 24
- 239000002904 solvent Substances 0.000 claims abstract description 19
- 239000013543 active substance Substances 0.000 claims description 14
- 239000000203 mixture Substances 0.000 claims description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical group CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- 241000158728 Meliaceae Species 0.000 claims description 3
- DYUQAZSOFZSPHD-UHFFFAOYSA-N Phenylpropyl alcohol Natural products CCC(O)C1=CC=CC=C1 DYUQAZSOFZSPHD-UHFFFAOYSA-N 0.000 claims description 3
- 229910052788 barium Inorganic materials 0.000 claims description 3
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 claims description 3
- -1 phenylpropyl alcohol triazole Chemical class 0.000 claims description 3
- 229920002545 silicone oil Polymers 0.000 claims description 3
- WSFQLUVWDKCYSW-UHFFFAOYSA-M sodium;2-hydroxy-3-morpholin-4-ylpropane-1-sulfonate Chemical compound [Na+].[O-]S(=O)(=O)CC(O)CN1CCOCC1 WSFQLUVWDKCYSW-UHFFFAOYSA-M 0.000 claims description 3
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims description 3
- 239000003921 oil Substances 0.000 abstract description 26
- 238000004519 manufacturing process Methods 0.000 abstract description 10
- 238000005260 corrosion Methods 0.000 abstract description 4
- 230000007797 corrosion Effects 0.000 abstract description 4
- 239000000463 material Substances 0.000 abstract description 2
- 239000002131 composite material Substances 0.000 abstract 4
- 239000003112 inhibitor Substances 0.000 abstract 2
- 239000003381 stabilizer Substances 0.000 abstract 2
- 239000004094 surface-active agent Substances 0.000 abstract 2
- 238000010438 heat treatment Methods 0.000 abstract 1
- 230000000638 stimulation Effects 0.000 abstract 1
- 238000004140 cleaning Methods 0.000 description 8
- 239000003350 kerosene Substances 0.000 description 6
- 239000002199 base oil Substances 0.000 description 5
- 238000001514 detection method Methods 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 208000003251 Pruritus Diseases 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 239000000383 hazardous chemical Substances 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 238000010561 standard procedure Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Landscapes
- Detergent Compositions (AREA)
- Preventing Corrosion Or Incrustation Of Metals (AREA)
Abstract
The invention discloses a dual-purpose lubricating agent for rust prevention and washing, comprising the following materials in percentage by weight: 89.5%-94.8% of special solvent oil, 0.1%-0.5% of surface active agent, 0.01%-0.05% of corrosion inhibitor, 4.8%-10% of rust-preventing oil composite agent 1, 0.04%-0.1% of rust-preventing oil composite agent 2, 0.01%-0.02% of stabilizing agent and 0.02%-0.06% of latent solvent. The dual-purpose lubricating agent for rust prevention and washing is prepared by the following steps of: adding the special solvent oil to a reaction kettle; heating to about 35-45 DEG C, and stirring; sequentially adding the rust-preventing oil composite agent 1 and the rust-preventing oil composite agent 2, continuously stirring for 25-35 minutes, and then sequentially adding the corrosion inhibitor, the stabilizing agent and the latent solvent; continuously stirring for 25-35 minutes, and then adding the surface active agent; and continuously stirring for 25-35 minutes to obtain the dual-purpose lubricating agent for rust prevention and washing. The dual-purpose lubricating agent for rust prevention and washing has simple production process, no odor or stimulation on skin and good washing performance.
Description
Technical field
The present invention relates to a kind of antirust washing two with lubricator and preparation method thereof.
Background technology
When the maintenance and repair of machining and mechanical means, automobile etc., need wash machine part, equipment greasy dirt, especially weigh dirt, need have the washing composition of strong cleansing power.Washing composition not only needs to have strong cleaning performance, and need have the function that makes the rust prevention during manufacture that cleans back mechanical component, equipment surface.
Present most washing composition as base oil, is mixed with rust-preventive agent with kerosene, is used for cleaning and rust prevention during manufacture, has the dirty cleaning of good weight.But because kerosene is hazardous substance, adopt the kerosene base oil as the washing composition cleaning components, the waste resource, and exist the potential unsafe factor, and careless slightly, may lead to fire, and have dense peculiar smell, easily cause user's red swelling of the skin to itch.
Summary of the invention
The object of the present invention is to provide a kind of antirust washing two with lubricator, safety, free from extraneous odour, non-stimulated to skin, and have good cleaning performance and rust prevention during manufacture ability.
Another object of the present invention is to provide this antirust washing two preparation method with lubricator.
Antirust washing two of the present invention is with lubricator, and is composed of the following components:
Special solvent oil 89.5～94.8wt%;
Tensio-active agent 0.1～0.5wt%;
Inhibiter 0.01～0.05wt%;
The multiple agent 1 4.8～10wt% of slushing oil;
The multiple agent 2 0.04～0.1wt% of slushing oil;
Stablizer 0.01～0.02wt%;
Solubility promoter 0.02～0.06wt%.
According to the present invention, described tensio-active agent is tensio-active agent OP-10.
According to the present invention, described inhibiter is the phenylpropyl alcohol triazole.
According to the present invention, the multiple agent 1 of described slushing oil is the mixture of barium mahogany sulfonate and 5# white oil.
According to the present invention, the multiple agent 2 of described slushing oil is the mixture of zinc naphthenate and dialkyl succinylsuccinate.
According to the present invention, described stablizer is a methyl-silicone oil.
According to the present invention, described solubility promoter is an ethanol.
Antirust washing two of the present invention preparation method with lubricator may further comprise the steps:
(a), in reactor, add special solvent oil, be warmed to about 35-45 ℃, stir;
(b), successively add the multiple agent 1 of rust-preventive agent, the multiple agent 2 of rust-preventive agent, continue to stir 25-35 minute;
(c), successively add inhibiter, stablizer and solubility promoter, continue to stir 25-35 minute;
(d), add tensio-active agent continuation stirring and obtained described antirust washing two with lubricator in 25-35 minute.
According to the present invention, also comprise step (f): described antirust washing two is with lubricator filtered.
The dual-purpose lubricant production technology of antirust washing of the present invention is simple, is formed by commercially available starting material allotment, and the technology cost is low.Adopt special solvent oil to replace traditional kerosene, safe in utilization, in Working environment, have no irritating odor, non-stimulated to skin, and have good cleaning, can satisfy the rust prevention during manufacture demand.
Embodiment
Below in conjunction with specific embodiment, the present invention will be further described.Should be understood that following examples only are used to the present invention to be described but not to be used to limits the scope of the invention.
Embodiment 1
With the special solvent oil is base oil.In process of production, earlier the 91.56kg special solvent oil is joined in the reactor, be warmed to about 35-45 ℃, stir; Add the multiple agent 1 of 8kg rust-preventive agent, the multiple agent 2 of 0.06kg rust-preventive agent successively, continue to stir 25-35 minute; Add 0.03kg inhibiter, 0.01kg stablizer and 0.04kg solubility promoter successively, continue to stir 25-35 minute; Add 0.3kg tensio-active agent continuation stirring at last and obtained antirust washing two with lubricator in 25-35 minute.
Embodiment 2
With the special solvent oil is base oil.In process of production, earlier the 94.50kg special solvent oil is joined in the reactor, be warmed to about 35-45 ℃, stir; Add the multiple agent 1 of 5kg rust-preventive agent, the multiple agent 2 of 0.1kg rust-preventive agent successively, continue to stir 25-35 minute; Add 0.05kg inhibiter, 0.02kg stablizer and 0.06kg solubility promoter successively, continue to stir 25-35 minute; Add 0.27kg tensio-active agent continuation stirring at last and obtained antirust washing two with lubricator in 25-35 minute.
Embodiment 3
With the special solvent oil is base oil.In process of production, earlier the 89.5kg special solvent oil is joined in the reactor, be warmed to about 35-45 ℃, stir; Add the multiple agent 1 of 10kg rust-preventive agent, the multiple agent 2 of 0.08kg rust-preventive agent successively, continue to stir 25-35 minute; Add 0.02kg inhibiter, 0.01kg stablizer and 0.02kg solubility promoter successively, continue to stir 25-35 minute; Add 0.37kg tensio-active agent continuation stirring at last and obtained antirust washing two with lubricator in 25-35 minute.
In the present invention, special solvent oil adopts commercially available conventional products.Described tensio-active agent is preferably tensio-active agent OP-10.Described inhibiter is preferably the phenylpropyl alcohol triazole.The multiple agent 1 of described slushing oil is preferably the mixture of barium mahogany sulfonate and 5# white oil.The multiple agent 2 of described slushing oil is preferably the mixture of zinc naphthenate and dialkyl succinylsuccinate.Described stablizer is preferably methyl-silicone oil.Described solubility promoter is preferably ethanol.Should be appreciated that above content is not a limitation of the present invention, the replacement that those skilled in the art can make multiple change or be equal to according to technical scheme of the present invention.
The antirust washing two of table 1 is technical indicator with lubricator
| Project | Index |
| Outward appearance | Yellow transparent liquid |
| Smell | The minor solvent flavor |
| Density (20 ℃) kg/M 3 | 0.79～0.82 |
| Gold-plating journey ℃ | 180～250 |
| 25 ℃ of min of evaporation rate | 6～8 |
| Kinematic viscosity (40 ℃), mm 2/s | 1.5～2.0 |
| Flash-point (remaining silent), ℃ | 65～75 |
| Water-soluble soda acid | Do not have |
| The rust prevention during manufacture sky | 8～15 |
| Corrosion test (50 ℃, the T3 copper sheet, 3h) | Qualified |
| (steel disc, d) is no less than humid heat test by 49 ± 1 ℃ | 2 |
| Cleaning rate (washing greasy dirt weight/greasy dirt original weight) | 90～99％ |
The antirust washing two of above embodiment preparation is with lubricator put in storage after the barrelling after filtration.Antirust washing two is free from extraneous odour with lubricator, has no irritating odor in Working environment, and is non-stimulated to skin.Antirust washing two of the present invention is with lubricator detected, and technical indicator is as shown in table 1.Wherein kinematic viscosity detection, flash-point detection, water-soluble soda acid detection, corrosion test, humid heat test adopt GB/T265, GB/T261, GB/T259, GB/T378, GB/T2361 standard method respectively.The common method of the industry is all adopted in the detection of other technologies index.As shown in Table 1, antirust washing two of the present invention with lubricator has good cleaning rust-proof performance, can satisfy the antirust preceding washing requirement of black metal mechanical product assembling and part.
Use antirust washing two of the present invention with lubricator to clean component, equipment, cleansing power is strong, and evaporation rate is very fast, does not influence the outward appearance of metal, and the rust inhibition of short-term is arranged.The present invention adopts the marketable material special solvent oil to replace kerosene, add that tensio-active agent, inhibiter, stablizer and two kinds of multiple agent of rust-preventive agent etc. are refining to form allotment and form, improve the cleansing power of solvent oil, and free from extraneous odour, nuisanceless, non-stimulated to skin, stable performance, not perishable, safe in utilization.And can save a large amount of kerosene, cost is low, can satisfy market to antirust washing two demand with lubricator.
Claims (9)
1. an antirust washing two with lubricator is characterized in that, and is composed of the following components:
Special solvent oil 89.5～94.8wt%;
Tensio-active agent 0.1～0.5wt%;
Inhibiter 0.01～0.05wt%;
The multiple agent 1 4.8～10wt% of slushing oil;
The multiple agent 2 0.04～0.1wt% of slushing oil;
Stablizer 0.01～0.02wt%;
Solubility promoter 0.02～0.06wt%.
2. antirust washing two as claimed in claim 1 is characterized in that with lubricator described tensio-active agent is tensio-active agent OP-10.
3. antirust washing two as claimed in claim 1 is characterized in that with lubricator described inhibiter is the phenylpropyl alcohol triazole.
4. antirust washing two as claimed in claim 1 is characterized in that with lubricator the multiple agent 1 of described slushing oil is the mixture of barium mahogany sulfonate and 5# white oil.
5. antirust washing two as claimed in claim 1 is characterized in that with lubricator the multiple agent 2 of described slushing oil is the mixture of zinc naphthenate and dialkyl succinylsuccinate.
6. antirust washing two as claimed in claim 1 is characterized in that with lubricator described stablizer is a methyl-silicone oil.
7. antirust washing two as claimed in claim 1 is characterized in that with lubricator described solubility promoter is an ethanol.
8. as each described antirust washing two of claim 1～7 preparation method with lubricator, it is characterized in that, may further comprise the steps:
(a), in reactor, add special solvent oil, be warmed to about 35-45 ℃, stir;
(b), successively add the multiple agent 1 of rust-preventive agent, the multiple agent 2 of rust-preventive agent, continue to stir 25-35 minute;
(c), successively add inhibiter, stablizer and solubility promoter, continue to stir 25-35 minute;
(d), add tensio-active agent continuation stirring and obtained described antirust washing two with lubricator in 25-35 minute.
9. antirust washing two as claimed in claim 8 preparation method with lubricator is characterized in that, also comprises step (f): described antirust washing two is with lubricator filtered.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201010613200 CN102031192B (en) | 2010-12-30 | 2010-12-30 | Dual-purpose lubricating agent for rust prevention and washing and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201010613200 CN102031192B (en) | 2010-12-30 | 2010-12-30 | Dual-purpose lubricating agent for rust prevention and washing and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102031192A true CN102031192A (en) | 2011-04-27 |
| CN102031192B CN102031192B (en) | 2013-04-10 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201010613200 Expired - Fee Related CN102031192B (en) | 2010-12-30 | 2010-12-30 | Dual-purpose lubricating agent for rust prevention and washing and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102031192B (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103254785A (en) * | 2013-04-16 | 2013-08-21 | 马鞍山采石矶涂料有限公司 | Long-acting anti-rust oil and preparation method thereof |
| CN104593126A (en) * | 2015-02-09 | 2015-05-06 | 陈吉美 | Rustproof lubricant and preparation method thereof |
| CN104830491A (en) * | 2015-05-14 | 2015-08-12 | 张家港市山牧新材料技术开发有限公司 | Antirust lubricant and preparation method thereof |
| CN114317080A (en) * | 2021-12-29 | 2022-04-12 | 安美科技股份有限公司 | Ultra-precise machine tool spindle oil and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1114349A (en) * | 1994-06-22 | 1996-01-03 | 中国石油化工总公司石油化工科学研究院 | Process for preparing synthesized oil-soluble rust-preventive agent of barium sulfonate |
| EP1160308A2 (en) * | 2000-06-02 | 2001-12-05 | Nippon Mitsubishi Oil Corporation | Grease composition preventing flaking |
| CN1548505A (en) * | 2003-05-24 | 2004-11-24 | 启东尤希路化学工业有限公司 | Water soluble cutting fluid |
| CN101016497A (en) * | 2007-03-05 | 2007-08-15 | 中国石油化工集团公司 | Electrostatic spraying antirust oil |
| JP2009120636A (en) * | 2007-11-12 | 2009-06-04 | Toyota Boshoku Corp | Lubricating oil for metallic material working |
-
2010
- 2010-12-30 CN CN 201010613200 patent/CN102031192B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1114349A (en) * | 1994-06-22 | 1996-01-03 | 中国石油化工总公司石油化工科学研究院 | Process for preparing synthesized oil-soluble rust-preventive agent of barium sulfonate |
| EP1160308A2 (en) * | 2000-06-02 | 2001-12-05 | Nippon Mitsubishi Oil Corporation | Grease composition preventing flaking |
| CN1548505A (en) * | 2003-05-24 | 2004-11-24 | 启东尤希路化学工业有限公司 | Water soluble cutting fluid |
| CN101016497A (en) * | 2007-03-05 | 2007-08-15 | 中国石油化工集团公司 | Electrostatic spraying antirust oil |
| JP2009120636A (en) * | 2007-11-12 | 2009-06-04 | Toyota Boshoku Corp | Lubricating oil for metallic material working |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103254785A (en) * | 2013-04-16 | 2013-08-21 | 马鞍山采石矶涂料有限公司 | Long-acting anti-rust oil and preparation method thereof |
| CN104593126A (en) * | 2015-02-09 | 2015-05-06 | 陈吉美 | Rustproof lubricant and preparation method thereof |
| CN104830491A (en) * | 2015-05-14 | 2015-08-12 | 张家港市山牧新材料技术开发有限公司 | Antirust lubricant and preparation method thereof |
| CN114317080A (en) * | 2021-12-29 | 2022-04-12 | 安美科技股份有限公司 | Ultra-precise machine tool spindle oil and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102031192B (en) | 2013-04-10 |
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Granted publication date: 20130410 |